Confocal laser scanning microscopy method for quantitative characterization of silica monolith morphology

Analytical Chemistry

Volumn 82, Issue 15, 2010, Pages 6569-6575

  Bruns, Stefan ^a   Müllner, Tibor ^a   Kollmann, Martin ^a   Schachtner, Joachim ^a   Höltzel, Alexandra ^a   Tallarek, Ulrich ^a  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

CAPILLARY COLUMNS; CHORD LENGTH DISTRIBUTION; CONFOCAL LASER SCANNING MICROSCOPY; CROSS SECTIONAL IMAGE; IMAGE DATA; MACRO PORES; MONOLITHIC COLUMNS; MORPHOLOGICAL DATA; MORPHOLOGICAL INFORMATION; NON DESTRUCTIVE; PRE-TREATMENT; QUANTITATIVE APPROACH; QUANTITATIVE CHARACTERIZATION; RAPID ACQUISITION; SILICA MONOLITHS; STATISTICAL ANALYSIS;

CONFOCAL MICROSCOPY; IMAGE PROCESSING; MORPHOLOGY; SILICA; TRANSMISSION ELECTRON MICROSCOPY;

SCANNING ELECTRON MICROSCOPY;

SILICON DIOXIDE;

CHEMISTRY; CONFERENCE PAPER; CONFOCAL MICROSCOPY; IMAGE PROCESSING; METHODOLOGY;

IMAGE PROCESSING, COMPUTER-ASSISTED; MICROSCOPY, CONFOCAL; SILICON DIOXIDE;

EID: 77955132927     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac100909t     Document Type: Conference Paper

References (67)

1. Svec, F. J. Chromatogr., A 2010, 1217, 902-924
2. Bakry, R., Huck, C. W., and Bonn, G. K. J. Chromatogr. Sci. 2009, 47, 418-431
3. Nordborg, A. and Hilder, E. F. Anal. Bioanal. Chem. 2009, 394, 71-84
4. Vlakh, E. G. and Tennikova, T. B. J. Chromatogr., A 2009, 1216, 2637-2650
5. Urban, J. and Jandera, P. J. Sep. Sci. 2008, 31, 2521-2540
6. Jungbauer, A. and Hahn, R. J. Chromatogr., A 2008, 1184, 62-79
7. Wu, R., Hu, L., Wang, F., Ye, M., and Zou, H. J. Chromatogr., A 2008, 1184, 369-392
8. Nez, O., Nakanishi, K., and Tanaka, N. J. Chromatogr., A 2008, 1191, 231-252
9. Potter, O. G. and Hilder, E. F. J. Sep. Sci. 2008, 31, 1881-1906
10. Szumski, M. and Buszewski, B. J. Sep. Sci. 2007, 30, 55-66
11. Eeltink, S. and Svec, F. Electrophoresis 2007, 28, 137-147
12. Schaller, D., Hilder, E. F., and Haddad, P. R. J. Chromatogr. Sci. 2006, 29, 1705-1719
13. Maruška, A. and Kornysova, O. J. Chromatogr., A 2006, 1112, 319-330
14. Rieux, L., Niederländer, H., Verpoorte, E., and Bischoff, R. J. Sep. Sci. 2005, 28, 1628-1641
15. Cabrera, K. J. Sep. Sci. 2004, 27, 843-852
16. Guiochon, G. J. Chromatogr., A 2007, 1168, 101-168
17. Unger, K. K., Skudas, R., and Schulte, M. M. J. Chromatogr., A 2008, 1184, 393-415
18. Hlushkou, D., Bruns, S., and Tallarek, U. J. Chromatogr., A 2010, 1217, 3674-3682
19. Nakanishi, K., Minakuchi, H., Soga, N., and Tanaka, N. J. Sol.-Gel Sci. Technol. 1997, 8, 547-552
20. Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., and Tanaka, N. J. Chromatogr., A 1997, 762, 135-146
21. Nakanishi, K. J. Porous Mater. 1997, 4, 67-112
22. Ishizuka, N., Minakuchi, H., Nakanishi, K., Soga, N., and Tanaka, N. J. Chromatogr., A 1998, 797, 133-137
23. Nakanishi, K. and Tanaka, N. Acc. Chem. Res. 2007, 40, 863-873
24. Liapis, A. I., Meyers, J. J., and Crosser, O. K. J. Chromatogr., A 1999, 865, 13-25
25. Leinweber, F. C., Lubda, D., Cabrera, K., and Tallarek, U. Anal. Chem. 2002, 74, 2470-2477
26. Vervoort, N., Gzil, P., Baron, G. V., and Desmet, G. Anal. Chem. 2003, 75, 843-850
27. Leinweber, F. C. and Tallarek, U. J. Chromatogr., A 2003, 1006, 207-228
28. Skudas, R., Grimes, B. A., Thommes, M., and Unger, K. K. J. Chromatogr., A 2009, 1216, 2625-2636
29. Grimes, B. A., Skudas, R., Unger, K. K., and Lubda, D. J. Chromatogr., A 2007, 1144, 14-29
30. Babin, J., Iapichella, J., Lefèvre, B., Biolley, C., Bellat, J., Fajula, F., and Galarneau, A. New J. Chem. 2007, 31, 1907-1917
31. Lubda, D., Lindner, W., Quaglia, M., du Fresne von Hohenesche, C., and Unger, K. K. J. Chromatogr., A 2005, 1083, 14-22
32. Al-Bokari, M., Cherrak, D., and Guiochon, G. J. Chromatogr., A 2002, 975, 275-284
33. Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., and Tanaka, N. J. Chromatogr., A 1998, 797, 121-131
34. Courtois, J., Szumski, M., Georgsson, F., and Irgum, K. Anal. Chem. 2007, 79, 335-344
35. Motokawa, M., Ohira, M., Minakuchi, H., Nakanishi, K., and Tanaka, N. J. Sep. Sci. 2006, 29, 2471-2477
36. Saito, H., Kanamori, K., Nakanishi, K., Hirao, K., Nishikawa, Y., and Jinnai, H. Colloids Surf., A 2007, 300, 245-252
37. Saito, H., Nakanishi, K., Hirao, K., and Jinnai, H. J. Chromatogr., A 2006, 1119, 95-104
38. Saito, H., Kanamori, K., Nakanishi, K., Hirao, K., Nishikawa, Y., and Jinnai, H. Colloids Surf., A 2004, 241, 215-224
39. Jinnai, H., Watashiba, H., Kajihara, T., and Takahashi, M. J. Chem. Phys. 2003, 119, 7554-7559
40. Kanamori, K., Nakanishi, K., Hirao, K., and Jinnai, H. Langmuir 2003, 19, 5581-5585
41. Jinnai, H., Nakanishi, K., Nishikawa, Y., Yamanaka, J., and Hashimoto, T. Langmuir 2001, 17, 619-625
42. Jinnai, H., Nishikawa, Y., Morimoto, H., Koga, T., and Hashimoto, T. Langmuir 2000, 16, 4380-4393
43. Torquato, S. Random Heterogeneous Materials - Microstructure and Macroscopic Properties; Springer Science & Business Media, LLC: New York, 2002.
44. Smarsly, B., Antonietti, M., and Wolff, T. J. Chem. Phys. 2002, 116, 2618-2626
45. Gille, W., Enke, D., and Janowski, F. J. Porous Mater. 2002, 9, 221-230
46. Gille, W. Eur. Phys. J. B 2000, 17, 371-383
47. Rulf, A., Worlitschek, J., and Mazzotti, M. Part. Part. Syst. Charact. 2000, 17, 167-179
48. Abrams, B., Diwu, Z., Guryev, O., Aleshkov, S., Hingorani, R., Edinger, M., Lee, R., Link, J., and Dubrovsky, T. Anal. Biochem. 2009, 386, 262-269
49. El Kadib, A., Chimenton, R., Sachse, A., Fajula, F., Galarneau, A., and Coq, B. Angew. Chem., Int. Ed. 2009, 48, 4969-4972
50. Rasband, W. S. ImageJ; U.S. National Institutes of Health: Bethesda, MD, 1997, - 2006; http://rsb.info.nih.gov//ij/.
51. Wilhelm, S., Gröbler, B., Gluch, M., and Heinz, H. Confocal Laser Scanning Microscopy - Optical Image Formation and Electronic Signal Processing; Monography, Carl Zeiss: Jena, Germany, 2008.
52. "Nyquist Rate and PSF Calculator", Scientific Volume Imaging Support Wiki Pages, http://www.svi.nl/NyquistCalculator (Accessed June 2010).
53. Abia, J. A., Mriziq, K. S., and Guiochon, G. A. J. Chromatogr., A 2009, 1216, 3185-3191
54. Abia, J. A., Mriziq, K. S., and Guiochon, G. A. J. Sep. Sci. 2009, 32, 923-930
55. Tanaka, N., Kobayashi, H., Ishizuka, N., Minakuchi, H., Nakanishi, K., Hosoya, K., and Ikegami, T. J. Chromatogr., A 2002, 965, 35-49
56. Kanamori, K., Yonezawa, H., Nakanishi, K., Hirao, K., and Jinnai, H. J. Sep. Sci. 2004, 27, 874-886
57. Schrader, M., Hell, S., and van der Voort, H. T. M. Appl. Phys. Lett. 1996, 69, 3644-3646
58. Bruns, S. Dreidimensionale Rekonstruktion monolithischer Festphasen mittels konfokaler Lasermikroskopie. Diplomarbeit, Fachbereich Chemie, Philipps-Universität, Marburg, Germany, 2009.
59. Levitz, P. and Tchoubar, D. J. Phys. I 1992, 2, 771-790
60. Gille, W., Enke, D., and Janowski, F. J. Porous Mater. 2001, 8, 179-191
61. Abell, A. B., Willis, K. L., and Lange, D. A. J. Colloid Interface Sci. 1999, 211, 39-44
62. Hara, T., Makino, S., Watanabe, Y., Ikegami, T., Cabrera, K., Smarsly, B., and Tanaka, N. J. Chromatogr., A 2010, 1217, 89-98
63. Tallarek, U., Rapp, E., Scheenen, T., Bayer, E., and Van As, H. Anal. Chem. 2000, 72, 2292-2301
64. Tallarek, U., Rapp, E., Seidel-Morgenstern, A., and Van As, H. J. Phys. Chem. B 2002, 106, 12709-12721
65. Gillespie, E., Connolly, D., Macka, M., Nesterenko, P. N., and Paull, B. Analyst 2007, 132, 1238-1245
66. Connolly, D., Barron, L. P., Gillespie, E., and Paull, B. Chromatographia 2009, 70, 915-920
67. Khirevich, S., Höltzel, A., Seidel-Morgenstern, A., and Tallarek, U. Anal. Chem. 2009, 81, 7057-7066