Synthesis, structure, and bridge-terminal exchange kinetics of pyrazolate-bridged digallium and diindium complexes containing bridging phenyl groups

Organometallics

Volumn 24, Issue 25, 2005, Pages 6184-6193

  Sirimanne, Chatu T ^a   Zheng, Wenjun ^a   Yu, Zhengkun ^a   Heeg, Mary Jane ^a   Winter, Charles H ^a  

^a WAYNE STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

NITROGEN ATOMS; PHENYL-BRIDGED COMPLEXES;

INDIUM COMPOUNDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION KINETICS; STOICHIOMETRY; SYNTHESIS (CHEMICAL); X RAY CRYSTALLOGRAPHY;

GALLIUM COMPOUNDS;

EID: 28944436355     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om050623r     Document Type: Article

References (69)

1. Crystal structure determinations of dimeric trimethylaluminum: (a) Huffman, J. C.; Streib, W. E. Chem. Commun. 1971, 911.
2. (b) Byram, S. K.; Fawcett, J. K.; Nyburg, S. C.; O'Brien, R. J. Chem. Commun. 1970, 16.
3. (c) Vranka, R. G.; Amma, E. L. J. Am. Chem. Soc. 1967, 89, 3121.
4. (d) Lewis, P. H.; Rundle, R. E. J. Chem. Phys. 1953, 21, 986.
5. (e) Evans, W. J.; Anwander, R.; Ziller, J. W. Organometallics 1995, 14, 1107.
6. Recent selected reports of structurally characterized aluminum complexes with bridging alkyl ligands: (a) Son, A. J. R.; Thorn, M. G.; Fanwick, P. E.; Rothwell, I. P. Organometallics 2003, 22, 2318.
7. (b) Hair, G. S.; Cowley, A. H.; Gorden, J. D.; Jones, J. N.; Jones, R. A.; MacDonald, C. L. B. Chem. Commun. 2003, 424.
8. (c) Yu, Z. K.; Heeg, M. J.; Winter, C. H. Chem. Commun. 2001, 353.
9. (d) Korolev, A. V.; Ihara, E.; Guzei, I. A.; Young, V. G., Jr.; Jordan, R. F. J. Am. Chem. Soc. 2001, 123, 8291.
10. (e) Wochele, R.; Klinkhammer, K. W.; Weidlein, J. Z. Anorg. Allg. Chem. 2001, 627, 1420.
11. (f) Kickham, J. E.; Guérin, F.; Stewart, J. C.; Urbanska, E.; Stephan, D. W. Organometallics 2001, 20, 1175.
12. (g) Yu, Z. K.; Wittbrodt, J. M.; Heeg, M. J.; Schlegel, H. B.; Winter, C. H. J. Am. Chem. Soc. 2000, 122, 9338.
13. (h) McGrady, G. S.; Turner, J. F. C.; Ibberson, R. M.; Prager, M. Organometallics 2000, 19, 4398.
14. (i) Chen, E. Y.-X.; Abboud, K. A. Organometallics 2000, 19, 5541.
15. (j) Kickham, J. E.; Guérin, F.; Stewart, J. C.; Stephan, D. W. Angew. Chem., Int. Ed. 2000, 39, 3263.
16. (k) Wochele, R.; Schwarz, W.; Klinkhammer, K. W.; Locke, K.; Weidlein, J. Z. Anorg. Allg. Chem. 2000, 626, 1963.
17. (l) Cottone, A., III; Scott, M. J. Organometallics 2000, 19, 5254.
18. (m) Klosin, J.; Roof, G. R.; Chen, E. Y.-X.; Abboud, K. A. Organometallics 2000, 19, 4684.
19. (n) Waezsada, S. D.; Rennekamp, C.; Roesky, H. W.; Röpken, C.; Parsini, E. Z. Anorg. Allg. Chem. 1998, 624, 987.
20. (o) Ihara, E.; Young, V. G., Jr.; Jordan, R. F. J. Am. Chem. Soc. 1998, 120, 8277.
21. (p) Waezsada, S. D.; Liu, F.-Q.; Murphy, E. F.; Roesky, H. W.; Teichert, M.; Usón, I.; Schmidt, H.-G.; Albers, T.; Parsini, E.; Noltemeyer, M. Organometallics 1997, 16, 1260.
22. (a) Malone, J. F.; McDonald, W. S. Chem. Commun. 1967, 444.
23. (b) Malone, J. F.; McDonald, W. S. J. Chem. Soc., Dalton Trans. 1972, 2646.
24. (c) Malone, J. F.; McDonald, W. S. J. Chem. Soc., Dalton Trans. 1972, 2649.
25. (d) Brauer, D. J.; Kruger, C. Z. Naturforsch. 1979, 34B, 1293.
26. (e) Barber, M.; Liptak, D.; Oliver, J. P. Organometallics 1982, 1, 1307.
27. (a) Uhl, W.; Breher, F.; Mbonimana, A.; Gauss, J.; Haase, D.; Lützen, A.; Saak, W. Eur. J. Inorg. Chem. 2001, 3059.
28. (b) Uhl, W.; Breher, F.; Lützen, A.; Saak, W. Angew. Chem., Int. Ed. 2000, 39, 406.
29. (c) Uhl, W.; Breher, F.; Grunenberg, J.; Lützen, A.; Saak, W. Organometallics 2000, 19, 4536.
30. (d) Korolev, A. V.; Guzei, I. A.; Jordan, R. F. J. Am. Chem. Soc. 1999, 127, 11605.
31. (e) Erker, G.; Albrecht, M.; Krüger, C.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
32. (f) Albright, M. J.; Butler, W. M.; Anderson, T. J.; Glick, M. D.; Oliver, J. P. J. Am. Chem. Soc. 1976, 98, 3995.
33. (g) Stucky, G. D.; McPherson, A. M.; Rhine, W. E.; Eisch, J. J.; Considine, J. L. J. Am. Chem. Soc. 1974, 96, 1941.
34. (a) Tecle, B.; Ilsley, W. H.; Oliver, J. P. Inorg. Chem. 1981, 20, 2335.
35. (b) Cowley, A. H.; Brown, D. S.; Decken, A.; Kamepalli, S. Chem. Commun. 1996, 2425.
36. Rahbarnoohi, H.; Kumar, R.; Heeg, M. J.; Oliver, J. P. Organometallics 1994, 13, 3300.
37. (a) Althoff, A.; Jutzi, P.; Lenze, N.; Neumann, B.; Stammler, A.; Stammler, H.-G. Organometallics 2002, 21, 3018.
38. (b) Scholz, S.; Green, J. C.; Lerner, H.-W.; Bolte, M.; Wagner, M. Chem. Commun. 2002, 36.
39. (c) Jutzi, P.; Lenze, N.; Neumann, B.; Stammler, H.-G. Angew. Chem., Int. Ed. 2001, 40, 1424.
40. (d) Uhl, W.; Hahn, I.; Jantschak, A.; Spies, T. J. Organomet. Chem. 2001, 637, 300.
41. (e) Hecht, E. Z. Anorg. Allg. Chem. 2000, 626, 759.
42. (f) Beachey, O. T., Jr.; Rosenblum, D. B.; Churchill, M. R.; Lake, C. H.; Krajkowski, L. M. Organometallics 1995, 14, 4402.
43. (g) Lee, B.; Pennington, W. T.; Laske, J. A.; Robinson, G. H. Organometallics 1990, 9, 2864.
44. For selected leading references, see: (a) Jones, J. N.; Macdonald, C. L. B.; Gorden, J. D.; Cowley, A. H. J. Organomet. Chem. 2003, 666, 3.
45. (b) Cowley, A. H.; Macdonald, C. L. B.; Silverman, J. S.; Gorden, J. D.; Voigt, A. Chem. Commun. 2001, 175.
46. (c) Dashti-Mommertz, A.; Neumuller, B.; Melle, S.; Haase, D.; Uhl, W. Z. Anorg. Allg. Chem. 1999, 625, 1828.
47. (d) Beachley, O. T., Jr.; Robirds, E. S.; Atwood, D. A.; Wei, P. Organometallics 1999, 18, 2561.
48. (e) Schumann, H.; Kucht, H.; Kucht, A.; Görlitz, F. H.; Dietrich, A. Z. Naturforsch. 1992, 47B, 1241.
49. (f) Beachley, O. T., Jr.; Lees, J. F.; Rogers, R. D. J. Organomet. Chem. 1991, 418, 165.
50. (g) Beachley, O. T., Jr.; Pazik, J. C.; Glassman, T. E.; Churchill, M. R.; Fettinger, J. C.; Blom, R. Organometallics 1988, 7, 1051.
51. Schulte, M.; Gabbaï, F. P. Chem. Eur. J. 2002, 8, 3802.
52. Englert, U.; Herberich, G. E.; Rosenplänter, J. Z. Anorg. Allg. Chem. 1997, 623, 1098.
53. Malone, J. F.; McDonald, W. S. J. Chem. Soc. 1970, 3362.
54. (a) Mitzel, N. W.; Lustig, C.; Berger, R. J. F.; Runeberg, N. Angew. Chem., Int. Ed. 2002, 41, 2519.
55. (b) Boese, R.; Downs, A. J.; Greene, T. M.; Hall, A. W.; Morrison, C. A.; Parsons, S. Organometallics 2003, 22, 2450.
56. (c) Blake, A. J.; Cradock, S. J. Chem. Soc., Dalton Trans. 1990, 2393.
57. (d) Amma, E. L.; Rundle, R. E. J. Am. Chem. Soc. 1958, 80, 4141.
58. Sirimanne, C. T.; Knox, J. E.; Heeg, M. J.; Schlegel, H. B.; Winter, C. H. J. Am. Chem. Soc. 2003, 125, 11152.
59. (a) Rendle, A. F.; Storr, A.; Trotter, J. Can. J. Chem. 1975, 53, 2930.
60. (b) Rendle, A. F.; Storr, A.; Trotter, J. Can. J. Chem. 1975, 53, 2944.
61. (c) Hausen, H.-D.; Locke, K.; Weidlein, J. J. Organomet. Chem. 1992, 429, C27.
62. gNMR; Version 4; Cherwell Scientific Publishing, 1997.
63. Elguéro, J.; Gonzalez, E.; Jacquier, R. Bull. Soc. Chim. Fr. 1968, 707.
64. Xiushan, Z.; Xiaolin, Z.; Lei, F.; Wentian, T. Huaxue Shiji 1997, 19, 246.
65. Viktorova, I. M.; Endovin, Yu. P.; Sheverdina, N. I.; Kocheshkov, K. A. Dokl. Akad. Nauk. SSSR 1967, 177, 103.
66. SMART, SAINT, and SADABS collection and processing programs; Bruker AXS Inc.: Madison WI.
67. Sheldrick, G. SHELX-97; University of Gottingen: Germany, 2003 and 1997.
68. Spek, A. L. PLATON; Utrecht University: The Netherlands, 2003.
69. Spek, A. L. J. Appl. Crystallogr. 2003, 36, 1.