Packing density of slurry-packed capillaries at low aspect ratios

Journal of Separation Science

Volumn 31, Issue 10, 2008, Pages 1719-1728

  Ehlert, Steffen ^a   Rösler, Thomas ^a   Tallarek, Ulrich ^a  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

Author keywords

Column to particle diameter ratio; Nano HPLC; Packed capillaries; Porosity; Wall effect

Indexed keywords

ASPECT RATIO; MICROCIRCULATION;

PACKING DENSITIES; VOIDAGE;

DIMENSIONAL STABILITY;

POLYSTYRENE; SILICON DIOXIDE; SOLVENT;

ARTICLE; CAPILLARY CHROMATOGRAPHY; CHEMICAL STRUCTURE; CONTROLLED STUDY; GEOMETRY; PARTICLE SIZE; POROSITY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SURFACE PROPERTY;

EID: 46249116925     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200800018     Document Type: Article

References (43)

1. de Klerk, A., AIChE J. 2003, i 49, 2022-2029.
2. Theuerkauf, J., Witt, P., Schwesig, D., Powder Technol. 2006, 165, 92-99.
3. Karlsson, K.-E., Novotny, M., Anal. Chem. 1988, 69, 1662-1665.
4. Kennedy, R. T., Jorgenson, J. W., Anal. Chem. 1989, 61, 1128-1135.
5. Li, W., Pyo, D., Wan, Y., Ibanez, E., Malik, A., Lee, M. L., J. Microcolumn Sep. 1996, 8, 259-268.
6. Hsieh, S. Jorgenson, J. W., Anal. Chem. 1996, 68, 1212-1217.
7. Winterberg, M., Tsotsas, E., AIChE J. 2000, 46, 1084-1088.
8. Eeltink, S., Rozing, G. P., Schoenmakers, P. J., Kok, W. Th., J. Chromatogr. A 2004, 1044, 311-316.
9. Delgado, J. M. P. Q., Heat Mass Transf. 2006, 42, 279-310.
10. Maier, R. S., Kroll, D. M., Davis, H. T., AChE J. 2007, 53, 527-530.
11. Roblee, L. H. S., Baird, R. M., Tierney, J. W., AIChE J. 1958, 4, 460-464.
12. Benenati, R. F., Brosilow, C. B., AIChE J. 1962, 8, 359-361.
13. Ridgway, K., Tarbuck, K.J., Chem. Eng. Sci. 1968, 23, 1147-1155.
14. Dixon, A. G., Can. J. Chem. Eng. 1988, 66, 705-708.
15. Mueller, R., Hofmann, H., Chem. Eng. Sci. 1990, 45, 2141-2146.
16. Mueller, G. E., Powder Technol. 1992, 72, 269-275.
17. Hosseini-Ashrafi, M. E., Tüzün, U., Chem. Eng. Sci. 1993, 48, 53-67.
18. Giese, M., Rottschäfer, K., Vortmeyer, D., AIChE J. 1998, 44, 484-490.
19. Sederman, A. J., Alexander, P., Gladden, L. F., Powder Technol. 2001, 117, 255-269.
20. Tang, D., Jess, A., Ren, X., Blümich, B., Stapf, S., Chem. Eng. Technol. 2004, 27, 866-873.
21. Ren, X., Stapf, S., Blümich, B., AIChE J. 2005, 51, 392-405.
22. Manz, B., Gladden, L. F., Warren, P. B., AIChE J. 1999, 45, 1845-1854.
23. Nandakumar, K., Shu, Y., Chuang, K. T., AIChE J. 1999, 45, 2286-2297.
24. Schnitzlein, K., Chem. Eng. Sci. 2001, 56, 579-585.
25. Maier, R. S., Kroll, D. M., Bernard, R. S., Howington, S. E., Peters, J. F., Davis, H. T., Phys. Fluids 2003, 15, 3795-3815.
26. Hlushkou, D., Seidel-Morgenstern, A., Tallarek, U., Langmuir 2005, 21, 6097-6112.
27. Freund, H., Bauer, J., Zeiser, T., Emig, G., Ind. Eng. Chem. Res. 2005, 44, 6423-6434.
28. Khirevich, S., Höltzel, A., Hlushkou, D., Tallarek, U., Anal. Chem. 2007, 79, 9340-9349.
29. Leva, M., Grummer, M., Chem. Eng. Prog. 1947, 43, 713-718.
30. Guiochon, G., Drumm, E., Cherrak, D., J. Chromatogr. A 1999, 835, 41-58.
31. Shalliker, R. A., Broyles, B. S., Guiochon, G., J. Chromatogr. A 2000, 888, 1-12.
32. Shalliker, R. A., Wong, V., Broyles, B. S., Guiochon, G., J. Chromatogr. A 2002, 977, 213-223.
33. Chen, G., Paces, M., Marek, M., Zhang, Y., Seidel-Morgenstern, A., Tallarek, U., Chem. Eng. Technol. 2004, 27, 417-428.
34. Vissers, J. P. C., Claessens, H. A., Laven, J., Cramers, C. A., Anal. Chem. 1995, 67, 2103-2109.
35. Tobis, J., Vortmeyer, D., Chem. Eng. Process. 1991, 29, 147-153.
36. Halász, I., Martin, K., Angew. Chem. Int. Ed. 1978, 17, 901-908.
37. Yau, W. W., Kirkland, J. J., Bly, D. D., Modern Size-Exclusion Liquid Chromatography, John Wiley & Sons, New York 1979.
38. Guan, H., Guiochon, G., J. Chromatogr. A 1996, 731, 27-40.
39. Carman, P.C., Trans. Inst. Chem. Eng. 1937, 15, 150-166.
40. Sonntag, G., Chem. Ing. Tech. 1960, 32, 317-329.
41. Yang, R.Y,, Zou, R. P., Yu, A.B., Phys. Rev. E 2000, 62, 3900-3908.
42. Gritti, F., Guiochon, G., J. Chromatogr. A 2007, 1166, 30-46.
43. Billen, J., Guillarme, D., Rudaz, S., Veuthey, J.-L., Ritchie, H., Grady, B., Desmet, G. J. Chromatogr. A 2007, 1161, 224-233.