Crystallographic and spectroscopic characterization of tetrakis(μ-N,N'- diarylformamidinato)dichlorodirhenium(III,III) compounds

European Journal of Inorganic Chemistry

Volumn , Issue 11, 1999, Pages 2095-2103

  Eglin, Judith L ^a   Lin, Chun ^b   Ren, Tong ^b   Smith, Laura ^a   Staples, Richard J ^c   Wipf, David O ^a  

^a MISSISSIPPI STATE UNIVERSITY   (United States)

^b Florida Institute of Technology   (United States)

^c HARVARD UNIVERSITY   (United States)

Author keywords

Electrochemistry; Formamidinate; Metal metal bonds; Rhenium; UV Vis spectroscopy

Indexed keywords

CHEMICAL BONDS; LIGANDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RHENIUM; RHENIUM COMPOUNDS; SUBSTITUTION REACTIONS; ULTRAVIOLET VISIBLE SPECTROSCOPY; X RAY CRYSTALLOGRAPHY;

ARYL RINGS; ARYL SUBSTITUENTS; CRYSTALLOGRAPHIC CHARACTERIZATION; FORMAMIDINATE; METAL-METAL BONDS; NMR-SPECTROSCOPY; SPECTROSCOPIC CHARACTERIZATION; SYNTHESISED; TETRAKIS; UV/ VIS SPECTROSCOPY;

ELECTROCHEMISTRY;

FORMAMIDE DERIVATIVE; LIGAND; RHENIUM COMPLEX;

ABSORPTION SPECTROSCOPY; ARTICLE; COMPLEX FORMATION; ELECTROCHEMISTRY; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 0032746402     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1099-0682(199911)1999:11<2095::aid-ejic2095>3.0.co;2-t     Document Type: Article

References (80)

1. J. Barker, M. Kilner, Coord. Chem. Rev. 1994, 133, 219-300.
2. P. J. Stewart, A. J. Blake, P. Mountford, Inorg. Chem. 1997, 36, 3616-3622.
3. J. R. Hagadorn, J. Arnold, Inorg. Chem. 1997, 36, 2928-2929.
4. S. Hao, K. Feghali, S. Gambarotta, Inorg. Chem. 1997, 36, 1745-1748.
5. A. Horton, J. deWith, Organometallics 1997, 16, 5424-5436.
6. F. A. Cotton, L. M. Daniels, C. A. Murillo, Inorg. Chem. 1993, 32, 2881-2885.
7. F. A. Cotton, R. Poli, Inorg. Chim. Acta 1988, 141, 91-98.
8. F. A. Cotton, L. M. Daniels, C. A. Murillo, X. Wang, J. Am. Chem. Soc. 1996, 118, 4830-4833.
9. F. A. Cotton, L. M. Daniels, J. H. Matonic, X. Wang, C. A. Murillo, Polyhedron 1997, 16, 1177-1191.
10. F. A. Cotton, L. M. Daniels, C. A. Murillo, X. Wang, Inorg. Chem. 1997, 36, 896-901.
11. F. A. Cotton, D. J. Maloney, J. Su, Inorg. Chim. Acta 1995, 236, 21-29.
12. F. A. Cotton, T. Ren, J. Am. Chem. Soc. 1992, 114, 2237-2242.
13. W. H. DeRoode, K. Vrieze, J. Organomet. Chem. 1977, 135, 183-193.
14. C. Lin, J. D. Protasiewicz, E. T. Smith, T. Ren, J. Chem. Soc., Chem. Commun. 1995, 2257-2258.
15. C. Lin, J. D. Protasiewicz, E. T. Smith, T. Ren, Inorg. Chem. 1996, 35, 6422-6428.
16. F. A. Cotton, T. Inglis, M. Kilner, T. R. Webb, Inorg. Chem. 1975, 14, 2023-2026.
17. F. A. Cotton, L. M. Daniels, C. A. Murillo, D. J. Timmons, Chem. Commun. 1997, 1449-1450.
18. F. A. Cotton, X. Feng, M. Matusz, Inorg. Chem. 1989, 28, 594-601.
19. F. A. Cotton, S. C. Haefner, A. P. Sattelberger, Inorg. Chem. 1996, 35, 7350-7357.
20. F. A. Cotton, W. H. Ilsley, W. Kaim, Inorg. Chem. 1980, 19, 2360-2364.
21. F. A. Cotton, T. Ren, J. Am. Chem. Soc. 1992, 114, 2495-2502.
22. F. A. Cotton, L. M. Daniels, J. H. Matonic, C. A. Murillo, Inorg. Chim. Acta 1997, 256, 277-282.
23. F. A. Cotton, L. M. Daniels, L. R. Falvello, J. H. Matonic, C. A. Murillo, Inorg. Chim. Acta 1997, 256, 269-275.
24. F. A. Cotton, L. M. Daniels, C. A. Murillo, Inorg. Chim. Acta 1994, 224, 5-9.
25. F. A. Cotton, X. Feng, C. A. Murillo, Inorg. Chim. Acta 1997, 256, 303-308.
26. C. Lin, T. Ren, E. J. Valente, J. D. Zubkowski, E. T. Smith, Chem. Lett. 1997, 753-754.
27. C. Lin, T. Ren, E. J. Valente, J. D. Zubkowski, J. Chem. Soc., Dalton Trans. 1998, 571-576.
28. C. Lin, T. Ren, E. J. Valente, J. D. Zubkowski, J. Organomet. Chem. 1999, 579, 114-121.
29. F. A. Cotton, T. Ren, Inorg. Chem. 1991, 30, 3675-3679.
30. J. Bear, B. Han, S. Huang, K. Kadish, Inorg. Chem. 1996, 35, 3012-3021.
31. F. A. Cotton, T. Ren, Inorg. Chem. 1995, 34, 3190-3193.
32. Y. Li, B. Han, K. Kadish, J. L. Bear, Inorg. Chem. 1993, 32, 4175-4176.
33. F. A. Cotton, T. Ren, J. L. Eglin, Inorg. Chem. 1991, 30, 2559-2563.
34. L. P. He, C. L. Yao, M. Naris, J. C. Lee, J. D. Korp, J. L. Bear, Inorg. Chem. 1992, 31, 620-625.
35. F. A. Cotton, L. M. Daniels, D. J. Maloney, J. H. Matonic, C. A. Murillo, Inorg. Chim. Acta 1997, 256, 283-289.
36. F. A. Cotton, L. M. Daniels, X. Feng, D. J. Maloney, J. H. Matonic, C. A. Murillo, Inorg. Chim. Acta 1997, 256, 291-301.
37. F. A. Cotton, L. M. Daniels, D. J. Maloney, C. A. Murillo, Inorg. Chim. Acta 1996, 249, 9-11.
38. J. C. Le, M. Y. Chavan, L. K. Chau, J. L. Bear, K. M. Kadish, J. Am. Chem. Soc. 1985, 107, 7195-7197.
39. S. L. Schiavo, G. Bruno, P. Zanello, F. Laschi, P. Piraino, Inorg. Chem. 1997, 36, 1004-1012.
40. P. Piraino, G. Bruno, S. L. Schiavo, F. Laschi, P. Zanello, Inorg. Chem. 1987, 26, 2205-2211.
41. J. L. Bear, C. L. Yao, R. S. Lifsey, J. D. Korp, K. M. Kadish, Inorg. Chem. 1991, 30, 336-340.
42. D. I. Arnold, F. A. Cotton, D. J. Maloney, J. H. Matonic, C. A. Murillo, Polyhedron 1997, 16, 133-141.
43. C. Lin, J. D. Protasiewicz, T. Ren, Inorg. Chem. 1996, 35, 7455-7458.
44. F. A. Cotton, M. Matusz, R. Poli, X. Feng, J. Am. Chem. Soc. 1988, 110, 1144-1154.
45. C. L. Yao, L. P. He, J. D. Korp, J. L. Bear, Inorg. Chem. 1988, 27, 4389-4395.
46. F. A. Cotton, J. H. Matonic, C. A. Murillo, Inorg. Chem. 1996, 35, 498-503.
47. F. A. Cotton, J. H. Matonic, C. A. Murillo, Inorg. Chim. Acta 1997, 264, 61-65.
48. F. A. Cotton, X. Feng, M. Matusz, R. Poli, J. Am. Chem. Soc. 1988, 110, 7077-7083.
49. T. Ren, C. Lin, P. Amalberti, D. Macikenas, J. D. Protasiewicz, J. C. Baum, T. L. Gibson, Inorg. Chem. Commun. 1998, 1, 23-26.
50. Y. Zhou, D. S. Richeson, Inorg. Chem. 1996, 35, 1423-1424.
51. Y. Zhou, D. S. Richeson, J. Am. Chem. Soc. 1996, 118, 10850-10852.
52. K. M. Carlson-Day, J. L. Eglin, C. Lin, L. T. Smith, R. J. Staples, D. O. Wipf, Polyhedron 1999, 18, 817-824.
53. T. Ren, Coord. Chem. Rev. 1998, 175, 43-58.
54. P. Zuman, The Elucidation of Organic Electrode Processes; Academic Press, New York 1969.
55. L. P. Hammett, Physical Organic Chemistry; McGraw-Hill, New York 1970.
56. J. Shorter, Correlation Analysis in Organic Chemistry; Clarendon Press, Oxford 1973.
57. J. E. Leffler, E. Grunwald, Rates and Equilibria of Organic Reactions; John Wiley and Sons, New York 1963.
58. F. A. Cotton, R. A. Walton, Multiple Bonds between Metal Atoms, 2nd edition; Oxford University Press, Oxford 1993.
59. K. M. Carlson-Day, Judith L. Eglin, L. T. Smith, R. J. Staples, Inorg. Chem. 1999, 38, 2216-2220.
60. L. Pauling, The Nature of the Chemical Bond; Cornell University Press, Ithaca, New York 1960.
61. K. M. Carlson-Day, J. L. Eglin, C. Lin, T. Ren, E. J. Valente, J. D. Zubkowski., Inorg. Chem. 1996, 35, 4727-4732.
62. V. Srinivasan, R. A. Walton, Inorg. Chem. 1980, 19, 1635-1640.
63. B. E. Bursten, F. A. Cotton, A. H. Cowley, B. E. Hanson, M. Lattman, G. G. Stanley, J. Am. Chem. Soc. 1979, 101, 6244-6249.
64. A. J. Bard, L. R. Faulkner, Electrochemical Methods.; John Wiley and Sons, New York 1980.
65. D. H. Evans, K. Hu, J. Chem. Soc., Faraday Trans. 1996, 92, 3983-3990.
66. J.-F. Capon, R. Kergoat, N. L. Berre-Cosquer, S. Peron, J.-Y. Saillard, J. Talarmin, Organometallics 1997, 16, 4645-4656.
67. K Hu, D. H. Evans, J. Phy. Chem. 1996, 100, 3030-3036.
68. G. J. Wagner, J. Q. Chambers, Langmuir 1997, 13, 3529-3541.
69. D. T. Pierce, W. E. Geiger, J. Am. Chem. Soc. 1992, 114, 6063-6073.
70. F. A. Cotton, C. A. James, Inorg. Chem. 1992, 31, 5298-5307.
71. T. J. Barder, R. A. Walton, Inorg. Chem. 1982, 21, 2510-2511.
72. F. A. Cotton, N. F. Curtis, B. F. G. Johnson, W. R. Robinson, Inorg. Chem. 1965, 4, 326-330.
73. W. Bradley, I. Wright, J. Chem. Soc. 1956, 640-648.
74. Ctystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication nos. CCDC-116605 (1),-116606 (2), -116609 (9), -116607 (10a), and -116605 (10b). Copies of the data may be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [Fax: (internat.) + 44-1223/336-033; E-mail: deposit@ccdc.cam.ac.uk].
75. SMART V 4.043 Software for the CCD Detector System, Siemens Analytical Instruments Division, Madison, WI, 1996.
76. SAINT V 4.035 Software for the CCD Detector System, Siemens Analytical Instruments Division, Madison, WI, 1995.
77. "SADABS, Program for Absorption corrections using Siemens CCD based on the method of Bob Blessing", Acta Crystallogr. 1995, A51, 33.
78. G. M. Sheldrick, SHELXL-90, Program for the Solution of Crystal Structures, University of Göttingen, Germany, 1986.
79. G. M. Sheldrick, SHELXL-93, Program for the Refinement of Crystal Structures, University of Göttingen, Germany, 1993.
80. SHELXTL 5.03 (PC Version), Program Library for Structure Solution and Molecular Graphics, Siemens Analytical Instruments Division, Madison, WI, 1995.