On-line solid phase extraction-high performance liquid chromatography-isotope dilution-tandem mass spectrometry approach to quantify N,N-diethyl-m-toluamide and oxidative metabolites in urine

Analytica Chimica Acta

Volumn 787, Issue , 2013, Pages 267-273

  Kuklenyik, Peter ^a   Baker, Samuel E ^a   Bishop, Amanda M ^a   Morales A, Pilar ^a   Calafat, Antonia M ^a  

^a NATIONAL CENTER FOR ENVIRONMENTAL HEALTH   (United States)

Author keywords

Column switching; DEET; HPLC; Mass spectrometry; N,N diethyl m toluamide; On line SPE

Indexed keywords

COLUMN SWITCHING; DEET; HPLC; N ,N-DIETHYL-M-TOLUAMIDE; ON-LINE SPE;

ATMOSPHERIC PRESSURE; BIOMOLECULES; CHROMATOGRAPHY; ENZYMATIC HYDROLYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOTOPES; MASS SPECTROMETRY; METABOLITES; ORGANIC POLYMERS; PHASE SEPARATION;

BODY FLUIDS;

3 (DIETHYLCARBAMOYL)BENZOIC ACID; BENZAMIDE DERIVATIVE; BENZOIC ACID DERIVATIVE; DIETHYLTOLUAMIDE; N,N DIETHYL 3 (HYDROXYMETHYL)BENZAMIDE; UNCLASSIFIED DRUG;

ACCURACY; ADULT; ARTICLE; AUTOMATION; BIOLOGICAL MONITORING; FEMALE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; HYDROLYSIS; IONIZATION; LIMIT OF DETECTION; MALE; OCCUPATIONAL EXPOSURE; ONLINE SOLID PHASE EXTRACTION HIGH PERFORMANCE LIQUID CHROMATOGRAPHY ISOTOPE DILUTION TANDEM MASS SPECTROMETRY; PRIORITY JOURNAL; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; URINALYSIS;

COLUMN SWITCHING; DEET; HPLC; MASS SPECTROMETRY; N,N-DIETHYL-M-TOLUAMIDE; ON-LINE SPE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DEET; FEMALE; HUMANS; MALE; OXIDATIVE STRESS; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

HEXAPODA;

EID: 84879879730     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2013.05.055     Document Type: Article

References (42)

1. U.S.E.P.A. Pesticides: Topical & Chemical Fact Sheets, The Insect Repellent DEET 2007, US EPA, United States.
2. C.D.C. Centers for Disease Control and Prevention, Fourth National Report on Human Exposure to Environmental Chemicals 2009, Atlanta, United States.
3. Snyder J.W., Poe R.O., Stubbins J.F., Garrettson L.K. J. Toxicol. - Clin. Toxicol. 1986, 24:429.
4. Chaney L.A., Rockhold R.W., Wineman R.W., Hume A.S. Toxicol. Sci. 1999, 49:306.
5. Sudakin D.L., Trevathan W.R. J. Toxicol. - Clin. Toxicol. 2003, 41:831.
6. Abou-Donia M.B., Wilmarth K.R., Abdel-Rahman A.A., Jensen K.F., Oehme F.W., Kurt T.L. Fundam. Appl. Toxicol. 1996, 34:201.
7. Abou-Donia M.B., Wilmarth K.R., Jensen K.F., Oehme F.W., Kurt T.L. J. Toxicol. Environ. Health 1996, 48:35.
8. McCain W.C., Lee R., Johnson M.S., Whaley J.E., Ferguson J.W., Beall P., Leach G. J. Toxicol. Environ. Health 1997, 50:113.
9. Abdel-Rahman A., Dechkovskaia A.M., Goldstein L.B., Bullman S.H., Khan W., El-Masry E.M., Abou-Donia M.B. J. Toxicol. Environ. Health. Part A 2004, 67:331.
10. Abou-Donia M.B., Goldstein L.B., Jones K.H., Abdel-Rahman A.A., Damodaran T.V., Dechkovskaia A.M., Bullman S.L., Amir B.E., Khan W.A. Toxicol. Sci. 2001, 60:305.
11. Corbel V., Stankiewicz M., Pennetier C., Fournier D., Stojan J., Girard E., Dimitrov M., Molgo J., Hougard J.M., Lapied B. BMC Biology 2009, 7:47.
12. Taylor W.G., Hall T.W., Vedres D.D. Drug Metab. Dispos. 1993, 21:133.
13. Usmani K.A., Rose R.L., Goldstein J.A., Taylor W.G., Brimfield A.A., Hodgson E. Drug Metab. Dispos. 2002, 30:289.
14. Constantino L., Iley J. Xenobiotica 1999, 29:409.
15. Selim S., Hartnagel R.E., Osimitz T.G., Gabriel K.L., Schoenig G.P. Fundam. Appl. Toxicol. 1995, 25:95.
16. Moody R.P., Benoit F.M., Riedel D., Ritter L. J. Toxicol. Environ. Health 1989, 26:137.
17. Wu A., Pearson M.L., Shekoski D.L., Soto R.J., Stewart R.D. J. High Resolut. Chromatogr. Chromatogr. Commun. 1979, 2:558. HRC CC.
18. Schoenig G.P., Hartnagel R.E., Osimitz T.G., Llanso S. Drug Metab. Dispos. 1996, 24:156.
19. Yeung J.M., Taylor W.G. Drug Metab. Dispos. 1988, 16:600.
20. Cherstniakova S.A., Garcia G.E., Strong J., Bi D., Weitz J., Roy M.J., Cantilena L.R. J. Anal. Toxicol. 2006, 30:21.
21. Taylor W.G. Drug Metab. Dispos. 1986, 14:532.
22. Taylor W.G., Spooner R.W. J. Agric. Food Chem. 1990, 38:1422.
23. Smallwood A.W., Debord K.E., Lowry L.K. J. Anal. Toxicol. 1992, 16:10.
24. Qiu H.C., Jun H.W. J. Pharm. Biomed. Anal. 1996, 15:241.
25. Abu-Qare A.W., Abou-Donia M.B. J. Chromatogr. B 2000, 749:171.
26. Abu-Qare A.W., Abou-Donia M.B. J. Pharm. Biomed. Anal. 2001, 26:291.
27. Abu-Qare A.W., Abou-Donia M.B. Fresenius J. Anal. Chem. 2001, 370:403.
28. Cherstniakova S., Garcia G., Strong J., Helbling N., Bi D., Roy M., Cantilena L.R. Clin. Pharmacol. Ther. 2003, 73:P27.
29. Olsson A.O., Baker S.E., Nguyen J.V., Romanoff L.C., Udunka S.O., Walker R.D., Flemmen K.L., Barr D.B. Anal. Chem. 2004, 76:2453.
30. Kasichayanula S., House J.D., Wang T., Gu X.C. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 2005, 822:271.
31. Quednow K., Puttmann W. Environ. Sci. Pollut. Res. Int. 2009, 16:630.
32. Kuklenyik Z., Calafat A.M., Barr J.R., Pirkle J.L. J. Separ. Sci. 2011, 34:3606.
33. Kuklenyik Z., Ye X., Needham L.L., Calafat A.M. J. Chromatogr. Sci. 2009, 47:12.
34. Ye X., Kuklenyik Z., Needham L.L., Calafat A.M. Anal. Bioanal. Chem. 2005, 383:638.
35. Ye X., Wong L.Y., Jia L.T., Needham L.L., Calafat A.M. Environ. Int. 2009, 35:1160.
36. Zhou X., Ye X., Calafat A.M. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 2012, 881-882:27.
37. Ye X., Kuklenyik Z., Needham L.L., Calafat A.M. Anal. Chem. 2005, 77:5407.
38. Silva M.J., Preau J.L., Needham L.L., Calafat A.M. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 2008, 873:180.
39. Ye X., Kuklenyik Z., Bishop A.M., Needham L.L., Calafat A.M. J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. 2006, 844:53.
40. Ye X., Tao L.J., Needham L.L., Calafat A.M. Talanta 2008, 76:865.
41. Taylor J.K. Quality Assurance of Chemical Measurements 1987, Lewis Publishers, Chelsea, MI.
42. Knepper T.P. Water Sci. Technol. 2004, 50:301.