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0004331129
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note
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It was also attempted to perform ring-closure on oligomers containing three functionalized triazine rings, leaving only one chlorine for the cyclization reaction. The reactivity of the remaining chlorine atom to be substituted was so low that ring-closure of the compounds did not take place.
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37
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0004284939
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note
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6]DMSO did not result in any significant change in the spectrum. At 140 °C the resonances for the protons of the ethylene bridges started to coalesce.
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38
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40
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0004242750
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note
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Each sample had to be sonicated for at least three hours before an equilibrium situation was reached.
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41
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0004284530
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note
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Because of the additional hydrogen bonding and smaller loss of entropy, the binding constant was expected to increase by at least 1-2 orders of magnitude, compared with the linear systems possessing only six hydrogen bonds in ref. 18a.
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42
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0004234745
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note
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Other signals were difficult to monitor, due to serious overlap of resonances.
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43
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84987358115
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