The evaluation of a fast and simple pesticide multiresidue method in various herbs by gas chromatography

Journal of Natural Medicines

Volumn 68, Issue 1, 2014, Pages 95-111

  Łozowicka, Bozena ^a   Jankowska, Magdalena ^a   Rutkowska, Ewa ^a   Hrynko, Izabela ^a   Kaczyński, Piotr ^a   Miciński, Jan ^b  

^a Laboratory of Pesticide Residues   (Poland)

^b UNIVERSITY OF WARMIA AND MAZURY IN OLSZTYN   (Poland)

Author keywords

Gas chromatography; Herb; LSE; MSPD; Multiresidue method; Pesticide

Indexed keywords

PESTICIDE RESIDUE;

ANALYSIS; CALIBRATION; CHEMISTRY; COMPARATIVE STUDY; ENVIRONMENTAL MONITORING; FOOD CONTAMINATION; GAS CHROMATOGRAPHY; LIMIT OF DETECTION; MEDICINAL PLANT; PROCEDURES; REPRODUCIBILITY; SOLID PHASE EXTRACTION; STANDARD; STANDARDS; VALIDATION STUDY;

CALIBRATION; CHROMATOGRAPHY, GAS; ENVIRONMENTAL MONITORING; FOOD CONTAMINATION; LIMIT OF DETECTION; PESTICIDE RESIDUES; PLANTS, MEDICINAL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SOLID PHASE EXTRACTION;

EID: 84893766422     PISSN: 13403443     EISSN: 18610293     Source Type: Journal    
DOI: 10.1007/s11418-013-0777-9     Document Type: Article

References (39)

1. Yang YC, Lu FH, Wu JS, Wu CH, Chang CJ (2004) The protective effect of habitual tea consumption on hypertension. Arch Intern Med 164:1534-1540
2. Gilani AH, Shaheen E, Saeed SA, Bibi S, Irfanullah, Sadiq M, Faizi S (2000) Hypotensive action of coumarin glycosides from Daucus carota. Phytomedicine 7:423-426
3. Panchawat S, Rathore KS, Sisodia SS (2010) A review on herbal antioxidants. Intern J Pharm Tech Res 2:232-239
4. Kaufmann SHE (2009) Your amazing immune system, how it protects your body. European Federation of Immunological Societies, pp 20-29
5. Kosalec I, Cvek J, Tomic S (2009) Contaminants of medicinal herbs and herbal products. Arh Hig Rada Toksikol 60:485-501
6. Rai V, Kakkar P, Misra C, Ojha SK, Srivastava N, Mehrotra S (2007) Metals and organochlorine pesticide residues in some herbal ayurvedic formulations. Bull Environ Contam Toxicol 79:269-272
7. Huggett DB, Khan IA, Allgood JC, Blosck DS, Schlenk D (2001) Organochlorine pesticides and metals in select botanical dietary supplements. Bull Environ Contam Toxicol 66:150-155
8. Ahmed MT, Loutfy N, Yousef Y (2001) Contamination of medicinal herbs with organophosphorus insecticides. Bull Environ Contam Toxicol 66:421-426
9. World Health Organization (2007) WHO guidelines for assessing quality of herbal medicines. http://apps.who.int/medicinedocs/documents/s14878e/s14878e.pdf
10. Regulation (EC) (2005) No 396/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC
11. European Pharmacopoeia (2011) 7th edn. European Directorate for the Quality of Medicines and Health Care, Strasbourg
12. DG SANCO (2008) EU Pesticide database. http://ec.europa.eu/sanco- pesticides/public/index.cfm. Accessed 15 Jan 2013
13. Wan YQ, Mao XJ, Yan AP, Shen MY, Wu YM (2010) Simultaneous determination of organophosphorus pesticides in Chinese herbal medicines by microwave-assisted extraction coupled with dispersive-solid phase extraction and gas chromatography. Biomed Chromatogr 24:961-968
14. Hao L, Xue J (2006) Multiresidue analysis of 18 organochlorine pesticides in traditional Chinese medicin. J Chromatogr Sci 44:518-522
15. Dai R, Ren X, He X, Huo Y (2011) Convenient analytical method for quantitative determination of 23 pesticide residues in herbs by gas chromatography-mass spectrometry. Bull Environ Contam Toxicol 86:559-564
16. Rao MM, Kumarmeena A, Galib (2011) Detection of toxic heavy metals and pesticide residue in herbal plants which are commonly used in the herbal formulations. Environ Monit Assess 181:267-271
17. Nguyen TD, Lee KJ, Lee MH, Lee GH (2010) A multiresidue method for the determination 234 pesticides in Korean herbs using gas chromatography mass spectrometry. Microchem J 95:43-49
18. Wang Y, Jin HY, Ma SC, Lu J, Lin RC (2011) Determination of 195 pesticide residues in Chinese herbs by gas chromatography-mass spectrometry using analyte protectants. J Chromatogr A 1218:334-342
19. Zanella R, Prestes OD, do Amaral Friggi C, Martins ML, Bohrer Adaime M (2012) Modern sample preparation methods for pesticide multiresidue determination in foods of animal origin by chromatographic-mass spectrometric techniques. In Jokanovic M, ed. The impact of pesticides. AcademyPublish.org
20. Hedges LJ, Lister CE (2007) Nutritional attributes of herbs. Crop and Food Research Confidential Report No. 1891, Horticulture, New Zealand
21. Myoung-Gun C, Min-Seuk L (2011) Optimal extraction conditions for simultaneous determination of catechins and caffeine in green tea leaves. Food Sci Biotechnol 20:327-333
22. Dawidowicz AL, Wianowska D (2009) Application of the MSPD technique for the HPLC analysis of rutin in Sambucus nigra L. The linear correlation of the MSPD process. J Chromatogr Sci 47:914-918
23. Martinez A, Ramil M, Montes R, Hernanz D, Rubi E, Rodrigez I, Cela Torrijos R (2005) Development of a matrix solid-phase dispersion method for the screening of polybrominated diphenyl ethers and polychlorinated biphenyls in biota samples using gas chromatography with electron-capture detection. J Chromatogr A 1072:83-91
24. Karasova G, Lehotay J (2004) MSPD extraction of phenolic compounds from fruit-green tea using different non-polar sorbents. J Liq Chrom 27:2837-2845
25. Perret D, Gentili A, Marchese S, Sergi M (2004) Determination of free fatty acids in chocolate by liquid chromatography with tandem mass spectrometry. Rapid Commun Mass Spectrom 18:1989-1994
26. Soler C, Manes J, Pico Y (2004) Liquid chromatography-electrospray quadrupole ion trap mass spectrometry of nine pesticides in fruits. J Chromatogr A 1048:41-49
27. Lozowicka B, Jankowska M, Kaczyński P (2012) Pesticide residues in Brassica vegetables and exposure assessment of consumers. Food Control 25:561-575
28. Lozowicka B, Jankowska M, Rutkowska E, Kaczyński P, Hrynko I (2012) Comparison of extraction techniques by matrix solid phase dispersion and liquid-liquid for screening 150 pesticides from soil, and determination by gas chromatography. Pol J Environ Stud 21:973-992
29. Kristenson EM, Shahmiri S, Slooten CJ, Vreuls RJJ, Brinkman UATh (2004) Matrix solid-phase dispersion micro-extraction of pesticides from single insects with subsequent GC-MS analysis. Chromatographia 59:315-320
30. De Carvalho PHV, De Menezes Prata V, Alves PB, Navickiene S (2009) Determination of six pesticides in the medicinal herb Cordia salicifolia by matrix solid-phase dispersion and gas chromatography/mass spectrometry. J AOAC Int 92:184-1189
31. De Carvalho PHV, Barreto AS, Rodrigues MO, de M Prata V, Alves PB, de Mesquita ME, Alves Jr S, Navickiene S (2009) Two-dimensional coordination polymer matrix for solid-phase extraction of pesticide residues from plant Cordia salicifolia. J Sep Sci 32:2132-2138
32. Tang F, Yue Y, Hua R, Cao H (2006) Matrix solid-phase dispersion microextraction and determination of pesticide residues in medicinal herbs by gas chromatography with a nitrogen-phosphorus detector. J AOAC Int 89:498-502
33. SANCO (2009) Document No. SANCO/10684/2009. Method validation and quality control procedures for pesticides residues analysis in food and feed, http://ec.europa.eu/food/plant/protection/resources/qualcontrol-en.pdf
34. GUM (1993) Guide to the expression of uncertainty in measurement. International Organization for Standardization, Geneva
35. PPDB, Pesticide Properties DataBase, University of Hertfordshire, http://sitem.herts.ac.uk/aeru/footprint/en/. Accessed 15 Jan 2013
36. ChemSpider, The free chemical database, http://www.chemspider.com/. Accessed 15 Jan 2013
37. PN-EN ISO/IEC (2005) 17025:2005 Ogólne wymagania dotyczãce kompetencji laboratoriów badawczych i wzorcuja̧cych. PKN Polski Komitet Normalizacyjny, Poland
38. The Stockholm Convention on Persistent Organic Pollutants (POPs) (2010) Amendments to Annexes A, B and C, Switzerland, Geneva
39. Capriotti AL, Cavaliere C, Lagana A, Piovesana S, Samperi R (2013) Recent trends in matrix solid-phase dispersion. Trends Anal Chem 43:53-66