Combined (S)TEM-FIB insight into the influence of the preparation method on the final surface structure of a Co3O4/La-modified- CeO2 washcoated monolithic catalyst

Journal of Physical Chemistry C

Volumn 117, Issue 25, 2013, Pages 13028-13036

  Hernández Garrido, Juan C ^a   Gómez, Diana M ^a   Gaona, Diana ^a   Vidal, Hilario ^a   Gatica, José M ^a   Sanz, Oihane ^b   Rebled, José M ^c,d   Peiró, Francesca ^c   Calvino, José J ^a  

^a UNIVERSITY OF CÁDIZ   (Spain)

^b UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

^c UNIVERSITY OF BARCELONA   (Spain)

^d INSTITUT DE CIÈNCIA DE MATERIALS DE BARCELONA ICMAB CSIC   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

BACKSCATTERED ELECTRON IMAGES; CHARACTERIZATION TECHNIQUES; CHEMICAL CHARACTERIZATION; FOCUSED ION BEAM TECHNIQUE; SUBNANOMETER RESOLUTION; THE SCANNING ELECTRON MICROSCOPES (SEM); WELL-DEFINED STRUCTURES; X-RAY ENERGY DISPERSIVE SPECTROSCOPY;

AGGREGATES; CATALYSTS; COATINGS; CRYSTALLOGRAPHY; ENERGY DISPERSIVE SPECTROSCOPY; MONOLITHIC INTEGRATED CIRCUITS; POWDERS; SCANNING ELECTRON MICROSCOPY; SURFACE STRUCTURE; TRANSMISSION ELECTRON MICROSCOPY;

NANOCRYSTALLITES;

EID: 84879612645     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/jp400151y     Document Type: Article

References (21)

1. Avila, P.; Montes, M.; Miro, E. E. Monolithic Reactors for Environmental Applications-A Review on Preparation Technologies Chem. Eng. J. 2005, 109 (1-3) 11-36
2. Cybulski, A.; Moulijn, J. A. Monoliths in Heterogeneous Catalysis Catal. Rev. 1994, 36 (2) 179-270
3. Gandhi, H. S.; Graham, G. W.; McCabe, R. W. Automotive Exhaust Catalysis J. Catal. 2003, 216 (1-2) 433-442
4. 2-Based Oxides in the Three-Way Catalysis Catal. Today 1999, 50 (2) 285-298
5. Boger, T.; Heibel, A. K.; Sorensen, C. M. Monolithic Catalysts for the Chemical Industry Ind. Eng. Chem. Res. 2004, 43 (16) 4602-4611
6. Moulijn, J. A.; Kreutzer, M. T.; Nijhuis, T. A.; Kapteijn, F. Monolithic Catalysts and Reactors: High Precision with Low Energy Consumption Adv. Catal. 2011, 54, 249-327
7. Cybulski, A.; Moulijn, J. A. Structured Catalysts and Reactors; Taylor & Francis: London, 2005.
8. Plummer, H. K.; Baird, R. J.; Hammerle, R. H.; Adamczyk, A. A.; Pakko, J. D. Measurement of Automotive Catalyst Washcoat Loading Parameters by Microscopy Techniques Microsc. Microanal. 1999, 5 (4) 267-281
9. Gomes, O. F. M.; Zotin, F. M. Z.; Alcover-Neto, A.; Cardoso, M. J. B.; Paciornik, S. In Measurement of Automotive Catalyst Wahscoat through BSE, SEM-CL and Digital Image Analysis; MICROMAT, Florianopolis, Sociedade Brasileira de Pesquisas em Materiais: Florianopolis, 2006.
10. Gai, P. L.; Calvino, J. J. Electron Microscopy in the Catalysis of Alkane Oxidation Environ. Control Altern. Energy Sources 2005, 35, 465-504
11. Bell, A. T. The Impact of Nanoscience on Heterogeneous Catalysis Science 2003, 299 (5613) 1688-1691
12. Haswell, R.; McComb, D. W.; Smith, W. Preparation of Site-Specific Cross-Sections of Heterogeneous Catalysts Prepared by Focused Ion Beam Milling J. Microsc. (Oxford, U. K.) 2003, 211, 161-166
13. Giannuzzi, L. A.; Stevie, F. A. A Review of Focused Ion Beam Milling Techniques for TEM Specimen Preparation Micron 1999, 30 (3) 197-204
14. Giannuzzi, L. A.; Prenitzer, B. I.; Drown-MacDonald, J. L.; Brown, S. R.; Irwin, R. B.; Stevie, F. A.; Shofner, T. L. Advances in the FIB Lift-Out Technique for TEM Specimen Preparation: HREM Lattice Imaging Microstruct. Sci. 1999, 26, 249-253
15. Ziegler, C.; Thiele, S.; Zengerle, R. Direct Three-Dimensional Reconstruction of a Nanoporous Catalyst Layer for a Polymer Electrolyte Fuel Cell J. Power Sources 2011, 196 (4) 2094-2097
16. Schulenburg, H.; Schwanitz, B.; Linse, N.; Scherer, G. G.; Wokaun, A.; Krbanjevic, J.; Grothausmann, R.; Manke, I. 3D Imaging of Catalyst Support Corrosion in Polymer Electrolyte Fuel Cells J. Phys. Chem. C 2011, 115 (29) 14236-14243
17. Ozkaya, D.; Matthews, M.; Spratt, S.; Goodlet, G.; Ash, P.; Boyd, D. Site-Specific Characterisation of an Auto Catalyst Using EPMA, FIB and TEM/STEM J. Phys.: Conf. Ser. 2006, 26, 323-326
18. Li, J.; Malis, T.; Dionne, S. Recent Advances in FIB-TEM Specimen Preparation Techniques Mater. Charact. 2006, 57 (1) 64-70
19. Bernal, S.; Blanco, G.; El Amarti, A.; Cifredo, G.; Fitian, L.; Galtayries, A.; Martin, J.; Pintado, J. M. Surface Basicity of Ceria-Supported Lanthana. Influence of the Calcination Temperature Surf. Interface Anal. 2006, 38 (4) 229-233
20. Almeida, L. C.; Echave, F. J.; Sanz, O.; Centeno, M. A.; Odriozola, J. A.; Montes, M. Washcoating of Metallic Monoliths and Microchannel Reactors Stud. Surf. Sci. Catal. 2010, 175, 25-33
21. Langford, R. M.; Petford-Long, A. K. Preparation of Transmission Electron Microscopy Cross-Section Specimens Using Focused Ion Beam Milling J. Vac. Sci. Technol., A 2001, 19 (5) 2186-2193