Analysis of phytosterols and phytostanols in enriched dairy products by fast gas chromatography with mass spectrometry

Journal of Separation Science

Volumn 37, Issue 20, 2014, Pages 2911-2919

  Inchingolo, Raffaella ^a   Cardenia, Vladimiro ^a   Rodriguez Estrada, Maria Teresa ^a  

^a UNIVERSITY OF BOLOGNA   (Italy)

Author keywords

Enriched products; Fast gas chromatography; Functional dairy products; Phytostanols; Phytosterols

Indexed keywords

ALCOHOLS; COLUMN CHROMATOGRAPHY; DAIRIES; DAIRY PRODUCTS; GASES; LIPIDS; MASS SPECTROMETRY; SILICONES;

ANALYTICAL PERFORMANCE; CAPILLARY GAS CHROMATOGRAPHY; CHROMATOGRAPHIC PEAKS; ENRICHED PRODUCTS; FAST GAS CHROMATOGRAPHY; GAS CHROMATOGRAPHY-MASS SPECTROMETRY METHODS; PHYTOSTANOLS; PHYTOSTEROLS;

GAS CHROMATOGRAPHY;

CAMPESTANOL; CAMPESTEROL; SITOSTANOL; SITOSTEROL; STIGMASTEROL; PHYTOSTEROL;

ARTICLE; CAPILLARY GAS CHROMATOGRAPHY; DAIRY PRODUCT; EXTRACTION; MASS FRAGMENTOGRAPHY; SAPONIFICATION; SILYLATION; ANALYSIS; LIMIT OF DETECTION; PROCEDURES; REPRODUCIBILITY; STANDARD;

DAIRY PRODUCTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; PHYTOSTEROLS; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS;

EID: 84908027565     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201400322     Document Type: Article

References (29)

1. García-Llatas, G., Rodríguez-Estrada, M. T., Chem. Phys. Lipids 2011, 164, 607-624.
2. Lagarda, M. J., García-Llatas, G., Farré, R., J. Pharm. Biomed. Anal. 2006, 41, 1486-1496.
3. Cantrill, R., Kawamura, Y., Phytosterols, phytostanols and their esters, chemical and technical assessments. Proceedings of 69th JEFCA 2008, 1-13.
4. Commission Regulation (EU) No. 258/97 of 27 January 1997, Off. J. Eur. Commun. 1997, L43, 1-7.
5. Normén, L., Frohlich, J., Trautwein, E., in: Dutta, P. C. (Ed.), Phytosterols as Functional Food Components and Nutraceuticals, Marcel Dekker, New York 2004.
6. EFSA, The EFSA J. 2008, 133, 1-21.
7. Laakso, P., Eur. J. Lipid Sci. Technol. 2005, 107, 402-410.
8. Duchateau, G. S. M. J. E., Bauer-Plank, C. G., Louter, A. J. H., Van Der Ham, M., Boerma, J. A., Van Rooijen, J. J. M., Zandbelt, P. A., J. Am. Oil Chem. Soc. 2002, 79, 273-278.
9. Mendiara, I., Domeño, C., Nerín, C., J. Sep. Sci. 2012, 35, 3308-3316.
10. Esche, R., Barnsteiner, A., Scholz, B., Engel, K. H., J. Agric. Food Chem. 2012, 60, 5330-5339.
11. Esche, R., Carcelli, A., Barnsteiner, A., Sforza, S., Engel, K. H., Eur. Food Res. Technol. 2013, 236, 999-1007.
12. Commission Regulation (EEC) No. 2568/91 of 11 July 1991, Off. J. Eur. Commun. 1991, L248, 1-83.
13. International Organization for Standardization (ISO) No. 12228-1:2014 and 12228-2.
14. Abidi, S. L., J. Chromatogr. A 2001, 935, 173-201.
15. Cardenia, V., Rodríguez-Estrada, M. T., Baldacci, E., Savioli, S., Lercker, G., J. Sep. Sci. 2012, 35, 424-430.
16. Alemany-Costa, L., Gonzalez-Larena, M., García-Llatas, G., Alegria, A., Barbera, R., Sanchez-Siles, L. M., Lagarda, M. J., Food Res. Int. 2012, 48, 265-270.
17. Gonzalez-Larena, M., García-Llatas, G., Vidal, M. C., Barbera, R., Sanchez-Siles, L. M., Barbera, R., Lagarda, M. J., J. Agric. Food Chem. 2011, 59, 3624-3631.
18. Menendez-Carreño, M., Ansorena, D., Astiasaran, I., J. Agric. Food Chem. 2008, 56, 9997-10002.
19. Sweeley, C. C., Beutley, R., Mokita, M., Wells, W. W., J. Am. Chem. Soc. 1963, 85, 2497-2507.
20. Boselli, E., Velazco, V., Caboni, M. F., Lercker, G., J. Chromatogr. A 2001, 917, 239-244.
21. Folch, J., Lees, M., Sloane-Stanley, G. H., J. Biol. Chem. 1957, 226, 497-509.
22. Sander, B. D., Addis, P. B., Park, S. W., Smith, D. E., J. Food Prot. 1989, 52, 109-114.
23. McNaught, A. D., Wilkinson A., Compendium of Chemical Terminology IUPAC Recommendations, Blackwell Science, New York 1997.
24. Dutta, P. C., in: Guardiola, F., Dutta, P. C., Codony, R., Savage, G. P. (Eds.), Determination of Phytosterol Oxidation Products in Foods and Biological Samples in Cholesterol and Phytosterol Oxidation Products: Analysis, Occurrence and Biological Effects, AOCS Press, Champaign 2002, pp. 335-374.
25. Barnsteiner, A., Esche, R., di Gianvito, A., Chiavaro, E., Schmid, W., Engel, K.-H., Food Control 2012, 27, 275-283.
26. Borkovcová, I., Janoušková, E., Dračková, M., Janštová, B., Vorlová, L., Czech J. Food Sci. 2009, 27, S217-S219.
27. Conchillo, A., Cercaci, L., Ansorena, D., Rodriguez-Estrada, M. T., Lercker, G., Astiasarán, I., J. Agric. Food Chem. 2005, 53, 7844-7850.
28. Contarini, G., Povolo, M., Bonfitto, E., Berardi, S., Int. Dairy J. 2002, 12, 573-578.
29. European Commission Decision 2004/335 of 31 March 2004, Off. J. Eur. Commun. 2004, L105, 46-47.