Fabrication of a sealed electrochemical microcell for in situ soft X-ray microspectroscopy and testing with in situ co-polypyrrole composite electrodeposition for pt-free oxygen electrocatalysis

Analytical Chemistry

Volumn 86, Issue 1, 2014, Pages 664-670

  Bozzini, Benedetto ^a   Gianoncelli, Alessandra ^b   Bocchetta, Patrizia ^a   Dal Zilio, Simone ^c   Kourousias, George ^b  

^a UNIVERSITY OF SALENTO   (Italy)

^b SINCROTRONE TRIESTE   (Italy)

^c IOM CNR LABORATORIO TASC   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

COMPOSITE ELECTRODEPOSITION; ELECTROCHEMICAL CONTROL; ELECTROCHEMICAL EXPERIMENTS; ELECTROCHEMICAL MICRO-CELL; ELECTROCHEMICAL WET CELLS; MICROFABRICATED CHANNELS; OXYGEN ELECTROCATALYSIS; ULTRAVIOLET LITHOGRAPHY;

ELECTROCATALYSIS; ELECTROCATALYSTS; ELECTROLYTES; EXPERIMENTS; FABRICATION; POLYPYRROLES; X RAYS;

ELECTROCHEMICAL ELECTRODES;

OXYGEN; PLATINUM; POLYMER; POLYPYRROLE; PYRROLE DERIVATIVE;

ARTICLE; CATALYSIS; ELECTROCHEMICAL ANALYSIS; ELECTRON PROBE MICROANALYSIS; ELECTROPLATING INDUSTRY; METABOLISM; METHODOLOGY;

CATALYSIS; ELECTROCHEMICAL TECHNIQUES; ELECTRON PROBE MICROANALYSIS; ELECTROPLATING; OXYGEN; PLATINUM; POLYMERS; PYRROLES;

EID: 84891795238     PISSN: 00032700     EISSN: 15206882     Source Type: Journal    
DOI: 10.1021/ac403004v     Document Type: Article

References (32)

1. Bozzini, B.; Lacitignola, D.; Mele, C.; Sgura, I. Acta Appl. Math. 2012, 122, 53-68
2. Bozzini, B.; Kazemian Abyaneh, M.; Amati, M.; Gianoncelli, A.; Gregoratti, L.; Kaulich, B.; Kiskinova, M. Chem.-Eur. J. 2012, 18, 10196-10210
3. Guay, D.; Stewart-Ornstein, J.; Zhang, X.; Hitchcock, A. P. Anal. Chem. 2005, 77, 3479-3487
4. Bozzini, B.; Amati, M.; Gianoncelli, A.; Gregoratti, L.; Kaulich, B.; Kiskinova, M. J. Phys.: Conf. Ser 2013, 463, 182018
5. Bozzini, B.; Gianoncelli, A.; Kaulich, B.; Mele, C.; Prasciolu, M.; Kiskinova, M. Fuel Cells (Wiley), published online: 7 DEC 2012, DOI: 10.1002/fuce.201200036.
6. Bozzini, B.; Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Mele, C.; Prasciolu, M. Phys. Chem. Chem. Phys. 2011, 13, 7968-7974
7. Bozzini, B.; Mele, C.; Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Prasciolu, M. Microelectron. Eng. 2011, 88, 2456-2458
8. Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Prasciolu, M.; D'Urzo, L.; Bozzini, B. Micron 2011, 42, 342-347
9. Bozzini, B.; Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Prasciolu, M.; Sgura, I. ChemSusChem 2010, 7, 846-850
10. Bozzini, B.; D'Urzo, L.; Gianoncelli, A.; Kaulich, B.; Prasciolu, M.; Sgura, I.; Tondo, E.; Kiskinova, M. J. Phys. Chem. C 2009, 113, 9783-9788
11. Bozzini, B.; D'Urzo, L.; Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Prasciolu, M.; Tadjeddine, A. J. Phys.: Conf. Ser 2009, 186, 012103
12. Bozzini, B.; D'Urzo, L.; Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Prasciolu, M.; Tadjeddine, A. Electrochem. Commun. 2008, 10, 1680-1683
13. Bozzini, B.; Gianoncelli, A.; Mele, C.; Kiskinova, M. Electrochim. Acta 2013, 10.1016/j.electacta.2013.07.062
14. Gianoncelli, A.; Kaulich, B.; Kiskinova, M.; Mele, C.; Prasciolu, M.; Sgura, I.; Bozzini, B. J. Phys.: Conf. Ser. 2013, 425, 182010-182013
15. Bozzini, B.; Gianoncelli, A.; Kaulich, B.; Mele, C.; Prasciolu, M.; Kiskinova, M. J. Power Sources 2012, 211, 71-76
16. Bozzini, B.; Gianoncelli, A.; Mele, C.; Sgura, I.; Kiskinova, M. ChemElectroChem, in press.
17. Nguyen-Thanh, A. D.; Frenkelb, I.; Wang, J.; O'Brien, S.; Akins, D. L. Appl. Catal., B 2011, 105, 50-60
18. Bashyam, R.; Zelenay, P. Nature 2006, 443, 63-66
19. Yuasa, M.; Yamaguchi, A.; Itsuki, H.; Tanaka, K.; Yamamoto, M.; Oyaizu, K. Chem. Mater. 2005, 17, 4278-4281
20. Tourillon, G.; Garnier, F. J. Phys. Chem. 1984, 88, 5281-5285
21. COMSOL Multiphysics, V. 3.5, Modeling Guide; COSMOL: Burlington, MA, 2008.
22. Gianoncelli, A.; Morrison, G. R.; Kaulich, B.; Bacescu, D.; Kovac, J. Appl. Phys. Lett. 2006, 89, 251117-251119
23. Kaulich, B.; Susini, J.; David, C.; Di Fabrizio, E.; Morrison, G.; Charalambous, P.; Thieme, J.; Wilhein, T.; Kovac, J.; Bacescu, D.; Salome, M.; Dhez, O.; Weitkamp, T.; Cabrini, S.; Cojoc, D.; Gianoncelli, A.; Vogt, U.; Podnar, M.; Zangrando, M.; Zacchigna, M.; Kiskinova, M. In Proc. 8th Int. Conf. X-ray Microscopy; Aoki, S., Kagoshima, Y., Suzuki, Y., Eds.; Conf. Proc. Series IPAP Vol. 7, 2005; pp 22-25.
24. Kaulich, B.; Thibault, P.; Gianoncelli, A.; Kiskinova, M. J. Phys.: Condens. Matter 2011, 23, 083002-083025
25. Masa, J.; Schilling, T.; Bron, M.; Schuhmann, W. Electrochim. Acta 2012, 60, 410-418
26. Downard, A. J.; Pletcher, D. J. Electroanal. Chem. 1986, 206, 139-145
27. Zhou, M.; Heinze, J. J. Phys. Chem. B 1999, 103, 84519-8457
28. Mele, C.; Rondinini, S.; D'Urzo, L.; Romanello, V.; Tondo, E.; Minguzzi, A.; Vertova, A.; Bozzini, B. J. Solid State Electrochem. 2009, 13, 1577-1584
29. Morales, F.; de Groot, F. M. F.; Glatzel, P.; Kleimenov, E.; Bluhm, H.; Havecker, M.; Knop-Gericke, A.; Weckhuysen, B. M. J. Phys. Chem. B 2004, 108, 16201-16207
30. Zheng, F.; Alayoglu, S.; Pushkarev, V. V.; Beaumont, S. K.; Specht, C.; Aksoy, F.; Liud, Z.; Guo, J.; Somorjai, G. A. Catal. Today 2012, 182, 54-59
31. Liu, H.; Guo, J.; Yin, Y.; Augustsson, A.; Dong, C.; Nordgren, J.; Chang, C.; Alivalstos, P.; Thornton, G.; Ogletree, D. F.; Requjo, F. G.; De Groot, F.; Salmeron, M. Nano Lett. 2007, 7, 1919-1922
32. Papaefthimiou, V.; Dintzer, T.; Dupuis, V.; Tamion, A.; Tournus, F.; Hillion, A.; Teschner, D.; Hävecker, M.; Knop-Gericke, A.; Schlögl, R.; Zafeiratos, S. ACS Nano 2011, 5, 2182-2190