X-ray energy-dispersive spectrometry during in situ liquid cell studies using an analytical electron microscope

Microscopy and Microanalysis

Volumn 20, Issue 2, 2014, Pages 323-329

  Zaluzec, Nestor J ^a,b   Burke, M Grace ^b   Haigh, Sarah J ^b   Kulzick, Matthew A ^c  

^a ARGONNE NATIONAL LABORATORY   (United States)

^b UNIVERSITY OF MANCHESTER   (United Kingdom)

^c BP Corporate Research Center ^*  (United States)

Author keywords

AEM; eCell; EELS; in situ; liquid cell; microanalysis; spectroscopy; STEM; TEM; XEDS

Indexed keywords

EID: 84899473178     PISSN: 14319276     EISSN: 14358115     Source Type: Journal    
DOI: 10.1017/S1431927614000154     Document Type: Article

References (17)

1. Chenna, S. & Crozer, P.A. (2011). Operando TEM-Detection of gas phase catalysis in an environmental TEM with EELS. Microsc Microanal 17(Suppl 2), 476-477.
2. Crewe, A.V. (1971). High resolution scanning microscopy of biological specimens. Philos Trans R Soc B 261, 61-70.
3. Crozer, P.A. & Chenna, S. (2011). In situ analysis of gas composition by electron energy-loss spectroscopy for environmental transmission electron microscopy. Ultramicroscopy 111, 177-185.
4. De Jonge, N. & Ross, F.M. (2011). Electron microscopy of specimens in liquid. Nat Nanotechnol 6, 695-704.
5. Egerton, R.F. (1986). Electron Energy Loss Spectroscopy. NewYork: Plenum Press.
6. Fraser, H.L., Klenov, D.O., Wang, Y.C., Cheng, H. & Zaluzec, N.J. (2011). On the performance of XEDS and EELS in the AEM: 25 years later. Microsc Microanal 17(Suppl 2), 590-591, doi:10.1017/S1431927611003825.
7. Holtz, M.E., Yu, Y., Gao, J., Abruña, H.D. & Muller, D.A. (2013). In situ electron energy-loss spectroscopy in liquids. Microsc Microanal 19, 1027-1035.
8. Howie, A. (1979). Image-contrast and localized signal selection techniques. J Microsc 117, 11-23.
9. Jungjohann, K.L., Evans, J.E., Aguiar, J.A., Arslan, I. & Browning, N.D. (2012). Atomic-scale imaging and spectroscopy for in situ liquid scanning transmission electron microscopy. Microsc Microanal 18, 621-627.
10. Liu, K.L., Wu, C.C., Huang, Y.J., Pang, H.L., Chang, H.Y., Chang, P., Hsu, L. & Yew, T.R. (2008). Novel microchip for in situ TEM imaging of living organisms and bio-reactions in aqueous conditions. Lab Chip 8, 1915-1921.
11. Malis, T., Cheng, S.C. & Egerton, R.F. (1988). EELS log-ratio technique for specimen-Thickness measurement in the TEM. J Elec Micro Tech 8, 193-200.
12. Pennycook, S.J. (2012). Seeing the atoms more clearly: STEM imaging from the Crewe era to today. Ultramicroscopy 123, 28-37.
13. Ring, E.A. & De Jonge, N. (2010).Microfluidic systemfor transmission electron microscopy. Microsc Microanal 16, 622-629.
14. Symposium ON NEW OPPORTUNITIES FOR IN-SITU (2013). New opportunities for in situ techniques and instruments. Microsc Microanal 19(Suppl 2), 392-476.
15. Williams, D.B. & Carter, C.B. (2009). Transmission Electron Microscopy: A Textbook for Materials Science. USA: Springer-Verlag.
16. Zaluzec, N.J. (1979). Introduction to Analytical Electron Microscopy. New York: Plenum Press, Chapter 4, 121-168.
17. Zaluzec, N.J. (2009). Detector solid angle formulas for use in X-ray energy dispersive spectrometry. Microsc Microanal 15, 93-98.