Development of a method for direct elemental analysis of lithium ion battery degradation products by means of total reflection X-ray fluorescence

Spectrochimica Acta - Part B Atomic Spectroscopy

Volumn 112, Issue , 2015, Pages 34-39

  Evertz, Marco ^a   Lürenbaum, Constantin ^a   Vortmann, Britta ^a   Winter, Martin ^a   Nowak, Sascha ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

Lithium ion battery; NCM degradation; Non digestive; Sample pretreatment; TXRF

Indexed keywords

CATHODES; DEGRADATION; ELECTRIC BATTERIES; ELECTRIC DISCHARGES; ELECTRODES; ELECTROMAGNETIC WAVE REFLECTION; FLUORESCENCE; GRAPHITE; GRAPHITE ELECTRODES; INDUCTIVELY COUPLED PLASMA; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; IONS; LITHIUM; LITHIUM ALLOYS; MASS SPECTROMETRY; METAL ANALYSIS; OPTICAL EMISSION SPECTROSCOPY; PHOTODEGRADATION; SECONDARY BATTERIES; SPECTROMETRY; TRANSITION METALS;

INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRIES (ICPMS); INDUCTIVELY COUPLED PLASMA-OPTICAL EMISSION SPECTROMETRY; MICROWAVE-ASSISTED ACID DIGESTION; NON-DIGESTIVE; QUANTITATIVE AND QUALITATIVE ANALYSIS; SAMPLE PRETREATMENT; TOTAL REFLECTION X-RAY FLUORESCENCE; TXRF;

LITHIUM-ION BATTERIES;

EID: 84941100896     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.sab.2015.08.005     Document Type: Article

References (37)

1. R. Wagner, N. Preschitschek, S. Passerini, J. Leker, and M. Winter Current research trends and prospects among the various materials and designs used in lithium-based batteries J. Appl. Electrochem. 43 2013 481 496
2. M. Broussely, P. Biensan, F. Bonhomme, Ph. Blanchard, S. Herreyre, K. Nechev, and R.J. Staniewicz Main aging mechanisms in Li ion batteries J. Power Sources 146 2005 90 96
3. H. Buqa, R.I.R. Blyth, P. Golob, B. Evers, I. Schneider, M.V. Santis Alvarez, F. Hofer, F.P. Netzer, M.G. Ramsey, M. Winter, and J.O. Besenhard Negative electrodes in rechargeable lithium ion batteries - influence of graphite surface modification on the formation of the solid electrolyte interphase Ionics 6 2000 172 179
4. W. Kohs, H.J. Santner, F. Hofer, H. Schröttner, J. Doninger, I. Barsukov, H. Buqa, J.H. Albering, K.-C. Möller, J.O. Besenhard, and M. Winter A study on electrolyte interactions with graphite anodes exhibiting structures with various amounts of rhombohedral phase J. Power Sources 119-121 2003 528 537
5. M. Winter, and R. Brodd What are batteries, fuel cells, and supercapacitors? Chem. Rev. 104 2004 4245 4269
6. M. Winter, and J.O. Besenhard Wiederaufladbare batterien Chem. Unserer Zeit 33 1999 320 332
7. B. Scrosati, and J. Garche Lithium batteries: status, prospects and future J. Power Sources 195 2010 2419 2430
8. M. Winter, J.O. Besenhard, M.E. Spahr, and P. Novak Insertion electrode materials for rechargeable lithium batteries Adv. Mater. 10 1998 725 763
9. P. He, H. Yu, D. Li, and H. Zhou Layered lithium transition metal oxide cathodes towards high energy lithium-ion batteries J. Mater. Chem. 22 2012 3680 3696
10. M. Grützke, V. Kraft, B. Hoffmann, S. Klamor, J. Diekmann, A. Kwade, M. Winter, and S. Nowak Aging investigations of a lithium-ion battery electrolyte from a field-tested hybrid electric vehicle J. Power Sources 273 2015 83 88
11. C. Dippel, S. Krueger, R. Kloepsch, P. Niehoff, B. Hoffmann, S. Nowak, S. Passerini, M. Winter, and J. Li Aging of Li2FeSiO4 cathode material in fluorine containing organic electrolytes for lithium-ion batteries Electrochim. Acta 85 2012 66 71
12. C. Dippel, S. Krueger, V. Kraft, S. Nowak, M. Winter, and J. Li Aging stability of Li2FeSiO4 polymorphs in LiPF6 containing organic electrolyte for lithium-ion batteries Electrochim. Acta 105 2013 542 546
13. L. Terborg, S. Weber, F. Blaske, S. Passerini, M. Winter, U. Karst, and S. Nowak Investigation of thermal aging and hydrolysis mechanisms in commercial lithium ion battery electrolyte J. Power Sources 242 2013 832 837
14. M. Pyschik, V. Kraft, S. Passerini, M. Winter, and S. Nowak Thermal aging of anions in ionic liquids containing lithium salts by IC/ESI-MS Electrochim. Acta 130 2014 426 430
15. J. Vetter, P. Novák, M.R. Wagner, C. Veit, K.-C. Möller, J.O. Besenhard, M. Winter, M. Wohlfahrt-Mehrens, C. Vogler, and A. Hammouche Ageing mechanisms in lithium-ion batteries J. Power Sources 147 2005 269 281
16. H. Zheng, Q. Sun, G. Liu, X. Song, and V.S. Battaglia Correlation between dissolution behavior and electrochemical cycling performance for LiNi1/3Co1/3Mn1/3O2-based cells J. Power Sources 207 2012 134 140
17. H. Schranzhofer, J. Bugajski, H.J. Santner, C. Korepp, K.-C. Möller, J.O. Besenhard, M. Winter, and W. Sitte Electrochemical impedance spectroscopy study of the SEI formation on graphite and metal electrodes J. Power Sources 153 2006 391 395
18. J.P. Olivier, and M. Winter Determination of the absolute and relative extents of basal plane surface area and "non-basal plane surface" area of graphites and their impact on anode performance in lithium ion batteries J. Power Sources 97-98 2001 151 155
19. V.A. Agubra, and J.W. Fergus The formation and stability of the solid electrolyte interface on the graphite anode J. Power Sources 268 2014 153 162
20. S. Krüger, C. Hanisch, A. Kwade, M. Winter, and S. Nowak Effect of impurities caused by a recycling process on the electrochemical performance of Li[Ni0.33Co0.33Mn0.33]O2 J. Electroanal. Chem. 726 2014 91 96
21. P. Niehoff, and M. Winter Composition and growth behavior of the surface and electrolyte decomposition Layer of/on a commercial lithium ion battery LixNi1/3Mn1/3Co1/3O2 cathode determined by sputter depth profile X-ray photoelectron spectroscopy Langmuir 29 2013 15813 15821
22. D.R. Gallus, R. Schmitz, R. Wagner, B. Hoffmann, S. Nowak, I. Cekic-Laskovic, R.W. Schmitz, and M. Winter The influence of different conducting salts on the metal dissolution and capacity fading of NCM cathode material Electrochim. Acta 134 2014 393 398
23. P. Wobrauschek Total reflection X-ray fluorescence analysis - a review X-ray Spectrom. 36 2007 289 300
24. S. Weber, S. Nowak, and F. Schappacher Analytical methods for investigation of lithium-ion battery ageing A. Thaler, D. Watzenig, Automotive Battery Technology 2014 Springer International Publishing 71 87
25. I. De La Calle, N. Cabaleiro, V. Romero, I. Lavilla, and C. Bendicho Sample pretreatment strategies for total reflection X-ray fluorescence analysis: a tutorial review Spectrochim. Acta Part B 90 2013 23 54
26. B.U. Peschel, U.E.A. Fittschen, G. Pepponi, C. Jokubonis, C. Streli, P. Wobrauschek, G. Falkenberg, and J.A.C. Broekaert Direct analysis of Al2O3 powders by total reflection X-ray fluorescence spectrometry Anal. Bioanal. Chem. 382 2005 1958 1964
27. T.M. May, and R.H. Wiedmeyer A table of polyatomic interferences in ICP-MS At. Spectrosc. 19 1998 150 155
28. G. Ning, B. Haran, and B.N. Popov Capacity fade study of lithium-ion batteries cycled at high discharge rates J. Power Sources 117 2003 160 169
29. M. Winter, J.O. Besenhard, J.H. Albering, J. Yang, and M. Wachtler Lithium storage alloys as anode materials for lithium ion batteries Prog. Batteries Battery Mater. 17 1998 208
30. W.-R. Liu, Y.-C. Yen, H.-C. Wu, M. Winter, and N.-L. Wu Nano-porous SiO/carbon composite anode for lithium-ion batteries J. Appl. Electrochem. 39 2009 1643 1649
31. S. Goriparti, E. Miele, F. De Angelis, E. Di Fabrizio, R.P. Zaccaria, and C. Capiglia Review on recent progress of nanostructured anode materials for Li-ion batteries J. Power Sources 257 2014 421 443
32. P. Wobrauschek, R. Görgl, P. Kregsamer, Ch. Streli, S. Pahlke, L. Fabry, M. Haller, A. Knöchel, and M. Radtke Analysis of Ni on Si-wafer surfaces using synchrotron radiation excited total reflection X-ray fluorescence analysis1 Spectrochim. Acta Part B 52 1997 901 906
33. L. Terborg, S. Nowak, S. Passerini, M. Winter, U. Karst, P.R. Haddad, and P.N. Nesterenko Ion chromatographic determination of hydrolysis products of hexafluorophosphate salts in aqueous solution Anal. Chim. Acta 714 2012 121 126
34. V. Kraft, M. Grützke, W. Weber, J. Menzel, S. Wiemers-Meyer, M. Winter, and S. Nowak Two-dimensional ion chromatography for the separation of ionic organophosphates generated in thermally decomposed lithium hexafluorophosphate-based lithium ion battery electrolytes J. Chromatogr. A 1409 2015 201 209
35. V. Kraft, M. Grützke, W. Weber, M. Winter, and S. Nowak Ion chromatography electrospray ionization mass spectrometry method development and investigation of lithium hexafluorophosphate-based organic electrolytes and their thermal decomposition products J. Chromatogr. A 1354 2014 92 100
36. B. Vortmann, S. Nowak, and C. Engelhard Rapid characterization of lithium-ion battery electrolytes and thermal aging products by low-temperature plasma ambient ionization high-resolution mass spectrometry Anal. Chem. 85 2013 3433 3438
37. Y. Terada, Y. Nishiwaki, I. Nakai, and F. Nishikawa Study of Mn dissolution from LiMn2O4 spinel electrodes using in situ total reflection X-ray fluorescence analysis and fluorescence XAFS technique J. Power Sources 97-98 2001 420 422