Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride

Journal of Organometallic Chemistry

Volumn 557, Issue 2, 1998, Pages 227-230

  Luttikhedde, Hendrik J G ^a   Leino, Reko ^a   Ahlgrén, Markku J ^b   Pakkanen, Tapani A ^b   Näsman, Jan H ^a  

^a ÅBO AKADEMI UNIVERSITY   (Finland)

^b UNIVERSITY OF EASTERN FINLAND   (Finland)

Author keywords

Aminoindenyl; Meso; Metallocene

Indexed keywords

EID: 0032580541     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(97)00694-3     Document Type: Article

References (32)

1. (a) P.C. Möhring, N.J.Coville, J. Organomet. Chem. 479 (1994) 1.
2. (b) K.B. Sinclair, R.B. Wilson, Chem. Ind. 20 (1994) 257.
3. (c) H.H. Brintzinger, D. Fischer, R. Mülhaupt, B. Rieger, R.M. Waymouth, Angew. Chem. Int. Ed. Engl. 34 (1995) 1143.
4. (d) M. Bochmann, J. Chem. Soc. Dalton Trans. (1996) 255.
5. (e) W. Kaminsky, M. Arndt, Adv. Polym. Sci. 127 (1997) 143.
6. (a) A.H. Hoveyda, J.P. Morken, Angew. Chem. Int. Engl. Ed. 35 (1996) 1262.
7. (b) G.M. Diamond, R.F. Jordan, J.F. Petersen, J. Am. Chem. Soc. 118 (1996) 8024 and references therein.
8. Nitrogen substituted, see: (a) K.-P. Stahl, G. Boche, W. Massa, J. Organomet. Chem. 227 (1984) 113.
9. (b) E. Barsties, Ph.D. Thesis, Universität Konstanz, 1995.
10. (c) E. Barsties, S. Schaible, M.-H. Prosenc, U. Rief, W. Röll, O. Weyand, B. Dorer, H.H. Brintzinger, J. Organomet. Chem. 520 (1996) 63.
11. (d) H.J.G. Luttikhedde, R.P. Leino, C.-E. Wilén, J.H. Näsman, M.J. Ahlgrén, T.A. Pakkanen, Organometallics 15 (1996) 3092.
12. (e) H. Plenio, D. Burth, J. Organomet. Chem. 519 (1996) 269.
13. Oxygen substituted, see: (a) R. Leino, H.J.G. Luttikhedde, C.-E. Wilén, R. Sillanpää; J.H. Näsman, Organometallics 15 (1996) 2450.
14. (b) R. Leino, H.J.G. Luttikhedde, P. Lehmus, C.-E. Wilén, R. Sjöholm, A. Lehtonen, J.V. Seppälä, J.H. Näsman, Macromolecules 30 (1997) 3477.
15. (c) R. Leino, H.J.G. Luttikhedde, A. Lehtonen, P. Ekholm, J.H. Näsman, submitted for publication in Organometallics.
16. (d) H. Plenio, A. Warnecke, J. Organomet. Chem. 544 (1997) 133.
17. (e) R. Leino, H.J.G. Luttikhedde, P. Lehmus, C.-E. Wilén, R. Sjöholm, A. Lehtonen, J.V. Seppälä, J.H. Näsman, J. Organomet. Chem., in press.
18. (f) H.J.G. Luttikhedde, R. Leino, A. Lehtonen, J.H. Näsman, J. Organomet. Chem, in press.
19. (g) R. Leino, H.J.G. Luttikhedde, A. Lehtonen, R. Sillanpää, A. Penninkangas, J. Strandén, J. Mattinen, J.H. Näsman, J. Organomet. Chem., in press.
20. Boron substituted, see: (a) M.T. Reetz, H. Brümmer, M. Kessler, J. Kuhnigk, Chimia 49 (1995) 501.
21. (b) K.A. Rufanov, V.V. Kotov, N.B. Kazennova, D.A. Lemenovskii, E.V. Avtomov, J. Lorberth, J. Organomet. Chem. 525 (1996) 287.
22. (c) S.A. Larkin, J.T. Golden, P.J. Shapiro, G.P.A. Yap, D. Ming Jin Foo, A.L. Rheingold, Organometallics 15 (1996) 2393.
23. (d) K. Rufanov, E. Avtomov, N. Kazennova, V. Kotov, A. Khvorost, D. Lemenovskii, J. Lorberth, J. Organomet. Chem. 536-537 (1997) 361.
24. Sulfur substituted, see: R. Broussier, C. Bourdon, O. Blacque, A. Vallat, M.M. Kubicki, B. Gautheron, J. Organomet. Chem. 538 (1997) 83.
25. Arsenic substituted, see: ref. 5(d).
26. A'B=4.8 Hz.
27. (a) F. Piemontesi, I. Camurati, L. Resconi, D. Balboni, M. Moret, R. Zeigler, N. Piccolrazzavi, Organometallics 14 (1995) 1256.
28. (b) L. Resconi, F. Piemontesi, I. Camurati, D. Balboni, A. Sironi, M. Moret, H. Rychlicki, R. Zeigler, Organometallics 15 (1996) 5046.
29. Collins S., Gauthier W.J., Holden D.A., Kuntz B.A., Taylor N.J., Ward D.G. Organometallics. 10:1991;2061.
30. (a) Selected torsion angles (°) for 3: C(211)-N(12)-C(12)-C(13)=8.3(15), C(212)-N(12)-C(12)-C(11)=67.3(13), C(221)-N(22)-C(22)-C(23)=-0.3(18), C(222)-N(22)-C(22)-C(21)=-42.5(17).
31. Sheldrick G.M. Acta Crystallogr. A46:1990;467.
32. G.M. Sheldrick, SHELXL93. Program for the Refinement of Crystal Structures. University of Göttingen, Germany, 1993.