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27
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note
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13C NMR (DMSO, 125 MHz): δ 27.6, 33.1, 45.7, 52.3, 54.9, 106.9, 117.4, 124.4, 126.3, 127.1, 128.5, 129.0, 130.0, 138.2, 150.4.
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28
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85031217403
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Analytical chiral HPLC was performed on a LiChroCART250-4 ChiraDex column. Eluent: methanol/water+0.1% triethylamine (pH 4.1) from 5/95 to 95/5 V/V. Flow rate: 0.8 ml/min. Detection: UV 260 nm. Retention time of R isomer was 7.5 min. Retention time of S isomer was 8.1 min.
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Analytical chiral HPLC was performed on a LiChroCART250-4 ChiraDex column. Eluent: methanol/water+0.1% triethylamine (pH 4.1) from 5/95 to 95/5 V/V. Flow rate: 0.8 ml/min. Detection: UV 260 nm. Retention time of R isomer was 7.5 min. Retention time of S isomer was 8.1 min.
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29
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0028173391
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Ostresh J.M., Husar G.M., Blondelle S.E., Dorner B., Weber P.A., Houghten R.A. Proc. Natl. Acad. Sci., USA. 91:1994;11138.
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Ostresh, J.M.1
Husar, G.M.2
Blondelle, S.E.3
Dorner, B.4
Weber, P.A.5
Houghten, R.A.6
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