-
1
-
-
33845471763
-
-
(a) Tomioka, K.; Ando, K.; Takemasa, Y.; Koga, K. J. Am. Chem. Soc. 1984, 106, 2718.
-
(1984)
J. Am. Chem. Soc
, vol.106
, pp. 2718
-
-
Tomioka, K.1
Ando, K.2
Takemasa, Y.3
Koga, K.4
-
3
-
-
0025895518
-
-
(c) Lubell, W. D.; Kitamura, M.; Noyori, R. Tetrahedron: Asymmetry 1991, 2, 543.
-
(1991)
Tetrahedron: Asymmetry
, vol.2
, pp. 543
-
-
Lubell, W.D.1
Kitamura, M.2
Noyori, R.3
-
4
-
-
0028003718
-
-
(d) Bartoli, G.; Cimarelli, C.; Marcantoni, E.; Palmieri, G.; Petrini, M. J. Org. Chem. 1994, 59, 5328.
-
(1994)
J. Org. Chem
, vol.59
, pp. 5328
-
-
Bartoli, G.1
Cimarelli, C.2
Marcantoni, E.3
Palmieri, G.4
Petrini, M.5
-
5
-
-
37049066616
-
-
(a) Bartoli, G.; Bosco, M.; Cimarelli, C.; Dalpozzo, R.; Guercio, G.; Palmieri, G. J. Chem. Soc., Perkin Trans. 1 1993, 2081.
-
(1993)
J. Chem. Soc., Perkin Trans. 1
, pp. 2081
-
-
Bartoli, G.1
Bosco, M.2
Cimarelli, C.3
Dalpozzo, R.4
Guercio, G.5
Palmieri, G.6
-
6
-
-
37049084255
-
-
(b) Bartoli, G.; Bosco, M.; Cimarelli, C.; Dalpozzo, R.; Palmieri, G. J. Chem. Soc., Perkin Trans. 1 1992, 2095.
-
(1992)
J. Chem. Soc., Perkin Trans. 1
, pp. 2095
-
-
Bartoli, G.1
Bosco, M.2
Cimarelli, C.3
Dalpozzo, R.4
Palmieri, G.5
-
7
-
-
0001538857
-
-
(c) Bartoli, G.; Bosco, M.; Cimarelli, C.; Dalpozzo, R.; Munno, G. D.; Guercio, G.; Palmier, G. J. Org. Chem. 1992, 57, 6020.
-
(1992)
J. Org. Chem
, vol.57
, pp. 6020
-
-
Bartoli, G.1
Bosco, M.2
Cimarelli, C.3
Dalpozzo, R.4
Munno, G.D.5
Guercio, G.6
Palmier, G.7
-
8
-
-
0033601207
-
-
(a) Alberola, A.; Calvo, L. A.; Ortega, A. G.; Ruiz, M. C. S.; Yustos, P. J. Org. Chem. 1999, 64, 9493.
-
(1999)
J. Org. Chem
, vol.64
, pp. 9493
-
-
Alberola, A.1
Calvo, L.A.2
Ortega, A.G.3
Ruiz, M.C.S.4
Yustos, P.5
-
9
-
-
37049100321
-
-
(b) Chaaban, I.; Greenhill, J. V.; Akhtar, P. J. Chem. Soc., Perkin Trans. 1 1979, 1593.
-
(1979)
J. Chem. Soc., Perkin Trans. 1
, pp. 1593
-
-
Chaaban, I.1
Greenhill, J.V.2
Akhtar, P.3
-
13
-
-
0348082239
-
-
(f) Müller, A.; Maier, A.; Neumann, R.; Maas, G. Eur. J. Org. Chem. 1998, 1177.
-
(1998)
Eur. J. Org. Chem
, pp. 1177
-
-
Müller, A.1
Maier, A.2
Neumann, R.3
Maas, G.4
-
14
-
-
2742515855
-
-
(g) Bejan, E.; Aït-Haddou, H.; Daran, J. C.; Balavoine, G. G. A. Eur. J. Org. Chem. 1998, 2907.
-
(1998)
Eur. J. Org. Chem
, pp. 2907
-
-
Bejan, E.1
Aït-Haddou, H.2
Daran, J.C.3
Balavoine, G.G.A.4
-
15
-
-
0037367811
-
-
Eddington, N. D.; Cox, D. S.; Khurana, M.; Salama, N. N.; Stables, J. P.; Harrison, S. J.; Negussie, A.; Taylor, R. S.; Tran, U. Q.; Moore, J. A.; Barrow, J. C.; Scott, K. R. Eur. J. Med. Chem. 2003, 49.
-
(2003)
Eur. J. Med. Chem
, pp. 49
-
-
Eddington, N.D.1
Cox, D.S.2
Khurana, M.3
Salama, N.N.4
Stables, J.P.5
Harrison, S.J.6
Negussie, A.7
Taylor, R.S.8
Tran, U.Q.9
Moore, J.A.10
Barrow, J.C.11
Scott, K.R.12
-
17
-
-
0001153055
-
-
Dannhardt, G.; Bauer, A.; Nowe, U. J. Prakt. Chem. 1998, 340, 256.
-
(1998)
J. Prakt. Chem
, vol.340
, pp. 256
-
-
Dannhardt, G.1
Bauer, A.2
Nowe, U.3
-
18
-
-
0024393748
-
-
Boger, D. L.; Ishizaki, T.; Wysocki, J. R.; Munk, S. A.; Kitos, P. A.; Suntornwat, O. J. Am. Chem. Soc. 1989, 111, 6461.
-
(1989)
J. Am. Chem. Soc
, vol.111
, pp. 6461
-
-
Boger, D.L.1
Ishizaki, T.2
Wysocki, J.R.3
Munk, S.A.4
Kitos, P.A.5
Suntornwat, O.6
-
20
-
-
0001862808
-
-
(b) Martin, D. F.; Janusonis, G. A.; Martin, B. B. J. Am. Chem. Soc. 1961, 83, 73.
-
(1961)
J. Am. Chem. Soc
, vol.83
, pp. 73
-
-
Martin, D.F.1
Janusonis, G.A.2
Martin, B.B.3
-
21
-
-
0001180149
-
-
(c) Ferraz, H. M. C.; Oliceira, E. O.; Payret-Arrua, M. E.; Brandt, C. A. J. Org. Chem. 1995, 60, 7357.
-
(1995)
J. Org. Chem
, vol.60
, pp. 7357
-
-
Ferraz, H.M.C.1
Oliceira, E.O.2
Payret-Arrua, M.E.3
Brandt, C.A.4
-
25
-
-
0032887356
-
-
(a) Zhu, G.; Chen, Z.; Zhang, X. J. Org. Chem. 1999, 64, 6907.
-
(1999)
J. Org. Chem
, vol.64
, pp. 6907
-
-
Zhu, G.1
Chen, Z.2
Zhang, X.3
-
29
-
-
0037074078
-
-
Rodríguez, H.; Reyes, O.; Suarez, M.; Garay, H. E.; Pérez, R.; Cruz, L. J.; Verdecia, Y.; Martín, N.; Seoane, C. Tetrahedron Lett. 2002, 43, 439.
-
(2002)
Tetrahedron Lett
, vol.43
, pp. 439
-
-
Rodríguez, H.1
Reyes, O.2
Suarez, M.3
Garay, H.E.4
Pérez, R.5
Cruz, L.J.6
Verdecia, Y.7
Martín, N.8
Seoane, C.9
-
33
-
-
0001862808
-
-
Martin, D. F.; Janusonis, G. A.; Martin, B. B. J. Am. Chem. Soc. 1961, 83, 73.
-
(1961)
J. Am. Chem. Soc
, vol.83
, pp. 73
-
-
Martin, D.F.1
Janusonis, G.A.2
Martin, B.B.3
-
35
-
-
84953866141
-
-
(b) Bieräugel, H.; Akkerman, J. M.; Lapierre Armande, J. C.; Pandit, U. K. Recl. Trav. Chim. Pays-Bas 1976, 95, 266.
-
(1976)
Recl. Trav. Chim. Pays-Bas
, vol.95
, pp. 266
-
-
Bieräugel, H.1
Akkerman, J.M.2
Lapierre Armande, J.C.3
Pandit, U.K.4
-
37
-
-
0034532847
-
-
(d) Yapi, A. D.; Mustofa, M.; Valentin, A.; Chavignon, O.; Teulade, J. C.; Mallie, M.; Chapat, J.-P.; Blache, Y. Chem. Pharm. Bull. 2000, 48, 1886.
-
(2000)
Chem. Pharm. Bull
, vol.48
, pp. 1886
-
-
Yapi, A.D.1
Mustofa, M.2
Valentin, A.3
Chavignon, O.4
Teulade, J.C.5
Mallie, M.6
Chapat, J.-P.7
Blache, Y.8
-
39
-
-
29944447672
-
-
(b) Brown, R. J.; Carver, F. W. S.; Hollingsworth, B. L. J. Org. Chem. 1967, 32, 2624.
-
(1967)
J. Org. Chem
, vol.32
, pp. 2624
-
-
Brown, R.J.1
Carver, F.W.S.2
Hollingsworth, B.L.3
-
40
-
-
3142767629
-
-
(c) Brandt, C. A.; Da Silva, A. C. M. P.; Pancote, C. G.; Brito, C. L.; Da Silveira, M. A. B. Synthesis 2004, 1557.
-
(2004)
Synthesis
, pp. 1557
-
-
Brandt, C.A.1
Da Silva, A.C.M.P.2
Pancote, C.G.3
Brito, C.L.4
Da Silveira, M.A.B.5
-
41
-
-
32844458664
-
-
Das, B.; Venkateswarlu, K.; Majhi, A.; Reddy, R. M.; Reddy, N. K.; Rao, K. Y.; Ravikumar, K.; Sridhar, B. J. Mol. Catal. A: Chem. 2006, 246, 276.
-
(2006)
J. Mol. Catal. A: Chem
, vol.246
, pp. 276
-
-
Das, B.1
Venkateswarlu, K.2
Majhi, A.3
Reddy, R.M.4
Reddy, N.K.5
Rao, K.Y.6
Ravikumar, K.7
Sridhar, B.8
-
42
-
-
0031454850
-
-
Cartaya-Marin, C. P.; Henderson, D. G.; Soeder, R. W. Synth. Commun. 1997, 27, 4275.
-
(1997)
Synth. Commun
, vol.27
, pp. 4275
-
-
Cartaya-Marin, C.P.1
Henderson, D.G.2
Soeder, R.W.3
-
43
-
-
0027160846
-
-
(a) Rechsteimer, B.; Texier-Boullet, F.; Hamelin, J. Tetrahedron Lett. 1993, 34, 5071.
-
(1993)
Tetrahedron Lett
, vol.34
, pp. 5071
-
-
Rechsteimer, B.1
Texier-Boullet, F.2
Hamelin, J.3
-
44
-
-
0842286088
-
-
(b) Braibante, H. T. S.; Braibante, M. E. F.; Rosso, G. B.; Oriques, D. A. J. Braz. Chem. Soc. 2003, 14, 994.
-
(2003)
J. Braz. Chem. Soc
, vol.14
, pp. 994
-
-
Braibante, H.T.S.1
Braibante, M.E.F.2
Rosso, G.B.3
Oriques, D.A.4
-
45
-
-
0031827953
-
-
Valduga, C. J.; Squizani, A.; Braibante, H. S.; Braibante, M. E. F. Synthesis 1998, 1019.
-
(1998)
Synthesis
, pp. 1019
-
-
Valduga, C.J.1
Squizani, A.2
Braibante, H.S.3
Braibante, M.E.F.4
-
48
-
-
1642410348
-
-
Gao, Y.-H.; Zhang, Q.-H.; Xu, J.-X. Synth. Commun. 2004, 34, 909.
-
(2004)
Synth. Commun
, vol.34
, pp. 909
-
-
Gao, Y.-H.1
Zhang, Q.-H.2
Xu, J.-X.3
-
49
-
-
1342344846
-
-
Bartoli, G.; Bosco, M.; Locatelli, M.; Marcantoni, E.; Melchiorre, P.; Sambri, L. Synlett 2004, 239.
-
(2004)
Synlett
, pp. 239
-
-
Bartoli, G.1
Bosco, M.2
Locatelli, M.3
Marcantoni, E.4
Melchiorre, P.5
Sambri, L.6
-
51
-
-
0043154088
-
-
Arcadi, A.; Bianchi, G.; Di Giuseppe, S.; Marinelli, F. Green Chem. 2003, 5, 64.
-
(2003)
Green Chem
, vol.5
, pp. 64
-
-
Arcadi, A.1
Bianchi, G.2
Di Giuseppe, S.3
Marinelli, F.4
-
52
-
-
33645959544
-
-
Dalpozzo, R.; Nino, A. D.; Nardi, M.; Russo, B.; Procopio, A. Synthesis 2006, 1127.
-
(2006)
Synthesis
, pp. 1127
-
-
Dalpozzo, R.1
Nino, A.D.2
Nardi, M.3
Russo, B.4
Procopio, A.5
-
53
-
-
1142288504
-
-
Silva, F. C.; De Souza, M. C. B. V.; Ferreira, V. F.; Sabino, S. J.; Antunes, O. A. C. Catal. Commun. 2004, 5, 151.
-
(2004)
Catal. Commun
, vol.5
, pp. 151
-
-
Silva, F.C.1
De Souza, M.C.B.V.2
Ferreira, V.F.3
Sabino, S.J.4
Antunes, O.A.C.5
-
54
-
-
0033771259
-
-
Stefani, H. A.; Costa, I. M.; de O. Silva, D. Synthesis 2000, 1526.
-
Stefani, H. A.; Costa, I. M.; de O. Silva, D. Synthesis 2000, 1526.
-
-
-
-
55
-
-
0842348272
-
-
Khosropour, A. R.; Khodaei, M. M.; Kookhazadeh, M. Tetrahedron Lett. 2004, 45, 1725.
-
(2004)
Tetrahedron Lett
, vol.45
, pp. 1725
-
-
Khosropour, A.R.1
Khodaei, M.M.2
Kookhazadeh, M.3
-
56
-
-
20044365621
-
-
Khodaei, M. M.; Khosropour, A. R.; Kookhazadeh, M. Can. J. Chem. 2005, 83, 209.
-
(2005)
Can. J. Chem
, vol.83
, pp. 209
-
-
Khodaei, M.M.1
Khosropour, A.R.2
Kookhazadeh, M.3
-
57
-
-
31544466241
-
-
Zhang, Z.-H.; Yin, L.; Wang, Y.-M. Adv. Synth. Catal. 2006, 348, 184.
-
(2006)
Adv. Synth. Catal
, vol.348
, pp. 184
-
-
Zhang, Z.-H.1
Yin, L.2
Wang, Y.-M.3
-
58
-
-
0035113507
-
-
Kaupp, G.; Schmeyers, J.; Boy, J. Chemosphere 2001, 43, 55.
-
(2001)
Chemosphere
, vol.43
, pp. 55
-
-
Kaupp, G.1
Schmeyers, J.2
Boy, J.3
-
59
-
-
62449114289
-
-
General Procedure for the Preparation of b-Enamino Ketones A mixture of the solid 1,3-dicarbonyl compound (5 mmol, amine (or ammonium, 5 mmol, and KHSO4/SiO2 (0.136 g, weight ratio 1:1) was ground in a mortar at r.t. for the appropriate time. After completion of the reaction as indicated by TLC, the reaction mixture was extracted with CH 2Cl2 (2 x 10 mL, The combined organic layers were dried over Na2SO4 and concentrated under reduced pressure to give a product with high purity. The solid product could be further purified by recrystallization in PE (Table 2, entries 1-15) or in EtOH (Table 3, entries 1-12, 3-Amino-1-phenylbut-2-en-1-one (2a) Mp 138-140°C; lit. 33a 144-145°C. 1H NMR (500 MHz, CDCl3, δ, 2.06 (s, 3 H, 5.21 (br, 1 H, NH, 5.74 (s, 1 H, 7.39-7.45 (m, 3 H, 7.87-7.89 (m, 2 H, 10.22 (br, 1 H, NH, 13C NMR 125 MHz, CDCl 3
-
3): δ = 21.18, 97.54, 122.26, 125.22,
-
-
-
-
67
-
-
37049092102
-
-
(h) Tan, S. F.; Ang, K. P.; Jayachandran, H. J. Chem. Soc., Perkin Trans. 2 1983, 1011.
-
(1983)
J. Chem. Soc., Perkin Trans. 2
, pp. 1011
-
-
Tan, S.F.1
Ang, K.P.2
Jayachandran, H.3
-
68
-
-
20044365621
-
-
(i) Khodaei, M. M.; Khosropour, A. R.; Kookhazadeh, M. Can. J. Chem. 2005, 83, 209.
-
(2005)
Can. J. Chem
, vol.83
, pp. 209
-
-
Khodaei, M.M.1
Khosropour, A.R.2
Kookhazadeh, M.3
-
69
-
-
45449090049
-
-
(j) Lyubchanskaya, V. M.; Mukhanova, T. I.; Panisheva, E. K.; Alekseeva, L. M.; Granik, V. G. Khim. Farm. Zh. 1995, 29, 40;
-
(1995)
Khim. Farm. Zh
, vol.29
, pp. 40
-
-
Lyubchanskaya, V.M.1
Mukhanova, T.I.2
Panisheva, E.K.3
Alekseeva, L.M.4
Granik, V.G.5
-
70
-
-
62449318687
-
-
Chem. Abstr. 1995, 124, 145843.
-
(1995)
Chem. Abstr
, vol.124
, pp. 145843
-
-
-
73
-
-
33847249481
-
-
(m) Bannikova, Y. N.; Khalturina, V. V.; Sedegova, E. A.; Maslivets, A. N. Russ. J. Org. Chem. 2007, 43, 154.
-
(2007)
Russ. J. Org. Chem
, vol.43
, pp. 154
-
-
Bannikova, Y.N.1
Khalturina, V.V.2
Sedegova, E.A.3
Maslivets, A.N.4
|