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Volumn 62, Issue 12, 2014, Pages 2506-2515

Accurate determination of reference materials and natural isolates by means of quantitative 1H NMR spectroscopy

Author keywords

ERETIC 2; PULCON; qHNMR; quantitative NMR; reference compounds

Indexed keywords

AMINO ACIDS; BENZOIC ACID; MOLECULES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PEPTIDES;

EID: 84896937905     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf405529b     Document Type: Article
Times cited : (135)

References (35)
  • 2
    • 84867456874 scopus 로고    scopus 로고
    • Electrospray ionization mass spectrometry. A technique to access the information beyond the molecular weight of the analyte
    • Banerjee, S.; Mazumdar, S. Electrospray ionization mass spectrometry. A technique to access the information beyond the molecular weight of the analyte Int. J. Anal. Chem. 2012, 2012, 40
    • (2012) Int. J. Anal. Chem. , vol.2012 , pp. 40
    • Banerjee, S.1    Mazumdar, S.2
  • 5
    • 0035146874 scopus 로고    scopus 로고
    • QHNMR - A versatile concept for validation of natural product reference compounds
    • Pauli, G. F. qHNMR-A versatile concept for validation of natural product reference compounds Phytochem. Anal. 2001, 12, 28-42
    • (2001) Phytochem. Anal. , vol.12 , pp. 28-42
    • Pauli, G.F.1
  • 7
    • 12944265405 scopus 로고    scopus 로고
    • 1H NMR: Development and potential of a method for natural products analysis
    • 1H NMR: development and potential of a method for natural products analysis J. Nat. Prod. 2005, 68, 133-149
    • (2005) J. Nat. Prod. , vol.68 , pp. 133-149
    • Pauli, G.F.1    Jaki, B.U.2    Lankin, D.C.3
  • 8
    • 23644446181 scopus 로고    scopus 로고
    • Validation of quantitative NMR
    • Malz, F.; Jancke, H. Validation of quantitative NMR J. Pharm. Biomed. Anal. 2005, 38, 813-823
    • (2005) J. Pharm. Biomed. Anal. , vol.38 , pp. 813-823
    • Malz, F.1    Jancke, H.2
  • 9
    • 33845444839 scopus 로고    scopus 로고
    • Calibration by NMR for quantitative analysis: P -toluenesulfonic acid as a reference substance
    • Shao, G.; Kautz, R.; Peng, S.; Cui, G.; Giese, R. W. Calibration by NMR for quantitative analysis: p -toluenesulfonic acid as a reference substance J. Chromatogr., A 2008, 1138, 305-308
    • (2008) J. Chromatogr., A , vol.1138 , pp. 305-308
    • Shao, G.1    Kautz, R.2    Peng, S.3    Cui, G.4    Giese, R.W.5
  • 10
    • 34948883306 scopus 로고    scopus 로고
    • A comparative uncertainty study of the calibration of macrolide antibiotic reference standards using quantitative nuclear magnetic resonance and mass balance methods
    • Liu, S.-Y.; Hu, C.-Q. A comparative uncertainty study of the calibration of macrolide antibiotic reference standards using quantitative nuclear magnetic resonance and mass balance methods Anal. Chim. Acta 2007, 602, 114-121
    • (2007) Anal. Chim. Acta , vol.602 , pp. 114-121
    • Liu, S.-Y.1    Hu, C.-Q.2
  • 11
    • 44749086734 scopus 로고    scopus 로고
    • Validation of quantitative NMR method for suspected counterfeit products exemplified on determination of benzethonium chloride in grapefruit seed extracts
    • Bekiroglu, S.; Myrberg, O.; Östman, K.; Ek, M.; Arvidsson, T.; Rundlöf, T.; Hakkarainen, B. Validation of quantitative NMR method for suspected counterfeit products exemplified on determination of benzethonium chloride in grapefruit seed extracts J. Pharm. Biomed. Anal. 2008, 47, 958-961
    • (2008) J. Pharm. Biomed. Anal. , vol.47 , pp. 958-961
    • Bekiroglu, S.1    Myrberg, O.2    Östman, K.3    Ek, M.4    Arvidsson, T.5    Rundlöf, T.6    Hakkarainen, B.7
  • 12
    • 62749136939 scopus 로고    scopus 로고
    • A quantitative NMR protocol for the simultaneous analysis of atropine and obidoxime in parenteral injection devices
    • Sharma, R.; Gupta, P. K.; Mazumder, A.; Dubey, D. K.; Ganesan, K.; Vijayaraghavan, R. A quantitative NMR protocol for the simultaneous analysis of atropine and obidoxime in parenteral injection devices J. Pharm. Biomed. Anal. 2009, 49, 1092-1096
    • (2009) J. Pharm. Biomed. Anal. , vol.49 , pp. 1092-1096
    • Sharma, R.1    Gupta, P.K.2    Mazumder, A.3    Dubey, D.K.4    Ganesan, K.5    Vijayaraghavan, R.6
  • 13
    • 77954215037 scopus 로고    scopus 로고
    • Quantitative NMR spectroscopy in pharmaceutical applications
    • Holzgrabe, U. Quantitative NMR spectroscopy in pharmaceutical applications Prog. Nucl. Magn. Reson. Spectrom. 2010, 57, 229-240
    • (2010) Prog. Nucl. Magn. Reson. Spectrom. , vol.57 , pp. 229-240
    • Holzgrabe, U.1
  • 16
    • 0033169005 scopus 로고    scopus 로고
    • Concentration measurement by proton NMR using the ERETIC method
    • Akoka, S.; Barantin, L.; Trierweiler, M. Concentration measurement by proton NMR using the ERETIC method Anal. Chem. 1999, 71, 2554-2557
    • (1999) Anal. Chem. , vol.71 , pp. 2554-2557
    • Akoka, S.1    Barantin, L.2    Trierweiler, M.3
  • 17
    • 0037112554 scopus 로고    scopus 로고
    • 2H NMR spectroscopy: The ERETIC method as a generic reference signal
    • 2H NMR spectroscopy: the ERETIC method as a generic reference signal Anal. Chem. 2002, 74, 5902-5906
    • (2002) Anal. Chem. , vol.74 , pp. 5902-5906
    • Billault, I.1    Robins, R.2    Akoka, S.3
  • 18
    • 0036138810 scopus 로고    scopus 로고
    • Quantitative NMR spectroscopy using coaxial inserts containing a reference standard: Purity determinations for military nerve agents
    • Henderson, T. J. Quantitative NMR spectroscopy using coaxial inserts containing a reference standard: purity determinations for military nerve agents Anal. Chem. 2002, 74, 191-198
    • (2002) Anal. Chem. , vol.74 , pp. 191-198
    • Henderson, T.J.1
  • 19
    • 49549133678 scopus 로고
    • The signal-to-noise ratio of the nuclear magnetic resonance experiment
    • Hoult, D. I.; Richards, R. E. The signal-to-noise ratio of the nuclear magnetic resonance experiment J. Magn. Reson. 1976, 24, 71-85
    • (1976) J. Magn. Reson. , vol.24 , pp. 71-85
    • Hoult, D.I.1    Richards, R.E.2
  • 20
    • 18844378856 scopus 로고    scopus 로고
    • 1H NMR with external standards: Use in preparation of calibration solutions for algal toxins and other natural products
    • 1H NMR with external standards: use in preparation of calibration solutions for algal toxins and other natural products Anal. Chem. 2005, 77, 3123-3131
    • (2005) Anal. Chem. , vol.77 , pp. 3123-3131
    • Burton, I.W.1    Quilliam, M.A.2    Walter, J.A.3
  • 21
    • 33644647902 scopus 로고    scopus 로고
    • Measuring protein concentrations by NMR spectroscopy
    • Wider, G.; Dreier, L. Measuring protein concentrations by NMR spectroscopy J. Am. Chem. Soc. 2006, 128, 2571-2576
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 2571-2576
    • Wider, G.1    Dreier, L.2
  • 22
    • 80054080818 scopus 로고    scopus 로고
    • Development of stable isotope dilution assay for ochratoxin A in blood samples
    • Korn, M.; Frank, O.; Hofmann, T.; Rychlik, M. Development of stable isotope dilution assay for ochratoxin A in blood samples Anal. Biochem. 2011, 419, 88-94
    • (2011) Anal. Biochem. , vol.419 , pp. 88-94
    • Korn, M.1    Frank, O.2    Hofmann, T.3    Rychlik, M.4
  • 23
    • 0242331098 scopus 로고    scopus 로고
    • Activity-guided identification of a chemopreventive in coffee using in vitro and in vivio techniques
    • Somoza, V.; Lindenmeier, M.; Wenzel, E.; Frank, O.; Erbersdobler, H. F.; Hofmann, T. Activity-guided identification of a chemopreventive in coffee using in vitro and in vivio techniques J. Agric. Food Chem. 2003, 51, 6861-6869
    • (2003) J. Agric. Food Chem. , vol.51 , pp. 6861-6869
    • Somoza, V.1    Lindenmeier, M.2    Wenzel, E.3    Frank, O.4    Erbersdobler, H.F.5    Hofmann, T.6
  • 24
    • 0039464472 scopus 로고
    • The preparation of salts of N -methylnicotinic acid
    • Chiusa, W.; Nebbia, G. The preparation of salts of N -methylnicotinic acid Gaz. Chim. Ital. 1950, 80, 98-99
    • (1950) Gaz. Chim. Ital. , vol.80 , pp. 98-99
    • Chiusa, W.1    Nebbia, G.2
  • 25
    • 58149383873 scopus 로고    scopus 로고
    • Driving force analysis of proton tunnelling across a reactivity series for an enzyme-substrate complex
    • Hothi, P.; Hay, S.; Roujeinikova, A.; Sutcliffe, M.; Lee, M.; Leys, D.; Scrutton, N. Driving force analysis of proton tunnelling across a reactivity series for an enzyme-substrate complex ChemBioChem 2008, 9, 2839-2845
    • (2008) ChemBioChem , vol.9 , pp. 2839-2845
    • Hothi, P.1    Hay, S.2    Roujeinikova, A.3    Sutcliffe, M.4    Lee, M.5    Leys, D.6    Scrutton, N.7
  • 26
    • 0028850152 scopus 로고
    • Synthesis of (S)-2-amino-1,1-diphenylbutan-4-ol; Conversion of an α-amino acid into an α-(diphenylmethyl) amine without loss of optical purity
    • Boyle, P. H.; Davis, A. P.; Dempsey, K. J.; Hosken, G. D. Synthesis of (S)-2-amino-1,1-diphenylbutan-4-ol; conversion of an α-amino acid into an α-(diphenylmethyl) amine without loss of optical purity Tetrahedron Asymmetry 1995, 6, 2819-2828
    • (1995) Tetrahedron Asymmetry , vol.6 , pp. 2819-2828
    • Boyle, P.H.1    Davis, A.P.2    Dempsey, K.J.3    Hosken, G.D.4
  • 27
    • 78049234356 scopus 로고    scopus 로고
    • 2-(1-carboxyethyl)guanosine 5′- monophosphate as an umami-enhancing Maillard-modified nucleotide in yeast extracts
    • 2-(1-carboxyethyl) guanosine 5′-monophosphate as an umami-enhancing Maillard-modified nucleotide in yeast extracts J. Agric. Food Chem. 2010, 58, 10614-10622
    • (2010) J. Agric. Food Chem. , vol.58 , pp. 10614-10622
    • Festring, D.1    Hofmann, T.2
  • 28
    • 0035138620 scopus 로고    scopus 로고
    • Method for the quantitative extraction of resveratrol and piceid isomers in grape berry skins. Effect of powdery mildew on the stilbene content
    • Romero-Pérez, A. I.; Lamuela-Raventós, R. M.; Andrés-Lacueva, C.; de la Torre-Boronat, M. C. Method for the quantitative extraction of resveratrol and piceid isomers in grape berry skins. Effect of powdery mildew on the stilbene content J. Agric. Food Chem. 2001, 49, 210-215
    • (2001) J. Agric. Food Chem. , vol.49 , pp. 210-215
    • Romero-Pérez, A.I.1    Lamuela-Raventós, R.M.2    Andrés-Lacueva, C.3    De La Torre-Boronat, M.C.4
  • 29
    • 84859743120 scopus 로고    scopus 로고
    • Isolation and structure elucidation of highly antioxidative 3,8″-linked biflavanones and flavanone-C-glycosides from Garcinia buchananii bark
    • Stark, T. D.; Matsumoto, T.; Lösch, S.; Boakye, P. A.; Balemba, O. B.; Pasilis, S. P.; Hofmann, T. Isolation and structure elucidation of highly antioxidative 3,8″-linked biflavanones and flavanone-C-glycosides from Garcinia buchananii bark J. Agric. Food Chem. 2012, 60, 2053-2062
    • (2012) J. Agric. Food Chem. , vol.60 , pp. 2053-2062
    • Stark, T.D.1    Matsumoto, T.2    Lösch, S.3    Boakye, P.A.4    Balemba, O.B.5    Pasilis, S.P.6    Hofmann, T.7
  • 30
    • 76449117175 scopus 로고    scopus 로고
    • Development of a stable isotope dilution analysis for the quantification of the Bacillus cereus toxin cereulide in foods
    • Bauer, T.; Stark, T.; Hofmann, T.; Ehling-Schulz, M. Development of a stable isotope dilution analysis for the quantification of the Bacillus cereus toxin cereulide in foods J. Agric. Food Chem. 2010, 58, 1420-1428
    • (2010) J. Agric. Food Chem. , vol.58 , pp. 1420-1428
    • Bauer, T.1    Stark, T.2    Hofmann, T.3    Ehling-Schulz, M.4
  • 31
    • 58149121310 scopus 로고    scopus 로고
    • Solvent signal as an NMR concentration reference
    • Mo, H.; Raftery, D. Solvent signal as an NMR concentration reference Anal. Chem. 2008, 80, 9835-9839
    • (2008) Anal. Chem. , vol.80 , pp. 9835-9839
    • Mo, H.1    Raftery, D.2
  • 32
    • 58949096676 scopus 로고    scopus 로고
    • Quantitative investigation of trigonelline, nicotinic acid, and nicotinamide in foods, urine, plasma by means of LC-MS/MS and stable isotope dilution analysis
    • Lang, R.; Yagar, E. F.; Eggers, R.; Hofmann, T. Quantitative investigation of trigonelline, nicotinic acid, and nicotinamide in foods, urine, plasma by means of LC-MS/MS and stable isotope dilution analysis J. Agric. Food Chem. 2008, 56, 11114-11121
    • (2008) J. Agric. Food Chem. , vol.56 , pp. 11114-11121
    • Lang, R.1    Yagar, E.F.2    Eggers, R.3    Hofmann, T.4
  • 33
  • 35
    • 0033593357 scopus 로고    scopus 로고
    • Cyclolinopeptides B-E, new cyclic peptides from Linum usitatissimum
    • Morita, H.; Shishido, A.; Matsumoto, T.; Itokawa, H.; Takeya, K. Cyclolinopeptides B-E, new cyclic peptides from Linum usitatissimum Tetrahedron 1999, 55, 967-976
    • (1999) Tetrahedron , vol.55 , pp. 967-976
    • Morita, H.1    Shishido, A.2    Matsumoto, T.3    Itokawa, H.4    Takeya, K.5


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.