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Volumn 51, Issue 57, 2015, Pages 11489-11492

Pd(OAc)2 in WERSA: A novel green catalytic system for Suzuki-Miyaura cross-coupling reactions at room temperature

Author keywords

[No Author keywords available]

Indexed keywords

ANISOLE DERIVATIVE; BENZENEBORONIC ACID; PALLADIUM COMPLEX; RICE STRAW ASH EXTRACT; UNCLASSIFIED DRUG;

EID: 84936944875     PISSN: 13597345     EISSN: 1364548X     Source Type: Journal    
DOI: 10.1039/c5cc04561d     Document Type: Article
Times cited : (87)

References (53)
  • 1
    • 24044470646 scopus 로고    scopus 로고
    • C. J. Li Chem. Rev. 2005 105 3095 3165
    • (2005) Chem. Rev. , vol.105 , pp. 3095-3165
    • Li, C.J.1
  • 21
  • 49
    • 85079918872 scopus 로고    scopus 로고
    • note
    • Method for preparation of WERSA: 10 g of rice straw ash was suspended in 100 mL of distilled water in a beaker and stirred well for 15 min at room temperature. The mixture was then filtered through a sintered glass crucible and the filtrate was used as WERSA
  • 52
    • 85079930461 scopus 로고    scopus 로고
    • note
    • 2 (1 mol%) in WERSA (3 mL) was stirred for the indicated time (Table 2) at room temperature. Afterward, the reaction solution was extracted three times with diethyl ether (3 × 10 mL). The products were purified by column chromatography over silica gel using n-hexane/ethyl acetate (9 : 1 v/v) to get the desired cross-coupling products. The products were characterized by IR and NMR spectroscopy methods.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.