Design of online solid phase extraction-liquid chromatography-tandem mass spectrometry (SPE-LC-MS/MS) hyphenated systems for quantitative analysis of small organic compounds in biological matrices

Journal of Separation Science

Volumn 34, Issue 24, 2011, Pages 3606-3618

  Kuklenyik, Zsuzsanna ^a   Calafat, Antonia M ^a   Barr, John R ^a   Pirkle, James L ^a  

^a NATIONAL CENTER FOR ENVIRONMENTAL HEALTH   (United States)

Author keywords

Atrazine; Bisphenol A; Mononucleotide; MS; Online SPE

Indexed keywords

ANALYTES; ANALYTICAL SEPARATIONS; ANION EXCHANGE; BIOLOGICAL MATRIXES; BISPHENOL A; CHROMATOGRAPHIC COLUMN; HIGH IONIC STRENGTH; HYPHENATED SYSTEMS; ION PAIRS; LC-MS/MS; MONONUCLEOTIDES; MS; NUCLEOTIDE TRIPHOSPHATES; ON-LINE SPE; PHENOLIC DERIVATIVE; PHYSICOCHEMICAL PROPERTY; PRE-CONCENTRATION; RESTRICTED ACCESS MEDIAS; REVERSED PHASE; SOLID-PHASE; SOLVENT SYSTEM; SPE-LC-MS; STRONG CATION EXCHANGES; TARGET ANALYTES; URINE MATRIX; WORK-FLOWS;

CHEMICAL ANALYSIS; DESIGN; HERBICIDES; ION EXCHANGE; IONIC STRENGTH; IONIZATION OF LIQUIDS; IONIZATION POTENTIAL; LIQUIDS; MASS SPECTROMETRY; ONLINE SYSTEMS; PHENOLS; SOLVENT EXTRACTION;

LIQUID CHROMATOGRAPHY;

4,4' ISOPROPYLIDENEDIPHENOL; ATRAZINE; NUCLEOTIDE DERIVATIVE; NUCLEOTIDE TRIPHOSPHATE DERIVATIVE; ORGANIC COMPOUND; PHENOL DERIVATIVE; SODIUM CHLORIDE; UNCLASSIFIED DRUG;

ARTICLE; CATION EXCHANGE; COMPUTER INTERFACE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; FLOW RATE; IONIZATION; LIQUID CHROMATOGRAPHY; ONLINE SYSTEM; PH; PRIORITY JOURNAL; PROTON TRANSPORT; QUALITY CONTROL; REACTION OPTIMIZATION; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; WORKFLOW;

CHROMATOGRAPHY, LIQUID; ORGANIC CHEMICALS; SOFTWARE; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 83455266609     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201100562     Document Type: Article

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