Slurry concentration effects on the bed morphology and separation efficiency of capillaries packed with sub-2μm particles

Journal of Chromatography A

Volumn 1318, Issue , 2013, Pages 189-197

  Bruns, Stefan ^a   Franklin, Edward G ^b   Grinias, James P ^b   Godinho, Justin M ^b   Jorgenson, James W ^b   Tallarek, Ulrich ^a  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

^b University of North Carolina at Chapel Hill   (United States)

Author keywords

Bed microstructure; Capillary UHPLC; Core shell particles; Packing process; Transcolumn dispersion; Wall effects

Indexed keywords

CAPILLARY UHPLC; CHROMATOGRAPHIC PERFORMANCE; CONFOCAL LASER SCANNING MICROSCOPY; CORE-SHELL PARTICLE; THREE-DIMENSIONAL ANALYSIS; THREE-DIMENSIONAL RECONSTRUCTION; ULTRA-HIGH-PRESSURE LIQUID CHROMATOGRAPHY; WALL EFFECTS;

CAPILLARITY; DISPERSIONS; EFFICIENCY; LIQUID CHROMATOGRAPHY; PARTICLE SIZE; THREE DIMENSIONAL;

PACKED BEDS;

ARTICLE; CAPILLARY CHROMATOGRAPHY; CONFOCAL LASER MICROSCOPY; CONTROLLED STUDY; PARTICLE SIZE; POROSITY; PRIORITY JOURNAL; SEPARATION TECHNIQUE; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; PARTICLE SIZE; POROSITY; RESINS, SYNTHETIC;

EID: 84887169153     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.10.017     Document Type: Article

References (58)

1. Gritti F., Guiochon G. J. Chromatogr. A 2012, 1228:2.
2. Farkas T., Chitty M., Layne J., Anspach J., Sanchez C. The New Cutting Edge in Reversed-Phase UHPLC Performance: 1.3μm Core-Shell Particles 2013, Oral Presentation at HPLC, Amsterdam, The Netherlands.
3. Hiemenz P.C., Rajagopalan R. Principles of Colloid and Surface Chemistry 1997, CRC Press, Taylor & Francis Group, Boca Raton. 3rd ed.
4. Wahab M.F., Pohl C.A., Lucy C.A. J. Chromatogr. A 2012, 1270:139.
5. Rogers B.J., Wirth M.J. ACS Nano 2013, 7:725.
6. Wu Z., Rogers B.J., Wei B., Wirth M.J. J. Sep. Sci. 2013, 36:1871.
7. Wei B., Rogers B.J., Wirth M.J. J. Am. Chem. Soc. 2012, 134:10780.
8. Nováková L., Veuthey J.-L., Guillarme D. J. Chromatogr. A 2011, 1218:7971.
9. Gritti F., Martin M., Guiochon G. Anal. Chem. 2009, 81:3365.
10. de Villiers A., Lauer H., Szucs R., Goodall S., Sandra P. J. Chromatogr. A 2006, 1113:84.
11. Gritti F., Guiochon G. Anal. Chem. 2013, 85:3017.
12. Guiochon G. J. Chromatogr. A 2006, 1126:6.
13. Kirkland J.J., Langlois T.J., DeStefano J.J. Am. Lab. 2007, 39:18.
14. Gritti F., Leonardis I., Shock D., Stevenson P., Shalliker A., Guiochon G. J. Chromatogr. A 2010, 1217:1589.
15. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:8167.
16. Guiochon G., Gritti F. J. Chromatogr. A 2011, 1218:1915.
17. Daneyko A., Höltzel A., Khirevich S., Tallarek U. Anal. Chem. 2011, 83:3903.
18. Gritti F., Guiochon G. J. Chromatogr. A 2013, 1280:35.
19. Gritti F., Guiochon G. LC-GC North Am. 2012, 30:586.
20. Bruns S., Stoeckel D., Smarsly B.M., Tallarek U. J. Chromatogr. A 2012, 1268:53.
21. Abia J.A., Mriziq K.S., Guiochon G. J. Chromatogr. A 2009, 1216:3185.
22. Kirkland J.J., DeStefano J.J. J. Chromatogr. A 2006, 1126:50.
23. Bruns S., Höltzel A., Tallarek U. LC-GC North Am. 2013, 31:486.
24. Hormann K., Müllner T., Bruns S., Höltzel A., Tallarek U. J. Chromatogr. A 2012, 1222:46.
25. Bruns S., Hara T., Smarsly B.M., Tallarek U. J. Chromatogr. A 2011, 1218:5187.
26. Bruns S., Tallarek U. J. Chromatogr. A 2011, 1218:1849.
27. Bruns S., Müllner T., Kollmann M., Schachtner J., Höltzel A., Tallarek U. Anal. Chem. 2010, 82:6569.
28. Koku H., Maier R.S., Schure M.R., Lenhoff A.M. J. Chromatogr. A 2012, 1237:55.
29. Müllner T., Zankel A., Mayrhofer C., Reingruber H., Höltzel A., Lv Y., Svec F., Tallarek U. Langmuir 2012, 49:16733.
30. Stoeckel D., Kübel C., Tallarek U., Smarsly B. 3D Reconstruction of a Mesoporous Monolithic Silica Structure Using Scanning Transmission Electron Microscopy (STEM) Tomography 2013, Poster Presentation at HPLC, Amsterdam, The Netherlands.
31. Bruns S., Grinias J.P., Blue L.E., Jorgenson J.W., Tallarek U. Anal. Chem. 2012, 84:4496.
32. Hsieh S.C., Jorgenson J.W. Anal. Chem. 1996, 68:1212.
33. Patel K.D., Jerkovich A.D., Link J.C., Jorgenson J.W. Anal. Chem. 2004, 76:5777.
34. Jung S., Höltzel A., Ehlert S., Mora J.A., Kraiczek K., Dittmann M., Rozing G.P., Tallarek U. Anal. Chem. 2009, 81:10193.
35. Jung S., Ehlert S., Mora J.A., Kraiczek K., Dittmann M., Rozing G.P., Tallarek U. J. Chromatogr. A 2009, 1216:264.
36. Ehlert S., Trojer L., Vollmer M., van de Goor T., Tallarek U. J. Mass Spectrom. 2010, 45:313.
37. Ehlert S., Kraiczek K., Mora J.A., Dittmann M., Rozing G.P., Tallarek U. Anal. Chem. 2008, 80:5945.
38. Wyndham K.D., O'Gara J.E., Walter T.H., Glose K.H., Lawrence N.L., Alden B.A., Izzo G.S., Hudalla C.J., Iraneta P.C. Anal. Chem. 2003, 75:6781.
39. Neue U.D. HPLC Columns: Theory, Technology, and Practice 1997, Wiley-VCH, New York.
40. MacNair J.E., Lewis K.C., Jorgenson J.W. Anal. Chem. 1997, 69:983.
41. MacNair J.E., Patel K.D., Jorgenson J.W. Anal. Chem. 1999, 71:700.
42. Mellors J.S., Jorgenson J.W. Anal. Chem. 2004, 76:5441.
43. Maiolica A., Borsotti D., Rappsilber J. Proteomics 2005, 5:3847.
44. Knecht L.A., Guthrie E.J., Jorgenson J.W. Anal. Chem. 1984, 56:479.
45. Luisier F. PureDenoise, Biomedical Imaging Group, École Polytechnique Fédéral de Lausanne 2010, http://bigwww.epfl.ch/algorithms/denoise.
46. Rasband W.S. ImageJ 1997-2011, U.S. National Institutes of Health, Bethesda, MD, http://rsb.info.nih.gov//ij/.
47. Gritti F., Guiochon G. AIChE J. 2010, 56:1495.
48. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:6350.
49. Gritti F., Guiochon G. J. Chromatogr. A 2013, 1297:85.
50. Kaiser T.J., Thompson J.W., Mellors J.S., Jorgenson J.W. Anal. Chem. 2009, 81:2860.
51. Gritti F., Guiochon G. J. Chromatogr. A 2013, 1302:1.
52. Giddings J.C. Dynamics of Chromatography, Part 1: Principles and Theory 1965, Marcel Dekker, New York.
53. Khirevich S., Höltzel A., Seidel-Morgenstern A., Tallarek U. Anal. Chem. 2009, 81:7057.
54. Khirevich S., Höltzel A., Seidel-Morgenstern A., Tallarek U. J. Chromatogr. A 2012, 1262:77.
55. Ehlert S., Rösler T., Tallarek U. J. Sep. Sci. 2008, 31:1719.
56. Baranau V., Hlushkou D., Khirevich S., Tallarek U. Soft Matter 2013, 9:3361.
57. Schure M.R., Maier R.S. J. Chromatogr. A 2006, 1126:58.
58. Treadway J., Jorgenson J. Highly Efficient Capillary Columns Packed with Sub-2μm Superficially Porous Particles 2013, Oral presentation at HPLC, Amsterdam, The Netherlands.