One-step column chromatographic extraction with gradient elution followed by automatic separation of volatiles, flavonoids and polysaccharides from Citrus grandis

Food Chemistry

Volumn 145, Issue , 2014, Pages 542-548

  Han, Han Bing ^a,b   Li, Hui ^b   Hao, Rui Lin ^b   Chen, Ya Fei ^b   Ni, He ^b   Li, Hai Hang ^b  

^a GUANGDONG UNIVERSITY OF PETROCHEMICAL TECHNOLOGY   (China)

^b SOUTH CHINA NORMAL UNIVERSITY   (China)

Author keywords

Chinese medicine; Citrus grandis; Column chromatographic extraction; Flavonoids; Gradient elution; Health food; Polysaccharides; Tomentosa; Traditional; Volatiles

Indexed keywords

CHINESE MEDICINES; CITRUS GRANDIS; GRADIENT ELUTION; HEALTH FOODS; TOMENTOSA; TRADITIONAL; VOLATILES;

CHROMATOGRAPHY; ETHANOL; ETHERS; EXTRACTION; FLAVONOIDS; MEDICINE;

POLYSACCHARIDES;

AURANTIIN; FLAVONOID; LIMONENE; POLYSACCHARIDE; VOLATILE AGENT; CYCLOHEXENE DERIVATIVE; PLANT EXTRACT; TERPENE; VOLATILE ORGANIC COMPOUND;

ARTICLE; COLUMN CHROMATOGRAPHY; ELUTION; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PARTICLE SIZE; PRECIPITATION; PUMMELO; CHEMISTRY; CHROMATOGRAPHY; CITRUS; FOOD ANALYSIS; PROCEDURES;

CITRUS MAXIMA;

CHROMATOGRAPHY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CITRUS; CYCLOHEXENES; FLAVONOIDS; FOOD ANALYSIS; PLANT EXTRACTS; POLYSACCHARIDES; TERPENES; VOLATILE ORGANIC COMPOUNDS;

EID: 84884185242     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2013.08.092     Document Type: Article

References (29)

1. M. Asamoto, H. Toriyama-Baba, T. Ohnishi, T. Ota, A. Naito, and A. Ando Mammary carcinomas induced in human c-Ha-ras proto-oncogene transgenic rats are estrogen-independent, but responsive to d-limonene treatment Japan Journal of Cancer Research 93 2002 32 35
2. H.F. Chen, X.F. Li, and H. Higashino Study on the chemistry and in vitro antioxidant activity of water soluble polysaccharides from Citrus grandis Chemical World 2 2002 91 93
3. Y.G. Chen, L. Lin, Y.H. Wei, F.X. Xiao, and X.H. Cui Comparison of ultrasonic extraction and Soxhlet extraction on the content determination of naringin in Citrus grandis Traditional Chinese Drug Research & Clinical Pharmacology 19 2008 309 311
4. H. Cheng, C. Cai, and X. Li Studies on isolation and composition of polysaccharide of Exocarpium citri grandis by GC Journal of Guangdong Medical College 16 1998 15 16
5. China Pharmacopoeia Committee China pharmacopoeia 2010 People's Medical Publishing House Ltd. Beijing
6. H.B. Dong, M.S. Jian, and W.J. Zhu Immunomodulatory effects of polysaccharides from Citrus grandis on mice Chinese Traditional Patent Medicine 30 2010 491 493
7. K. Hosni, N. Zahed, R. Chrif, I. Abid, W. Medfei, and M. Kallel Composition of peel essential oils from four selected Tunisian Citrus species: Evidence for the genotypic influence Food Chemistry 123 2010 1098 1104
8. X. Hou, Y. Shen, M. Xu, S. Wu, and W. Wang Extraction, purification and antioxidant activity of polysaccharide from exocarpium citri grandis China Brewing 31 2012 135 138
9. H.-D. Jang, K.-S. Chang, T.-C. Chang, and C.-L. Hsu Antioxidant potentials of buntan pumelo (Citrus grandis Osbeck) and its ethanolic and acetified fermentation products Food Chemistry 118 2010 554 558
10. J. Jung, M.K. Lee, and K.S. Jeong The hypoglycemic effects of hesperidin and naringin are partly mediated by hepatic glucose-regulating enzymes in C57BL.KsJ-db/db mice Journal of Nutrition 134 2004 2499 2503
11. G.-N. Kim, J.-G. Shin, and D.-D. Jang Antioxidant and antidiabetic activity of Dangyuja (Citrus grandis Osbeck) extract treated with Aspergillus saitoi Food Chemistry 117 2009 35 41
12. P.B. Li, Y. Ma, H.L. Yang, X. Jia, Y.G. Wang, and W.W. Su Anti-inflammatory effects of extracts from Citrus grandis (L.) Osbeck var. tomentosa Hort Chinese Traditional and Herbal Drugs 37 2006 251 253
13. H.-K. Lim, J.Y. Moon, H. Kim, M. Cho, and S.K. Cho Induction of apoptosis in U937 human leukaemia cells by the hexane fraction of an extract of immature Citrus grandis Osbeck fruits Food Chemistry 114 2009 1245 1250
14. C. Ma, and M.S. Jian Optimization of the extraction process of polysaccharides from Citrus grandis Chinese Journal of Ethnomedicine and Ethnopharmacy 10 2009 10
15. Q. Mu, and X.M. Ruan Study on the extraction of volatile oil distilled from Herba pogostemonis and Exocarpium Citri Rubrum Chinese Journal of Hospital Pharmacy 30 2010 1075 1077
16. H. Ni, X.H. Zhou, H.H. Li, and W.F. Huang Column chromatographic extraction and preparation of cordycepin from Cordyceps militaris waster medium Journal of Chromatography B 877 2009 2135 2141
17. S.M. Njoroge, H. Koaze, P.N. Karanja, and M. Sawamura Volatile constituents of redblush grapefruit (Citrus paradisi) and pummelo (Citrus gradis) peel essential oils from Kenya Journal of Agricultural and Food Chemistry 53 2005 9790 9794
18. A. Raasmaja, A. Lecklin, X.M. Li, J. Zou, G.-G. Zhu, and I. Laakso A water-alcohol extract of Citrus grandis whole fruits has beneficial metabolic effects in the obese Zucker rats fed with high fat/high cholesterol diet Food Chemistry 138 2013 1392 1399
19. D. Singh The effect of naringin, a bioflavonoid on ischemia-reperfusion induced renal injury in rats Pharmacological Research 50 2004 187 193
20. K. Sudto, S. Pornpakakul, and S. Wanichwecharungruang An efficient method for the large scale isolation of naringin from pomelo (Citrus grandis) peel International Journal of Food Science & Technology 44 2009 1737 1742
21. Y.-C. Wang, Y.-C. Chuang, and H.-W. Hsu The flavonoid, carotenoid and pectin content in peels of citrus cultivated in Taiwan Food Chemistry 106 2008 277 284
22. L. Wang, L.H. Gong, C.J. Chen, H.B. Han, and H.H. Li Column chromatographic extraction and separation of polyphenols, caffeine and theanine from green tea Food Chemistry 131 2012 1539 1545
23. Y. Wang, L. Yi, Y. Liang, H. Li, D. Yuan, and H. Gao Comparative analysis of essential oil components in Pericarpium Citri Reticulatae Viride and Pericarpium Citri Reticulatae by GC-MS combined with chemometric resolution method Journal of Pharmaceutical and Biomedical Analysis 46 2008 66 74
24. M. Wei, Z.L. Yang, and J.M. Wu Separation and purification of naringin from Citrus grandis Tomentosa by macroporous adsorption resin Chinese Traditional Patent Medicine 29 2007 352 354
25. H. Wu, Y.G. Shen, Z.P. Cai, and S.W. Fan Analysis on chemical constituents of essential oil from Citri Grandis by GC-MS Farm Products Processing 2011 2011 90 91
26. L. Yu, X. Li, S. Liu, G. Xu, and Y. Liang Comparative analysis of volatile constituents in Citrus reticulata Blanco using GC-MS and alternative moving window factor analysis Journal of Separation Science 32 2009 3457 3465
27. M. Zhang, C. Duan, Y. Zang, Z. Huang, and G. Liu The flavonoid composition of flavedo and juice from the pummelo cultivar (Citrus grandis (L.) Osbeck) and the grapefruit cultivar (Citrus paradisi) from China Food Chemistry 129 2011 1530 1536
28. J. Zhang, C. Sun, Y. Yan, Q. Chen, F. Luo, and X. Zhu Purification of naringin and neohesperidin from Huyou (Citrus changshanensis) fruit and their effects on glucose consumption in human HepG2 cells Food Chemistry 135 2012 1471 1478
29. B.W. Zhou, W.Y. Hu, and J.J. Wu Study on the pharmaceutical functions of polysaccharides from Citrus grandis or C. grandis var tomentosa Chinese Pharmaceutical Journal 28 1993 135 136