A rapid and highly sensitive UPLC-MS/MS method using pre-column derivatization with 2-picolylamine for intravenous and percutaneous pharmacokinetics of valproic acid in rats

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 938, Issue , 2013, Pages 35-42

  Joo, Kyung Mi ^a   Choi, Dalwoong ^b   Park, Yang Hui ^a   Yi, Chang Geun ^a   Jeong, Hye Jin ^a   Cho, Jun Cheol ^a   Lim, Kyung Min ^c  

^a AmorePacific Corporation   (South Korea)

^b Korea University   (South Korea)

^c Ewha Womans University   (South Korea)

Author keywords

2 Picolylamine; Derivatization; Pharmacokinetics; Topical application; UPLC MS MS; Valproic acid

Indexed keywords

2-PICOLYLAMINE; DERIVATIZATIONS; TOPICAL APPLICATION; UPLC-MS/MS; VALPROIC ACID;

LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

PHARMACOKINETICS;

2 PICOLYLAMINE; AMINE; AMMONIUM FORMATE; CARBOXYLIC ACID; FORMIC ACID; METHANOL; UNCLASSIFIED DRUG; VALPROIC ACID;

ACCURACY; ANIMAL EXPERIMENT; ANIMAL TISSUE; AREA UNDER THE CURVE; ARTICLE; CHROMATOGRAPHY; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; CORRELATION COEFFICIENT; DERIVATIZATION; DILUTION; DRUG STABILITY; ELECTROSPRAY MASS SPECTROMETRY; IN VIVO STUDY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID LIQUID EXTRACTION; MALE; NONHUMAN; PRIORITY JOURNAL; RAT; SENSITIVITY AND SPECIFICITY; SINGLE DRUG DOSE; TANDEM MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY;

2-PICOLYLAMINE; DERIVATIZATION; PHARMACOKINETICS; TOPICAL APPLICATION; UPLC-MS/MS; VALPROIC ACID;

ADMINISTRATION, INTRAVENOUS; ADMINISTRATION, TOPICAL; ANIMALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; LIMIT OF DETECTION; MALE; NONLINEAR DYNAMICS; RATS; RATS, SPRAGUE-DAWLEY; REPRODUCIBILITY OF RESULTS; TANDEM MASS SPECTROMETRY; VALPROIC ACID;

EID: 84884176634     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2013.08.022     Document Type: Article

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