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0003456901
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All isomer ratios are normalized to 100. For NMR determinations, error limits on each component are generally ±2 (e.g., 23:77 × (23± 2):(77±2)).
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0003405056
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c) The preceding papers report successful metatheses of olefinic thioethers with Schrock-type catalysts.
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A correct microanalysis of this compound was not obtained.
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We believe that E isomers likely dominate with 16 and 17 (44-42:56-58 Z/E), but the data are equivocal and the Z isomer dominates in crystalline 17 (58:42 Z/E).
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183W= 14.3%), and is not reflected in the peak multiplicity given.
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111
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0003454575
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5 signals were too weak for complete assignment.
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112
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0003339273
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note
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This signal was tentatively assigned to a dimeric product (ca. 15%) derived from intermolecular metathesis.
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