Deuterium NMR of liquid-crystalline samples at natural abundance

eMagRes

Volumn 2, Issue 3, 2013, Pages 315-334

  Lesot, Philippe ^a  

^a UNIVERSITÉ PARIS SACLAY   (France)

Author keywords

anisotropic media; chirality; deuterium NMR; isotope fractionation; natural abundance; stereochemistry

Indexed keywords

ANISOTROPIC MEDIA; LIQUID CRYSTALS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ANISOTROPIC MEDIUM; CRYOGENIC PROBES; CRYSTALLINE SAMPLES; DEUTERIUM NMR; ISOTOPE FRACTIONATION; LIQUID CRYSTALLINE; MAGNETIC-FIELD; NATURAL ABUNDANCE; NMR SOLVENTS; PULSE SEQUENCE;

DEUTERIUM;

EID: 85019814975     PISSN: None     EISSN: 20556101     Source Type: Book Series    
DOI: 10.1002/9780470034590.emrstm1318     Document Type: Article

References (75)

1. R. Hagemann, G. Nief, and E. Roth, Tellus, 1970, 22, 712.
2. C. Brevard and P. Granger, 'Handbook of High Resolution Multinuclear NMR', J. Wiley & Sons, New York, 1981, p. 84.
3. J. R. De Laeter, J. K. Böhlke, P. De Bievre, H. Hidaka, H. S. Peiser, K. J. R. Rosman, and P. D. P. Taylor, Pure Appl. Chem., 2003, 75, 683.
4. P. Lesot and J. Courtieu, Prog. Nucl. Magn. Reson. Spectrosc., 2009, 55, 128.
5. P. Lesot, M. Sarfati, and J. Courtieu, Chem. Eur. J., 2003, 9, 1724.
6. J. M. Briggs, L. F. Farnell, and E. W. Randall, Chem. Commun., 1973, 70.
7. J. Curtis, D. K. Dalling, and D. M. Grant, J. Org. Chem., 1986, 51, 136.
8. M. L. Martin and G. J. Martin, in 'NMR Basic Principles and Progress', ed. P. Diehl, Springer-Verlag, 1990, Vol. 23, p. 1-61.
9. P. Lesot, Z. Serhan, and I. Billault, Anal. Bioanal. Chem., 2011, 399, 1187.
10. J. W. Emsley and J. C. Lindon, in 'NMR Spectroscopy using Liquid Crystals', eds J. W. Emsley and J. C. Lindon, Pergamon Press, Oxford, 1975, Chapter 2.
11. H. Kovacs, D. Moskau, and M. Spraul, Prog. Nucl. Magn. Reson. Spectrosc., 2005, 46, 131.
12. P. Lesot and O. Lafon, Anal. Chem., 2012, 84, 4569.
13. R. R. Ernst, G. Bodenhausen, and A. Wokaun, 'Principles of Nuclear Magnetic Resonance in One and Two Dimensions', Clarendon Press, Oxford, 1987.
14. C. Zannoni, in 'Nuclear Magnetic Resonance of Liquid Crystals', ed. J. W. Emsley, NATO ASI Series, 1985, Chapter 1.
15. H. Jensen and K. Schaumburg, Acta Chem. Scand., 1971, 25, 663.
16. D. Neuhaus and M. P. Williamson, 'The Nuclear Overhauser Effect in Structural and Conformational Analysis', 2nd edn, Wiley-VCH, 2000.
17. T. C. Lubensky, Phys. Rev. A, 1970, 2, 2497.
18. R. R. Vold, in 'Nuclear Magnetic Resonance of Liquid Crystals', ed. J. W. Emsley, NATO ASI Series, Dordrecht, 1985, Chapter 11.
19. R. Y. Dong, Ann. Rep. on NMR Spect., 2004, 53, 67.
20. M. Sarfati, P. Lesot, D. Merlet, and J. Courtieu, Chem. Commun., 2001, 2069.
21. T. J. Wenzel, 'Discrimination of Chiral Compounds using NMR Spectroscopy', J. Wiley & Sons, 2007.
22. E. Sackmann, S. Meiboom, and L. C. Snyder, J. Am. Chem. Soc., 1968, 90, 2183.
23. P. Lesot, V. Reddy, and N. Suryaprakash, Chem. Commun., 2011, 47, 11736.
24. C. Naumann and P. W. Kuchel, Chem. Eur. J., 2009, 15, 12189.
25. C. Aroulanda, M. Sarfati, J. Courtieu, and P. Lesot, Enantiomer, 2001, 6, 281.
26. P. Lesot, D. Merlet, Y. Gounelle, and J. Courtieu, J. Phys. Chem. A., 1995, 99, 14871.
27. P. Diehl and T. Leipert, Helv. Chim. Acta, 1964, 47, 545.
28. P. Lesot, Spectra Analyse, 2008, 260, 16.
29. B. M. Fung, Prog. Nucl. Magn. Reson. Spectrosc., 2002, 41, 171.
30. P. Diehl, in 'Nuclear Magnetic Resonance of Liquid Crystals', ed. J. W. Emsley, NATO ASI Series, Drodrecht, 1985, Chapter 7.
31. L. D. Field, 'NMR of Ordered Liquids', eds E. E. Burnell and C. A. de Lange, Kluwer Academic Publisher, Dordrecht, 2003, Chapter 4.
32. J. Courtieu, J.-P. Bayle, and B. M. Fung, Prog. Nucl. Magn. Reson. Spectrosc., 1994, 26, 141.
33. E. E. Burnell and C. A. de Lange, in 'NMR of Ordered Liquids', eds E. E. Burnell and C. A. de Lange, Kluwer Academic Publishers, Dordrecht, 2003, Chapter 10.
34. J. W. Emsley, J. C. Lindon, J. M. Tabony, and T. H. Wilmshurst, Chem. Commun., 1971, 1277.
35. J. Atzrodt, V. Derdau, T. Fey, and J. Zimmermann, Angew. Chem. Int. Ed., 2007, 45, 7744.
36. R. Y. Dong, 'Nuclear Magnetic Resonance of Liquid Crystals', Spring-Verlag, New York, 1994.
37. R. S. Prosser, N. J. Heaton, and G. Kothe, J. Magn. Reson. B, 1996, 112, 51.
38. K. Tabayashi and K. Akasaka, J. Phys. Chem. B, 1997, 101, 5108.
39. I. P. Gerothanassis, Prog. Nucl. Magn. Reson.Spectrosc., 1987, 19, 267.
40. K. Tabayashi and K. Akasaka, Liquid Crystals, 1999, 26, 127.
41. J. W. Emsley, P. Lesot, G. de Luca, A. Lesage, D. Merlet, and G. Pileo, Liquid Crystals, 2008, 35, 443.
42. C. L. Khetrapal, K. V. Ramanathan, N. Suryaprakash, and S. Vivekanandan, J. Magn. Reson., 1998, 135, 265.
43. P. Lesot, D. Merlet, A. Loewenstein, and J. Courtieu, Tetrahedron: Asymmetry, 1998, 9, 1871.
44. D. Merlet, B. Ancian, J. Courtieu, and P. Lesot, J. Am. Chem. Soc., 1999, 121, 5249.
45. D. Merlet, M. Sarfati, B. Ancian, J. Courtieu, and P. Lesot, Phys. Chem. Chem. Phys., 2000, 2, 2283.
46. O. Lafon, P. Lesot, D. Merlet, and J. Courtieu, J. Magn. Reson., 2004, 171, 135.
47. O. Lafon and P. Lesot, Chem. Phys. Lett., 2005, 404, 90.
48. P. Lesot and O. Lafon, Chem. Phys. Lett., 2008, 458, 219.
49. O. Lafon, B. Hu, J.-P. Amoureux, and P. Lesot, Chem. Eur. J., 2011, 17, 6716.
50. C. Canlet, D. Merlet, P. Lesot, A. Meddour, A. Loewenstein, and J. Courtieu, Tetrahedron: Asymmetry, 2000, 11, 1911.
51. A. Parenty, J.-M. Campagne, C. Aroulanda, and P. Lesot, Org. Lett., 2002, 2, 1663.
52. A. Meddour, I. Canet, A. Loewenstein, J.-M. Péchiné, and J. Courtieu, J. Am. Chem. Soc., 1994, 116, 9652.
53. K. Czarniecka and E. T. Samulski, Mol. Cryst. Liq. Cryst., 1981, 63, 205.
54. P. Lesot, D. Merlet, M. Sarfati, J. Courtieu, H. Zimmermann, and Z. Luz, J. Am. Chem. Soc., 2002, 124, 10071.
55. E. E. Eliel and S. H. Wilen, 'Stereochemistry of Organic Compounds', J. Wiley & Sons, Inc., New York, 1994.
56. P. Lesot, O. Lafon, H. Zimmermann, and Z. Luz, J. Am. Chem. Soc., 2008, 130, 9754.
57. D. Merlet, J. W. Emsley, P. Lesot, and J. Courtieu, J. Chem. Phys., 1991, 111, 6890.
58. P. Lesot, C. Aroulanda, and I. Billault, Anal. Chem., 2004, 76, 2827.
59. A. Bilz, T. Stork, and G. Helmchen, Tetrahedron: Asymmetry, 1997, 8, 3999.
60. J. Huskens, R. Goddard, and M. T. Reetz, J. Am. Chem. Soc., 1998, 120, 6617.
61. C. Aroulanda, H. Zimmermann, Z. Luz, and P. Lesot, J. Chem. Phys., 2011, 134, 134502-1/8.
62. C. A. Fan, B. Ferber, H. B. Kagan, O. Lafon, and P. Lesot, Tetrahedron; Asymmetry, 2008, 19, 2666.
63. C. Aroulanda, P. Lesot, D. Merlet, and J. Courtieu, J. Phys. Chem. A, 2003, 107, 10911.
64. R. Berger, J. Courtieu, R. R. Gil, C. Griesinger, M. Köck, P. Lesot, B. Luy, D. Merlet, A. Navarro-Vazquez, M. Reggelin, U. M. Reinscheid, M. Thiele, and M. Zweckstetter, Angew. Chemie, Int. Ed., 2012, 51, 2.
65. L. Ziani, P. Lesot, A. Meddour, and J. Courtieu, Chem. Commun., 2007, 4737.
66. D. A. Singleton and A. A. Thomas, J. Am. Chem. Soc., 1995, 117, 9357.
67. J.-R. Duan, I. Billault, F. Mabon, and R. J. Robins, ChemBioChem, 2002, 3, 52.
68. P. Lesot, C. Aroulanda, and I. Billault, Anal. Chem., 2004, 76, 2827.
69. V. Baillif, I. Billault, R. J. Robins, and P. Lesot, J. Am. Chem. Soc., 2006, 128, 11180.
70. P. Lesot, V. Baillif, and I. Billault, Anal. Chem., 2008, 80, 2963.
71. P. Lesot, Z. Serhan, and I. Billault, Chem. Commun., 2011, 46, 6599.
72. V. Baillif, R. Robins, S. Le Feunten, P. Lesot, and I. Billault, J. Biol. Chem., 2009, 284, 10783.
73. I. Billault, A. Ledru, M. Ouetrani, Z. Serhan, P. Lesot, and R. J. Robins, Anal. Bioanal. Chem., 2012, 402, 2985.
74. Z. Serhan, I. Billault, A. Borgogno, A. Ferrarini, and P. Lesot, Chem. Eur. J., 2012, 18, 117.
75. P. Lesot, Z. Serhan, C. Aroulanda, and I. Billault, Magn. Reson. Chem., 2012, 50, S2.