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Volumn 70, Issue 3, 2014, Pages 637-642

Total synthesis and assignment of the absolute stereochemistry of xanthoangelol J: Development of a highly efficient method for Claisen-Schmidt condensation Dedicated to Late (Dr.) Jadab C. Sarma on his 55th birthday on first May 2013

Author keywords

Chalcone; Green synthesis; KHSO4; Total synthesis; Xanthoangelol J

Indexed keywords

ANTINEOPLASTIC AGENT; UNCLASSIFIED DRUG; XANTHOANGELOL J;

EID: 84892920425     PISSN: 00404020     EISSN: 14645416     Source Type: Journal    
DOI: 10.1016/j.tet.2013.11.106     Document Type: Article
Times cited : (13)

References (23)
  • 22
    • 0343777334 scopus 로고    scopus 로고
    • Enantiomeric excess (ee) was determined by HPLC analysis using a Waters 510 HPLC system. Compounds 5a and 5b were subjected to acetylation prior to HPLC using acetic anhydride in pyridine at 0 C, A Chiracel OD packed in a SS column of 4.6 mm i.d.×250 mm was used. Isocratic elution was applied with a mobile phase consisting of n-hexane 90% and isopropanol 10% at a flow rate of 0.8 mL/min and a pressure of 125 psi with UV detection at 243 nm
    • Enantiomeric excess (ee) was determined by HPLC analysis using a Waters 510 HPLC system. Compounds 5a and 5b were subjected to acetylation prior to HPLC using acetic anhydride in pyridine at 0 C A. Rodríguez, M. Nomen, B.W. Spur, J.-J. Godfroid, and T.H. Lee Eur. J. Org. Chem. 2000 2991 A Chiracel OD packed in a SS column of 4.6 mm i.d.×250 mm was used. Isocratic elution was applied with a mobile phase consisting of n-hexane 90% and isopropanol 10% at a flow rate of 0.8 mL/min and a pressure of 125 psi with UV detection at 243 nm
    • (2000) Eur. J. Org. Chem. , pp. 2991
    • Rodríguez, A.1    Nomen, M.2    Spur, B.W.3    Godfroid, J.-J.4    Lee, T.H.5


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.