메뉴 건너뛰기




Volumn 64, Issue 6, 1999, Pages 2119-2123

A highly efficient and practical synthesis of cyclic phosphinates using ring-closing metathesis

Author keywords

[No Author keywords available]

Indexed keywords

ALKADIENE; PHOSPHONIC ACID DERIVATIVE;

EID: 0033583160     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo981795j     Document Type: Note
Times cited : (89)

References (28)
  • 1
    • 0028567437 scopus 로고
    • Montchamp, J.-L.; Frost, J. W. J. Org. Chem. 1994, 59, 7596. Richard, J. P. J. Am. Chem. Soc. 1984, 106, 4926. Periana, R. A.; Motiu-DeGrood, R.; Chiang, Y.; Hupe, D. J. J. Am. Chem. Soc. 1980, 102, 3923.
    • (1994) J. Org. Chem. , vol.59 , pp. 7596
    • Montchamp, J.-L.1    Frost, J.W.2
  • 2
    • 0021471746 scopus 로고
    • Montchamp, J.-L.; Frost, J. W. J. Org. Chem. 1994, 59, 7596. Richard, J. P. J. Am. Chem. Soc. 1984, 106, 4926. Periana, R. A.; Motiu-DeGrood, R.; Chiang, Y.; Hupe, D. J. J. Am. Chem. Soc. 1980, 102, 3923.
    • (1984) J. Am. Chem. Soc. , vol.106 , pp. 4926
    • Richard, J.P.1
  • 5
    • 0027129567 scopus 로고
    • Campbell, M. M.; Carruthers, N. I.; Mickel, S. J.; Winton, P. M. J. Chem. Soc., Chem. Commun. 1984, 200. Gibbs, R. A.; Taylor, S.; Benkovic, S. J. Science 1992, 258, 803. Currie, M.; Suckling, C. J.; Zhu, L.-M.; Irvine, J.; Stimson, W. H. Tetrahedron 1995, 51, 8915.
    • (1992) Science , vol.258 , pp. 803
    • Gibbs, R.A.1    Taylor, S.2    Benkovic, S.J.3
  • 6
    • 0029122505 scopus 로고
    • Campbell, M. M.; Carruthers, N. I.; Mickel, S. J.; Winton, P. M. J. Chem. Soc., Chem. Commun. 1984, 200. Gibbs, R. A.; Taylor, S.; Benkovic, S. J. Science 1992, 258, 803. Currie, M.; Suckling, C. J.; Zhu, L.-M.; Irvine, J.; Stimson, W. H. Tetrahedron 1995, 51, 8915.
    • (1995) Tetrahedron , vol.51 , pp. 8915
    • Currie, M.1    Suckling, C.J.2    Zhu, L.-M.3    Irvine, J.4    Stimson, W.H.5
  • 11
  • 15
    • 0039530581 scopus 로고
    • Liotta, L. J.; Gibbs, R. A.; Taylor, S. D.; Benkovic, P.; Benkovic, S. J. J. Am. Chem. Soc. 1995, 117, 4729. Phillips, A. M.; Modro, T. A. Phosphorus, Sulfur, Silicon 1991, 55, 41.
    • (1991) Phosphorus, Sulfur, Silicon , vol.55 , pp. 41
    • Phillips, A.M.1    Modro, T.A.2
  • 17
    • 0344024754 scopus 로고    scopus 로고
    • note
    • 2 was chosen as the optimal solvent for the reactions with 3 based on lower overall conversion obtained in benzene. When the reaction was carried out at room temperature, the RCM of substrate 2a was slower and the overall conversion of 2a into 5a after 15 h did not go beyond 38%.
  • 18
    • 0344455909 scopus 로고    scopus 로고
    • note
    • The NMR analysis of the crude mixtures show only the desired cyclized product and the starting material with no side products. No trace of dimers was detected.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.