-
1
-
-
67651244535
-
Gas chromatographic method for analysis of p-synephrine in Citrus aurantium L products
-
Andrade AS, Schmitt GC, Rossato LG, Russowsky D, Limberger RP. 2009. Gas chromatographic method for analysis of p-synephrine in Citrus aurantium L products. Chromatographia. 69:225-229.
-
(2009)
Chromatographia
, vol.69
, pp. 225-229
-
-
Andrade, A.S.1
Schmitt, G.C.2
Rossato, L.G.3
Russowsky, D.4
Limberger, R.P.5
-
2
-
-
47149099720
-
Concentrations of p-synephrine in fruits and leaves of Citrus species (Rutaceae) and the acute toxicity testing of Citrus aurantium extract and p-synephrine
-
Arbo MD, Larentis ER, Linck VM, Aboy AL, Pimentel AL, Henriques AT, Dallegrave E, Garcia SC, Leal MB, Limberger RP. 2008. Concentrations of p-synephrine in fruits and leaves of Citrus species (Rutaceae) and the acute toxicity testing of Citrus aurantium extract and p-synephrine. Food Chem Toxicol. 46:2770-2775.
-
(2008)
Food Chem Toxicol
, vol.46
, pp. 2770-2775
-
-
Arbo, M.D.1
Larentis, E.R.2
Linck, V.M.3
Aboy, A.L.4
Pimentel, A.L.5
Henriques, A.T.6
Dallegrave, E.7
Garcia, S.C.8
Leal, M.B.9
Limberger, R.P.10
-
3
-
-
66049159732
-
Subchronic toxicity of Citrus aurantium L. (Rutaceae) extract and p-synephrine in mice
-
Arbo MD, Schmitt GC, Limberger MF, Charão MF, Moro AM, Ribeiro GL, Dallegrave E, Garcia SC, Leal MB, Limberger RP. 2009. Subchronic toxicity of Citrus aurantium L. (Rutaceae) extract and p-synephrine in mice. Regul Toxicol Pharmac. 54:114-117.
-
(2009)
Regul Toxicol Pharmac
, vol.54
, pp. 114-117
-
-
Arbo, M.D.1
Schmitt, G.C.2
Limberger, M.F.3
Charão, M.F.4
Moro, A.M.5
Ribeiro, G.L.6
Dallegrave, E.7
Garcia, S.C.8
Leal, M.B.9
Limberger, R.P.10
-
4
-
-
1042279493
-
Separation and determination of ephedrine enantiomers and synephrine by high performancecapillary electrophoresis in dietary supplements
-
Avula B, Khan IA. 2004. Separation and determination of ephedrine enantiomers and synephrine by high performancecapillary electrophoresis in dietary supplements. Chromatographia. 59:71-77.
-
(2004)
Chromatographia
, vol.59
, pp. 71-77
-
-
Avula, B.1
Khan, I.A.2
-
5
-
-
23844546561
-
Enantiomeric Separation of Adrenergic Amines in Citrus Species, Related Genera and Dietary Supplements by Capillary Electrophoresis
-
Avula B, Upparapalli SK, Khan IA. 2005. Enantiomeric Separation of Adrenergic Amines in Citrus Species, Related Genera and Dietary Supplements by Capillary Electrophoresis. Chromatographia. 62:151-157.
-
(2005)
Chromatographia
, vol.62
, pp. 151-157
-
-
Avula, B.1
Upparapalli, S.K.2
Khan, I.A.3
-
6
-
-
30644471164
-
Simultaneous quantification of adrenergic amines and flavonoids in C. aurantium, various Citrus species, and dietary supplements by liquid chromatography
-
Avula B, Upparapalli SK, Navarrete A, Khan IA. 2005. Simultaneous quantification of adrenergic amines and flavonoids in C. aurantium, various Citrus species, and dietary supplements by liquid chromatography. J AOAC Int. 88:1593-1606.
-
(2005)
J AOAC Int
, vol.88
, pp. 1593-1606
-
-
Avula, B.1
Upparapalli, S.K.2
Navarrete, A.3
Khan, I.A.4
-
7
-
-
78650895544
-
Presence of synthetic pharmaceuticals as adulterants in slimming phytotherapeutic formulations and their analytical determination
-
Carvalho LM, Martini M, Moreira APL, Lima APS, Correia D, Falcão T, Garcia SC, Bairros AV, Nascimento PC, Bohrer D. 2011. Presence of synthetic pharmaceuticals as adulterants in slimming phytotherapeutic formulations and their analytical determination. Forensic Sci Int. 204:6-12.
-
(2011)
Forensic Sci Int
, vol.204
, pp. 6-12
-
-
Carvalho, L.M.1
Martini, M.2
Moreira, A.P.L.3
Lima, A.P.S.4
Correia, D.5
Falcão, T.6
Garcia, S.C.7
Bairros, A.V.8
Nascimento, P.C.9
Bohrer, D.10
-
8
-
-
4444253164
-
Citrus aurantium, an ingredient of dietary supplements marketed for weight loss: current status of clinical and basic research
-
Fugh-Berman A, Myers A. 2004. Citrus aurantium, an ingredient of dietary supplements marketed for weight loss: current status of clinical and basic research. Experim Biol Med. 229:698-704.
-
(2004)
Experim Biol Med
, vol.229
, pp. 698-704
-
-
Fugh-Berman, A.1
Myers, A.2
-
9
-
-
18844439179
-
Simultaneous determination of Ephedra sinica and Citrus aurantium var. amara alkaloids by ion-pair chromatography
-
Ganzera M, Lanser C, Stuppner H. 2005. Simultaneous determination of Ephedra sinica and Citrus aurantium var. amara alkaloids by ion-pair chromatography. Talanta. 66:889-894.
-
(2005)
Talanta
, vol.66
, pp. 889-894
-
-
Ganzera, M.1
Lanser, C.2
Stuppner, H.3
-
10
-
-
84855349487
-
Determination of octopamine and tyramine traces in dietary supplements and phytoextracts by high performance liquid chromatography after derivatization with 2,5-dimethyl-1H-pyrrole-3,4-dicarbaldehyde
-
Gatti R, Lotti C, Morigi R, Andreani A. 2012. Determination of octopamine and tyramine traces in dietary supplements and phytoextracts by high performance liquid chromatography after derivatization with 2,5-dimethyl-1H-pyrrole-3,4-dicarbaldehyde. J Chrom A. 1220:92-100.
-
(2012)
J Chrom A
, vol.1220
, pp. 92-100
-
-
Gatti, R.1
Lotti, C.2
Morigi, R.3
Andreani, A.4
-
11
-
-
33644559665
-
An isotopically labeled internal standard liquid chromatography-Tandem mass spectrometry method for determination of ephedrine alkaloids and synephrine in dietary supplements
-
Gay ML, Niemann RA, Musser SM. 2006. An isotopically labeled internal standard liquid chromatography-Tandem mass spectrometry method for determination of ephedrine alkaloids and synephrine in dietary supplements. J Agric Food Chem. 54:285-291.
-
(2006)
J Agric Food Chem
, vol.54
, pp. 285-291
-
-
Gay, M.L.1
Niemann, R.A.2
Musser, S.M.3
-
12
-
-
1842687888
-
Enhanced stimulant and metabolic effects of combined ephedrine and caffeine
-
Haller CA, Jacob P, Benowitz NL. 2004. Enhanced stimulant and metabolic effects of combined ephedrine and caffeine. Cl Pharmacol Therap. 75:259-273.
-
(2004)
Cl Pharmacol Therap
, vol.75
, pp. 259-273
-
-
Haller, C.A.1
Jacob, P.2
Benowitz, N.L.3
-
13
-
-
0026697925
-
Determination of synephrine from Chinese medicinal drugs originating from citrus
-
Hashimoto K, Yasuda T, Ohsawa K. 1992. Determination of synephrine from Chinese medicinal drugs originating from citrus. J. Chromatogr. 623:386-389.
-
(1992)
J. Chromatogr
, vol.623
, pp. 386-389
-
-
Hashimoto, K.1
Yasuda, T.2
Ohsawa, K.3
-
14
-
-
0031565878
-
High-performance liquid chromatography-electrospray mass spectrometry in phytochemical analysis of sour orange (Citrus aurantium L)
-
He X, Lian L, Lin L, Bernart MW. 1997. High-performance liquid chromatography-electrospray mass spectrometry in phytochemical analysis of sour orange (Citrus aurantium L). J Chromatogr A. 791:127-134.
-
(1997)
J Chromatogr A
, vol.791
, pp. 127-134
-
-
He, X.1
Lian, L.2
Lin, L.3
Bernart, M.W.4
-
15
-
-
84892437892
-
-
Health Canada - Natural Health Products Directorate. 2011. Synephrine, octopamine and caffeine health risk assessment report [Internet]. [cited 2013 Jan 22]. Available from: http://www.nutratechinc.com/advz/Studies2011/Safety/S1%20Health%20Canada%200511.pdf
-
(2011)
Health Canada - Natural Health Products Directorate
-
-
-
17
-
-
84880926744
-
-
International Conference on Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use, ICH Steering Committee
-
International Conference on Harmonization of Technical Requirements for Registration of Pharmaceuticals for Human Use, ICH Steering Committee. 1996. Validation of analytical procedures: methodology [Internet]. Geneva, Switzerland: ICH. [cited 2013 Mar 13]. Available from: http://www.ich.org/fileadmin/Public_Web_Site/ICH_Products/Guidelines/Quality/Q2_R1/Step4/Q2_R1__Guideline.pdf
-
(1996)
Validation of analytical procedures: Methodology
-
-
-
18
-
-
84892433062
-
-
Italia. 2002. Circolare n.3, 18 luglio. Applicazione della procedura di notifica di etichetta di cui all'art. 7 del Decreto legislativo n.111/1992, ai prodotti a base di piante e derivati aventi finalità salutistiche. Gazzetta Ufficiale n. 188, 12 agosto 2002. [Internet]; Available from: http://www.frascati.enea.it/spp/legislazione/Igiene_alimenti/MS_C_3_02.pdf
-
(2002)
Italia
-
-
-
19
-
-
0027058967
-
Determination of synephrine and N-methyltyramine in Zhishi and Zhike (immature citrus fruits) by high-performance liquid chromatography with electrochemical detection
-
Kusu F, Li XD, Takamura K. 1992. Determination of synephrine and N-methyltyramine in Zhishi and Zhike (immature citrus fruits) by high-performance liquid chromatography with electrochemical detection. Chem Pharm Bull. 40:3284-3286.
-
(1992)
Chem Pharm Bull
, vol.40
, pp. 3284-3286
-
-
Kusu, F.1
Li, X.D.2
Takamura, K.3
-
20
-
-
0029866654
-
Determination ofsynephrine enantiomers in food and conjugated synephrine in urine by high-performance liquid chromatography with electrochemical detection
-
Kusu F, Matsumoto K, Arai K, Takamura K. 1996. Determination ofsynephrine enantiomers in food and conjugated synephrine in urine by high-performance liquid chromatography with electrochemical detection. Anal Biochem. 235:191-194.
-
(1996)
Anal Biochem
, vol.235
, pp. 191-194
-
-
Kusu, F.1
Matsumoto, K.2
Arai, K.3
Takamura, K.4
-
21
-
-
0029094693
-
Direct speciation and determination of synephrine enantiomers by high-performance liquid chromatography with electrochemical detection
-
Kusu F, Matsumoto K, Takamura K. 1995. Direct speciation and determination of synephrine enantiomers by high-performance liquid chromatography with electrochemical detection. Chem Pharm Bull. 43:1158-1161.
-
(1995)
Chem Pharm Bull
, vol.43
, pp. 1158-1161
-
-
Kusu, F.1
Matsumoto, K.2
Takamura, K.3
-
22
-
-
33646832547
-
A rapid and simple procedure for determination of synephrine in dietary supplements by gas chromatography-mass spectrometry
-
Marchei E, Pichini S, Pacifici R, Pellegrini M, Zuccaro P. 2006. A rapid and simple procedure for determination of synephrine in dietary supplements by gas chromatography-mass spectrometry. J Pharm Biomed Anal. 41:1468-1472.
-
(2006)
J Pharm Biomed Anal
, vol.41
, pp. 1468-1472
-
-
Marchei, E.1
Pichini, S.2
Pacifici, R.3
Pellegrini, M.4
Zuccaro, P.5
-
23
-
-
30544449361
-
A rapid liquid chromatography electrospray ionization mass spectrometryn method for evaluation of synephrine incitrus aurantium L. samples
-
Mattioli L, Cangi F, Maidecchi A, Ghiara C, Tubaro M, Traldi P. 2005. A rapid liquid chromatography electrospray ionization mass spectrometryn method for evaluation of synephrine incitrus aurantium L. samples. J Agric Food Chem. 53:9860-9866.
-
(2005)
J Agric Food Chem
, vol.53
, pp. 9860-9866
-
-
Mattioli, L.1
Cangi, F.2
Maidecchi, A.3
Ghiara, C.4
Tubaro, M.5
Traldi, P.6
-
24
-
-
0041833743
-
Determination of ephedrine alkaloids and synephrine in dietary supplements by column-switching cation exchange high-performance liquid chromatography with scanning-wavelength ultraviolet and fluorescence detection
-
Niemann RA, Gay ML. 2003. Determination of ephedrine alkaloids and synephrine in dietary supplements by column-switching cation exchange high-performance liquid chromatography with scanning-wavelength ultraviolet and fluorescence detection. J Agric Food Chem. 51:5630-5638.
-
(2003)
J Agric Food Chem
, vol.51
, pp. 5630-5638
-
-
Niemann, R.A.1
Gay, M.L.2
-
25
-
-
34447640514
-
Chromatographic and electrophoretic methods for the analysis of phenetylamine alkaloids in Citrus aurantium
-
Pellati F, Benvenutti S. 2007. Chromatographic and electrophoretic methods for the analysis of phenetylamine alkaloids in Citrus aurantium. J Chrom A. 1161:71-88.
-
(2007)
J Chrom A
, vol.1161
, pp. 71-88
-
-
Pellati, F.1
Benvenutti, S.2
-
26
-
-
0036681475
-
Determination of adrenergic agonists from extracts and herbal products of Citrus aurantium L. var. amara by LC
-
Pellati F, Benvenuti S, Melegari M, Firenzuoli F. 2002. Determination of adrenergic agonists from extracts and herbal products of Citrus aurantium L. var. amara by LC. J. Pharm Biomed Anal. 29:1113-1119.
-
(2002)
J. Pharm Biomed Anal
, vol.29
, pp. 1113-1119
-
-
Pellati, F.1
Benvenuti, S.2
Melegari, M.3
Firenzuoli, F.4
-
27
-
-
30444442837
-
Quantitative and qualitative analysis of flavonoid markers in Frucus aurantii of different geographical origin by capillary electrophoresis with electrochemical detection
-
Peng Y, Liu F, Ye J. 2006. Quantitative and qualitative analysis of flavonoid markers in Frucus aurantii of different geographical origin by capillary electrophoresis with electrochemical detection. J Chromatogr B. 830:224-230.
-
(2006)
J Chromatogr B
, vol.830
, pp. 224-230
-
-
Peng, Y.1
Liu, F.2
Ye, J.3
-
28
-
-
34249092949
-
Determination of synephrine in bitter orange raw materials, extracts, and dietary supplements by liquid chromatography with ultraviolet detection: single-laboratory validation
-
Roman MC, Betz JM, Hildreth J. 2007. Determination of synephrine in bitter orange raw materials, extracts, and dietary supplements by liquid chromatography with ultraviolet detection: single-laboratory validation. J AOAC Int. 90:68-81.
-
(2007)
J AOAC Int
, vol.90
, pp. 68-81
-
-
Roman, M.C.1
Betz, J.M.2
Hildreth, J.3
-
29
-
-
78650288647
-
Synephrine: from trace concentrations to massive consumption in weight-loss
-
Rossato LG, Costa VM, Limberger RP, Bastos ML, Remião F. 2011. Synephrine: from trace concentrations to massive consumption in weight-loss. Food Chem Toxicol. 49:8-16.
-
(2011)
Food Chem Toxicol
, vol.49
, pp. 8-16
-
-
Rossato, L.G.1
Costa, V.M.2
Limberger, R.P.3
Bastos, M.L.4
Remião, F.5
-
30
-
-
40849084967
-
Liquid chromatographic methods for the determination of para-synephrine and meta-synephrine positional isomers in bitterorange-containing dietary supplements
-
Santana J, Sharpless KE, Nelson BC. 2008. Liquid chromatographic methods for the determination of para-synephrine and meta-synephrine positional isomers in bitterorange-containing dietary supplements. Food Chem. 109:675-682.
-
(2008)
Food Chem
, vol.109
, pp. 675-682
-
-
Santana, J.1
Sharpless, K.E.2
Nelson, B.C.3
-
31
-
-
8744238294
-
Quantitative and qualitative HPLC analysis of thermogenic weight loss products
-
Schaneberg BT, Khan IA. 2004. Quantitative and qualitative HPLC analysis of thermogenic weight loss products. Pharmazie. 59:819-823.
-
(2004)
Pharmazie
, vol.59
, pp. 819-823
-
-
Schaneberg, B.T.1
Khan, I.A.2
-
32
-
-
84861914923
-
Toxicological effects of a mixture used in weight loss products: p-synephrine associated with ephedrine, salicin, and caffeine
-
Schmitt GC, Arbo MD, Lorensi AL, Maciel ES, Krahn CL, Mariotti KC, Dallegrave E, Leal MB, Limberger RP. 2012. Toxicological effects of a mixture used in weight loss products: p-synephrine associated with ephedrine, salicin, and caffeine. Int J Toxic. 31:184-191.
-
(2012)
Int J Toxic
, vol.31
, pp. 184-191
-
-
Schmitt, G.C.1
Arbo, M.D.2
Lorensi, A.L.3
Maciel, E.S.4
Krahn, C.L.5
Mariotti, K.C.6
Dallegrave, E.7
Leal, M.B.8
Limberger, R.P.9
-
33
-
-
34248656976
-
Determination of synephrine in weight-loss products using high performance liquid chromatography with acidic potassium permanganate chemiluminescence detection
-
Slezak T, Francis PS, Anastos N, Barnett NW. 2007. Determination of synephrine in weight-loss products using high performance liquid chromatography with acidic potassium permanganate chemiluminescence detection. Anal Chim Acta. 593:98-102.
-
(2007)
Anal Chim Acta
, vol.593
, pp. 98-102
-
-
Slezak, T.1
Francis, P.S.2
Anastos, N.3
Barnett, N.W.4
-
34
-
-
0023794680
-
Methylxanthines: toxicity to humans caffeine
-
Stavric B. 1988. Methylxanthines: toxicity to humans caffeine. Food Chem Toxicol. 26:645-662.
-
(1988)
Food Chem Toxicol
, vol.26
, pp. 645-662
-
-
Stavric, B.1
-
35
-
-
33746852014
-
Determination of octopamine, synephrine and tyramine in Citrus herbs by ionic liquid improved "green" chromatography
-
Tang F, Tao L, Luo X, Ding L, Guo M, Nie L, Yao S. 2006. Determination of octopamine, synephrine and tyramine in Citrus herbs by ionic liquid improved "green" chromatography. J. Chromatogr. A. 1125:182-188.
-
(2006)
J. Chromatogr. A
, vol.1125
, pp. 182-188
-
-
Tang, F.1
Tao, L.2
Luo, X.3
Ding, L.4
Guo, M.5
Nie, L.6
Yao, S.7
-
36
-
-
78650179346
-
Rapid simultaneous determination of amines and organic acids in citrus using high-performance liquid chromatography
-
Uckoo RM, Jayaprakasha GK, Nelson SD, Patil BS. 2011. Rapid simultaneous determination of amines and organic acids in citrus using high-performance liquid chromatography. Talanta. 83:948-954.
-
(2011)
Talanta
, vol.83
, pp. 948-954
-
-
Uckoo, R.M.1
Jayaprakasha, G.K.2
Nelson, S.D.3
Patil, B.S.4
-
37
-
-
84880927924
-
-
35th, Rockville,: United States Pharmacopeial Convention
-
The United States Pharmacopoeia Convention. 2011. 35th ed. Rockville: United States Pharmacopeial Convention; p. 2622-2625.
-
(2011)
The United States Pharmacopoeia Convention
, pp. 2622-2625
-
-
|