Graphene-oxide stacking and defects in few-layer films: Impact of thermal and chemical reduction

Carbon

Volumn 80, Issue 1, 2014, Pages 40-49

  Díez Betriu, Xavier ^a   Mompeán, Federico J ^a   Munuera, Carmen ^a   Rubio Zuazo, Juan ^a,b   Menéndez, Rosa ^c   Castro, Germán R ^a,b   De Andrés, Alicia ^a  

^a INSTITUTO DE CIENCIA DE MATERIALES DE MADRID   (Spain)

^b EUROPEAN SYNCHROTRON RADIATION FACILITY   (France)

^c INSTITUTO NACIONAL DEL CARBÓN   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMIC FORCE MICROSCOPY; COMPOSITE FILMS; DEFECTS; FUNCTIONAL GROUPS; GRAPHENE; MOLECULES; MORPHOLOGY; RADIATION EFFECTS; SYNCHROTRON RADIATION;

CHEMICAL REDUCTION; ELECTRICAL CONDUCTIVITY; IN-SITU SYNCHROTRONS; INTERLAYER DISTANCE; STRUCTURAL DEFECT; SUBSTRATE MORPHOLOGIES; THERMAL REDUCTION; THERMAL-ANNEALING;

OXIDE FILMS;

EID: 85027955783     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2014.08.016     Document Type: Article

References (33)

1. Bonaccorso F, Sun Z, Hasan T, Ferrari AC. Graphene photonics and optoelectronics. Nat. Photon. 2010;4(611-62): 2.
2. Ping Loh K, Bao Q, Eda G, Chhowalla M. Graphene oxide as a chemically tunable platform for optical applications. Nat Chem 2010; 2: 1015-24.
3. Pang S, Hernández Y, Feng X, Müllen K. Graphene as transparent electrode material for organic electronics. Adv Mater 2011;23: 2779-95.
4. Novoselov KS, Falko VI, Colombo L, Gellert PR, Schwab MG, Kim K. A roadmap for graphene. Nature 2012;490(192-20).
5. Lui CH, Li Z, Chen Z, Klimov PV, Brus LE, Heinz TF. Imaging stacking order in few-layer graphene. Nano Lett 2010;11(164- 16): 9.
6. Brodie BC. On the atomic weight of graphite. Philos Trans R Soc Lond 1859;149: 249-59.
7. Zhao J, Pei S, Ren W, Gao L, Cheng H. Efficient preparation of large-area graphene oxide sheets for transparent conductive films. ACS Nano 2010;9: 5245-52.
8. Jeong HK, Jin MH, So KP, Lim SC, Lee YH. Tailoring the characteristics of graphite oxides by different oxidation times. J Phys D Appl Phys 2009;42: 065418.
9. SzabóT, Barkesi O, ForgóP, Josepovits K, Sannakis Y, Petridis D, et al. Evolution of surface functional groups in a series of progressively oxidized graphite oxides. Chem Mater 2006;18: 2740-9.
10. Jeong H, Lee Y, Lahaye R, Park M, An KH, Kim I, et al. Evidence of graphitic AB stacking order of graphite oxides. J Am Chem Soc 2008;130: 1362-6.
11. Lerf A, Buchsteiner A, Pieper J, Schottl S, Dekany I, Szabo T, et al. Hydration behavior and dynamics of water molecules in graphite oxide. J Phys Chem Solids 2006;67: 1106-10.
12. Jeong H-K, Lee YP, Jin MH, Kim ES, Bae JJ, Lee YH. Thermal stability of graphite oxide. Chem Phys Lett 2009;470: 255-8.
13. Schniepp HC, Li JL, McAllister MJ, Sai H, Herrera-Alonso M, Adamson DH, et al. Functionalized single graphene sheets derived from splitting graphite oxide J Phys Chem B 2006; 110: 8535-9.
14. Ganguly A, Sharma S, Papakonstantinou P, Hamilton J. Probing the thermal deoxygenation of graphene oxide using high-resolution in situ X-ray-based spectroscopies. J Phys Chem C 2011;115: 17009-19.
15. Wick P, Louw-Gaume AE, Kucki M, Krug HF, Kostarelos K, Fadeel B, et al. Classification framework for graphene-based materials. Angew Chem (International ed. in English) 2014; 2-7.
16. Wang L, Sun Y, Lee K, West D, Chen Z, Zhao J, et al. Stability of graphene oxide phases from first-principles calculations. Phys Rev B 2010;82: 2-5.
17. Dikin D, Stankovich S, Zimney E, Piner R, Dommet G, Evmenko G, et al. Preparation and characterization of graphene oxide paper. Nature 2007; 448: 457-60.
18. Talyzin AV, Hausmaninger T, You S, SzabóT. The structure of graphene oxide membranes in liquid water, ethanol and water-ethanol mixtures. Nanoscale 2014; 6; 272-81.
19. McAllister MJ, Li JL, Adamson DH, Schniepp HC, Abdala AA, Jun Liu X, et al. Single sheet functionalized graphene by oxidation and thermal expansion of graphite. Chem Mater 2007;19: 4396-404.
20. Liscio A, Veronese GP, Treossi E, Suriano F, Rossella F, Bellani V, et al. Charge transport in graphene-polythiophene blends as studied by Kelvin Probe Force Microscopy and transistor characterization. J Mater Chem 2011;21: 2924.
21. Xia ZY, Pezzini S, Treossi E, Giambastiani G, Corticelli F, Morandi V, et al. The exfoliation of graphene in liquids by electrochemical chemical, and sonication-assisted techniques: A nanoscale study. Adv Funct Mater 2013. http://dx.doi.org/10.1002/adfm.201203686.
22. Díez-Betriu X, Álvarez S, Botas C, Álvarez P, Sánchez-Marcos J, Prieto C, et al. Raman spectroscopy for the study of reduction mechanisms and optimization of conductivity in graphene oxide thin films. J Mater Chem C 2013;1: 6905.
23. Botas C, Álvarez P, Blanco C, Gutierrez MD, Ares P, Zamani R, et al. Tailored graphene materials by chemical reduction of graphene oxides of different atomic structure. RSC Adv 2012;2(9643-965).
24. Yamaguchi H, Eda G, Mattevi C, Kim H, Chhowalla M. Highly uniform 300mm wafer-scale deposition of single and multilayered chemically derived graphene thin films. ACS Nano 2010;4: 524-8.
25. Gómez-Navarro C, Thomas Wietz R, Bittner A, Scolari M, Mews A, Burghard M, et al. Electronic transport properties of individual chemically reduced graphene oxide sheets. Nano Lett 2007; 7: 3499-503.
26. Horcas I, Fernandez R, Gómez-Rodríguez JM, Colchero J, Gómez-Herrero J, Baro AM. WSXM: A software for scanning probe microscopy and a tool for nanotechnology. Rev Sci Instrum 2007;78: 013705.
27. Rubio-Zuazo J, Ferrer P, López A, Gutiérrez-León A, da Silva I, Castro GR. The multipurpose X-ray diffraction end-station of the BM25B-SpLine synchrotron beamline at the ESRF. Nucl Instrum Methods Phys Res A 2013; 716: 23-8.
28. Novoselov KS, Geim AK, Morozov SV, Jiang D, Zhang Y, Dubonos S, et al. Electric field effect in atomically thin carbon films. Science (New York, NY) 2004; 306: 666-9.
29. Mkhoyan K, Contryman AW, Silcox J, Stewart DA, Eda G, Mattevi C, et al. Evolution of electrical, chemical, and structural properties of transparent and conducting chemically derived graphene thin films. Nano Lett 2009; 9: 1058-63.
30. Nair RR, Wu HA, Jayaram PN, Grigorieva IV, Geim AK. Unimpeded permeation of water through helium-leak-tight graphene-based membranes. Science (New York, N.Y.) 2012;335: 442-4.
31. Bagri A, Mattevi C, Acik M, Chabal YJ, Chhowalla M, Shenoy VB. Structural evolution during the reduction of chemically derived graphene oxide. Nat Chem 2010;2(581-58): 7.
32. We do not consider temperature dependent Debye-Waller factors since the predominant effect is the random static disorder.
33. Jung I, Pelton M, Piner R, Dikin DA, Stankovich S, Watcharotone S, et al. Simple approach for high-contrast optical imaging and characterization of graphene-based sheets. Nano Lett 2007;7(3569-357): 5.