Morphological analysis of physically reconstructed capillary hybrid silica monoliths and correlation with separation efficiency

Journal of Chromatography A

Volumn 1218, Issue 31, 2011, Pages 5187-5194

  Bruns, Stefan ^a   Hara, Takeshi ^b   Smarsly, Bernd M ^b   Tallarek, Ulrich ^a  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

^b JUSTUS LIEBIG UNIVERSITY   (Germany)

Author keywords

Chord length distribution; Eddy dispersion; Hybrid silica monoliths; Morphological analysis; Physical reconstruction; Radial heterogeneity

Indexed keywords

CHORD LENGTH DISTRIBUTION; EDDY DISPERSION; HYBRID SILICA MONOLITHS; MORPHOLOGICAL ANALYSIS; PHYSICAL RECONSTRUCTION; RADIAL HETEROGENEITY;

CONFOCAL MICROSCOPY; DISPERSIONS; LINGUISTICS; MORPHOLOGY; SILICA;

MONOLITHIC INTEGRATED CIRCUITS;

METHYLTRIMETHOXYSILANE; ORGANOSILICON DERIVATIVE; SILICON DIOXIDE; TETRAMETHOXYSILANE; UNCLASSIFIED DRUG;

ARTICLE; CALCULATION; CONFOCAL LASER MICROSCOPY; DISPERSION; IMAGE ANALYSIS; IMAGE PROCESSING; MORPHOLOGY; POROSITY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SEPARATION TECHNIQUE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MICROSCOPY, CONFOCAL; POROSITY; SILICON DIOXIDE;

EID: 79960128314     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.05.090     Document Type: Article

References (51)

1. Guiochon G. J. Chromatogr. A 2007, 1168:101.
2. Jungbauer A., Hahn R. J. Chromatogr. A 2008, 1184:62.
3. Unger K.K., Skudas R., Schulte M.M. J. Chromatogr. A 2008, 1184:393.
4. Aoki H., Tanaka N., Kubo T., Hosoya K. J. Sep. Sci. 2009, 32:341.
5. Sinner F., Buchmeiser M.R. Macromolecules 2000, 33:5777.
6. Mayr B., Hölzl G., Eder K., Buchmeiser M.R., Huber C.G. Anal. Chem. 2002, 74:6080.
7. Svec F. J. Sep. Sci. 2004, 27:747.
8. Nakanishi K., Tanaka N. Acc. Chem. Res. 2007, 40:863.
9. Nakanishi K., Minakuchi H., Soga N., Tanaka N. J. Sol-Gel Sci. Technol. 1997, 8:547.
10. Nakanishi K. J. Porous Mater. 1997, 4:67.
11. Minakuchi H., Nakanishi K., Soga N., Ishizuka N., Tanaka N. J. Chromatogr. A 1997, 762:135.
12. Nakanishi K., Minakuchi H., Soga N., Tanaka N. J. Sol-Gel Sci. Technol. 1998, 13:163.
13. Minakuchi H., Nakanishi K., Soga N., Ishizuka N., Tanaka N. J. Chromatogr. A 1998, 797:121.
14. Ishizuka N., Minakuchi H., Nakanishi K., Soga N., Tanaka N. J. Chromatogr. A 1998, 797:133.
15. Gritti F., Piatkowski W., Guiochon G. J. Chromatogr. A 2002, 978:81.
16. Leinweber F.C., Tallarek U. J. Chromatogr. A 2003, 1006:207.
17. Kele M., Guiochon G. J. Chromatogr. A 2002, 960:19.
18. Tallarek U., Leinweber F.C., Seidel-Morgenstern A. Chem. Eng. Technol. 2002, 25:1177.
19. Gritti F., Piatkowski W., Guiochon G. J. Chromatogr. A 2003, 983:51.
20. Cabrera K. J. Sep. Sci. 2004, 27:843.
21. Mazzeo J.R., Neue U.D., Kele M., Plumb R.S. Anal. Chem. 2005, 77:460A.
22. Kennedy R.T., Jorgenson J.W. Anal. Chem. 1989, 61:1128.
23. Guiochon G., Drumm E., Cherrak D. J. Chromatogr. A 1999, 835:41.
24. Shalliker R.A., Broyles B.S., Guiochon G. J. Chromatogr. A 2000, 888:1.
25. Shalliker R.A., Wong V., Broyles B.S., Guiochon G. J. Chromatogr. A 2002, 977:213.
26. Maier R.S., Kroll D.M., Bernard R.S., Howington S.E., Peters J.F., Davis H.T. Phys. Fluids 2003, 15:3795.
27. Khirevich S., Höltzel A., Hlushkou D., Tallarek U. Anal. Chem. 2007, 79:9340.
28. Khirevich S., Höltzel A., Seidel-Morgenstern A., Tallarek U. Anal. Chem. 2009, 81:7057.
29. Abia J.A., Mriziq K.S., Guiochon G.A. J. Chromatogr. A 2009, 1216:3185.
30. Abia J.A., Mriziq K.S., Guiochon G.A. J. Sep. Sci. 2009, 32:923.
31. Ishizuka N., Kobayashi H., Minakuchi H., Nakanishi K., Hirao K., Hosoya K., Ikegami T., Tanaka N. J. Chromatogr. A 2002, 960:85.
32. Bruns S., Müllner T., Kollmann M., Schachtner J., Höltzel A., Tallarek U. Anal. Chem. 2010, 82:6569.
33. Bruns S., Tallarek U. J. Chromatogr. A 2011, 1218:1849.
34. Courtois J., Szumski M., Georgsson F., Irgum K. Anal. Chem. 2007, 79:335.
35. Hlushkou D., Bruns S., Tallarek U. J. Chromatogr. A 2010, 1217:3674.
36. Hlushkou D., Bruns S., Höltzel A., Tallarek U. Anal. Chem. 2010, 82:7150.
37. Roux R., Abi Jaoudé M., Demesmay C. J. Chromatogr. A 2009, 1216:3857.
38. Hara T., Makino S., Watanabe Y., Ikegami T., Cabrera K., Smarsly B., Tanaka N. J. Chromatogr. A 2010, 1217:89.
39. Kanamori K., Yonezawa H., Nakanishi K., Hirao K., Jinnai H. J. Sep. Sci. 2004, 27:874.
40. Motokawa M., Ohira M., Minakuchi H., Nakanishi K., Tanaka N. J. Sep. Sci. 2006, 29:2471.
41. Malitson I.H. J. Opt. Soc. Am. 1965, 55:1205.
42. W.S. Rasband, ImageJ, U.S. National Institutes of Health, Bethesda, MD, 1997-2006, http://rsb.info.nih.gov//ij/.
43. S. Bochkanov, V. Bystritsky, ALGLIB (). http://www.alglib.net/.
44. Aste T., Di Matteo T. Phys. Rev. E 2008, 77:021309.
45. Giddings J.C. Dynamics of Chromatography. Part 1: Principles and Theory 1965, Marcel Dekker, New York.
46. Gritti F., Guiochon G. J. Chromatogr. A 2009, 1216:4752.
47. D. Hlushkou, S. Bruns, A. Seidel-Morgenstern, U. Tallarek, J. Sep. Sci. 34 (2011) in press, doi:10.1002/jssc.201100158.
48. Khirevich S., Daneyko A., Höltzel A., Seidel-Morgenstern A., Tallarek U. J. Chromatogr. A 2010, 1217:4713.
49. Schenker I., Filser F.T., Gauckler L.J., Aste T., Herrmann H.J. Phys. Rev. E 2009, 80:021302.
50. Kobayashi H., Tokuda D., Ichimaru J., Ikegami T., Miyabe K., Tanaka N. J. Chromatogr. A 2006, 1109:2.
51. Hara T., Kobayashi H., Ikegami T., Nakanishi K., Tanaka N. Anal. Chem. 2006, 78:7632.