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As noted in ref. 20 of our previous work (22), at 20°C, the CD band of 8 approximately coincident with the UV absorption at 395 nm is essentially negative, although a small, positive, longer wavelength band was apparent. At lower temperature, a new band in the UV spectrum was noted at about 320 nm. Further variable temperature CD/UV experiments down to -70°C on this sample indicate a relative decrease of the intensity of the negative Cotton effect compared with that of the positive Cotton effect. Thus, at -10°C, two CD bands, one positive and one negative, are apparent, values for both of which are given in Table 1.
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