Propylthiotetramethylcyclopentadienyl complexes of iron, titanium and zirconium. Structural characterization of [η5-C5Me4SCH2CH2CH3]2TiCl2

Journal of Organometallic Chemistry

Volumn 538, Issue 1-2, 1997, Pages 83-90

  Broussier, Roland ^a   Bourdon, Cyrille ^a   Blacque, Olivier ^a   Vallat, Alain ^a   Kubicki, Marek M ^a   Gautheron, Bernard ^a  

^a UNIVERSITÉ DE BOURGOGNE   (France)

Author keywords

Cyclopentadienyl; Ferrocene; Sulphur; Titanium; Zirconium

Indexed keywords

EID: 0031580145     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(96)06909-4     Document Type: Article

References (38)

1. [1] P. Kalck, C. Serra, C. Machet, R. Broussier, B. Gautheron, G. Delmas, G. Trouvé and M.M. Kubicki, Organometallics, 12 (1993) 1021.
2. [2] S. Ninoreille, R. Broussier, R. Amardeil, M.M. Kubicki and B. Gautheron, Bull. Soc. Chim. Fr., 132 (1995) 128.
3. [3] M. Herberhold, in A. Togni and T. Hahashi (eds.), Ferrocenes, VCH, Weinheim, 1995, Chap. 5, p. 219.
4. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
5. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
6. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
7. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
8. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
9. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
10. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
11. [4] K. Sünkel and D. Motz, Chem. Ber., 121 (1988) 799; Angew. Chem., 27(7) (1988) 939; K. Sünkel and D. Steiner, Chem. Ber., 122 (1989) 609; M. Herberhold and M. Biersack, J. Organomet. Chem., 381 (1990) 379; K. Sünkel and A. Blum, Chem. Ber., 125 (1992) 1605; M. Herberhold and M. Biersack, J. Organomet. Chem., 445 (1993) 1; K. Sünkel, A. Blum and B. Wagner, Z. Naturforsch., 48b (1993) 583; K. Sünkel, U. Birk, A. Blum and W. Kempinger, J. Organomet. Chem., 465 (1994) 167.
12. [5] F. Wudl, D. Nalewajek, F.L. Rotella and E. Gebert, J. Am. Chem. Soc., 103 (1981) 5885.
13. [6] R. Broussier, C. Bourdon, O. Blacque, A. Vallat, M.M. Kubicki and B. Gautheron, Bull. Soc. Chim. Fr., in press.
14. [7] K.H. Den Haan, J.L. De Boer, J.H. Teuben, A.L. Spek, B.K. Prodic, G.R. Hays and R. Huis, Organometallics, 5 (1985) 1726.
15. [8] R. Broussier et al., unpublished results, 1996.
16. [9] Y. Mugnier, C. Moïse and E. Laviron, J. Organomet. Chem., 204 (1981) 61; A. Fakhr, Y. Mugnier, B. Gautheron and E. Laviron, J. Organomet. Chem., 302 (1986) C7.
17. [9] Y. Mugnier, C. Moïse and E. Laviron, J. Organomet. Chem., 204 (1981) 61; A. Fakhr, Y. Mugnier, B. Gautheron and E. Laviron, J. Organomet. Chem., 302 (1986) C7.
18. [10] A. Fakhr, Y. Mugnier, B. Gautheron and E. Laviron, New J. Chem., 70 (1986) 601.
19. [11] R.F. Johnston, R.E. Borjas and J.L. Furilla, Electrochim. Acta, 40 (1995) 473.
20. [12] E. Laviron and L. Roullier, J. Electroanal. Chem., 186 (1985) 1.
21. [13] R.S. Nicholson and I. Shain, Anal. Chem., 36(4) (1964) 706.
22. [14] T.C. McKenzie, R.D. Sanner and J.E. Bercaw, J. Organomet. Chem., 102 (1975) 457.
23. [15] J. Szymoniak, M.M Kubicki, J. Besançon and C. Moïse, Inorg. Chim. Acta, 180 (1991) 153.
24. [16] A. Clearfield, D.K. Warner, C.H. Saldarriaga-Molina, R. Ropal and I. Bernal, Can. J. Chem., 53 (1975) 1622.
25. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
26. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
27. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
28. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
29. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
30. [17] K.P. Stahl, G. Boche and W. Massa, J. Organomet. Chem., 277 (1984) 113; R.A. Howie, G.P. McQuillan and D.W. Thompson, Acta Crystallogr., C41 (1985) 1045; J. Organomet. Chem., 268 (1984) 149; I.F. Urazowski, V.I. Ponomaryov, O.G. Ellert, I.E. Nifant'ev and D.E. Lemenovskii, J. Organomet. Chem., 356 (1988) 181; D.T. Mallin, M.D. Rausch, E.A. Mintz and A.L. Rheingold, J. Organomet. Chem., 381 (1990) 35; R.D. Rogers, M.M. Benning, L.K. Kurihara, K.J. Moriarty and M.D. Rausch, J. Organomet. Chem., 293 (1985) 51.
31. [18] J.W. Lauher and R. Hoffmann, J. Am. Chem. Soc., 98 (1976) 1729; M.Y. Davensbourg, C.J. Bischoff, S.A. Houliston, M. Pala and J. Reibenspies, J. Am. Chem. Soc., 112 (1990) 6905; P.C. Möhring, N. Vlachakis, N.E. Grimmer and N.J. Coville, J. Organomet. Chem., 483 (1994) 159.
32. [18] J.W. Lauher and R. Hoffmann, J. Am. Chem. Soc., 98 (1976) 1729; M.Y. Davensbourg, C.J. Bischoff, S.A. Houliston, M. Pala and J. Reibenspies, J. Am. Chem. Soc., 112 (1990) 6905; P.C. Möhring, N. Vlachakis, N.E. Grimmer and N.J. Coville, J. Organomet. Chem., 483 (1994) 159.
33. [18] J.W. Lauher and R. Hoffmann, J. Am. Chem. Soc., 98 (1976) 1729; M.Y. Davensbourg, C.J. Bischoff, S.A. Houliston, M. Pala and J. Reibenspies, J. Am. Chem. Soc., 112 (1990) 6905; P.C. Möhring, N. Vlachakis, N.E. Grimmer and N.J. Coville, J. Organomet. Chem., 483 (1994) 159.
34. [19] L.E. Manzer, Inorg. Synth., 21 (1982) 135.
35. [20] E.L. Lund and T. Livinghouse, Organometallics, 9 (1990) 2426.
36. [21] M. Aresta, C.F. Nobile and D. Petruzzelli, Inorg. Chem., 16 (1977) 1817.
37. [22] C.K. Fair, Molen, Structure Determination System, Enraf-Nonius, Delft, Netherlands, 1990.
38. [23] International Tables for X-Ray Crystallography, Kynoch Press, Birmingham, UK, 1974.