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Volumn 18, Issue 4, 2014, Pages 520-527

Development of a robust process for the preparation of high-quality dicyclopropylamine hydrochloride

Author keywords

[No Author keywords available]

Indexed keywords

OPTIMIZATION;

EID: 84898980069     PISSN: 10836160     EISSN: 1520586X     Source Type: Journal    
DOI: 10.1021/op500031z     Document Type: Article
Times cited : (23)

References (35)
  • 10
    • 84864596036 scopus 로고    scopus 로고
    • references therein
    • Rao, K. S.; Wu, T.-S. Tetrahedron 2012, 68, 7735-7754 and references therein
    • (2012) Tetrahedron , vol.68 , pp. 7735-7754
    • Rao, K.S.1    Wu, T.-S.2
  • 11
    • 0000611561 scopus 로고
    • 2 character of the cyclopropyl groups and increased acidity of N-H, we postulate that the following anionic degradation pathway may be occurring: A similar radical bond scission has been reported for DCPA, see: Maeda, Y.; Ingold, K. U. J. Am. Chem. Soc. 1980, 102, 328-331
    • (1980) J. Am. Chem. Soc. , vol.102 , pp. 328-331
    • Maeda, Y.1    Ingold, K.U.2
  • 19
    • 84863337570 scopus 로고    scopus 로고
    • Cu(II) sulfate has been used in Chan-Lam couplings, see
    • Cu(II) sulfate has been used in Chan-Lam couplings, see: Xu, H.-J.; Zhao, Y.-Q.; Feng, T.; Feng, Y.-S. J. Org. Chem. 2012, 77, 2878-2884
    • (2012) J. Org. Chem. , vol.77 , pp. 2878-2884
    • Xu, H.-J.1    Zhao, Y.-Q.2    Feng, T.3    Feng, Y.-S.4
  • 30
    • 70149117010 scopus 로고    scopus 로고
    • Use of more stable CPBA MIDA ester resulted in no reaction under the standard process conditions, see
    • Use of more stable CPBA MIDA ester resulted in no reaction under the standard process conditions, see: Knapp, D. M.; Gillis, E. P.; Burke, M. D. J. Am. Chem. Soc. 2009, 131, 6961-63
    • (2009) J. Am. Chem. Soc. , vol.131 , pp. 6961-6963
    • Knapp, D.M.1    Gillis, E.P.2    Burke, M.D.3
  • 31
    • 41449085514 scopus 로고    scopus 로고
    • For use of other odorless thiols in deprotection of nosylamines, see
    • For use of other odorless thiols in deprotection of nosylamines, see: Matoba, M.; Kajimoto, T.; Node, M. Synth. Commun. 2008, 38, 1194-1200
    • (2008) Synth. Commun. , vol.38 , pp. 1194-1200
    • Matoba, M.1    Kajimoto, T.2    Node, M.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.