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Tin tetrachloride (1.0 g, 3.8 mmol) was added to a solution of 1 (1.0 g, 5.3 mmol) in chloroform (10 ml) at 0°C. The mixture was stirred at 0°C for 6 h , and further 12 h at room temperature. After usual work-up, a white powder was obtained in 90% yield.
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0040981128
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+CH), 7.0-8.1 (9H,Ar).
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