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1. For recent reviews on RCM, see: (a) Blechert, S.; Schuster, M. Angew. Chem., Int. Ed. Engl. 1997, 36, 2036;
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(b) Nguyen, S. T.; Johnson, L. K.; Grubbs, R. H.; Ziller, J. W. J. Am. Chem. Soc. 1992, 114, 3974;
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(c) Schwab, P.; Grubbs, R. H.; Ziller, J. W. J. Am. Chem. Soc. 1996, 118, 100.
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(c) Bujard, M.; Gouverneur, V.; Mioskowski, C. J. Org. Chem. 1999, 64, 2119;
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(d) Leconte, M.; Jourdan, I.; Pagano, S.; Lefebvre, F; Basset, J.-M. J. Chem. Soc., Chem. Commun. 1995, 857.
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Morrison, J. D. Ed.; Academic Press: Orlando, chap. 1
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5. Kagan, H. B. In Asymmetric Synthesis; Morrison, J. D. Ed.; Academic Press: Orlando, 1985; Vol. 5, chap. 1, 3.
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Patent US 2711403; B
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10. For the preparation of methyl allylphenylphosphinate, see: Shell Development Co., Patent US 2711403; B; Kawashima, T.; Miki, Y.; Tomita, T.; Inamoto, N. Chem. Lett. 1986, 501.
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20
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0009679813
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note
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2 under reflux, was added portionwise 2-10% of the Ru-catalyst 2a. The reaction was monitored by TLC. After maximum conversion, the reaction was concentrated and purified on silica gel.
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