Spectroscopic and chromatographic characterisation of a pentafluorophenylpropyl silica phase end-capped in supercritical carbon dioxide as a reaction solvent

Journal of Chromatography A

Volumn 1298, Issue , 2013, Pages 86-94

  Ashu Arrah, Benjamin A ^a   Glennon, Jeremy D ^a   Albert, Klaus ^b  

^a UNIVERSITY COLLEGE CORK   (Ireland)

^b UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

29Si and 13C CP MAS NMR investigation; HPLC characterisation; PFPP silica bonded stationary phase; Supercritical carbon dioxide (sc CO2) silanisation and end capping

Indexed keywords

CHROMATOGRAPHIC SEPARATIONS; CP/MAS NMR; HPLC CHARACTERISATION; PENTAFLUOROPHENYLPROPYL-SILICA; SILANISATION; SOLID STATE NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; STATIONARY PHASE; SUPERCRITICAL CARBON DIOXIDES;

COLUMN CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; LOADING; NAPHTHALENE; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SCANNING ELECTRON MICROSCOPY; SILICA; SILICON; SUPERCRITICAL FLUID EXTRACTION; THERMOGRAVIMETRIC ANALYSIS;

CARBON DIOXIDE;

3 [(PENTAFLUOROPHENYL)PROPYLDIMETHYLCHLOROSILANE]; ACETAMIDE DERIVATIVE; ALICYCLIC COMPOUND; BIS N,O TRIMETHYLSILYLACETAMIDE; CARBENE; CARBON; CHLOROTRIMETHYLSILANE; DIPROPYLPHTHALATE; HEXAMETHYLDISILAZANE; METHYL GROUP; NAPHTHALENE; PENTAFLUOROPHENYLPROPYL; PHTHALIC ACID DERIVATIVE; SILANE DERIVATIVE; SILANOL; SILICON DIOXIDE; SILOXANE; SOLVENT; SUPERCRITICAL CARBON DIOXIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL MODIFICATION; CHEMICAL REACTION; CHROMATOGRAPHY; CONTROLLED STUDY; ELEMENTAL MICROANALYSIS; END CAPPING REACTION; HYDROPHOBICITY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRESSURE; PRIORITY JOURNAL; SCANNING ELECTRON MICROSCOPY; SILANIZATION; SOLID STATE; SUPERCRITICAL FLUID; SURFACE PROPERTY; TEMPERATURE; THERMOGRAVIMETRY;

CARBON DIOXIDE; FLUOROBENZENES; MAGNETIC RESONANCE SPECTROSCOPY; PHENOLS; SILICON DIOXIDE; SOLVENTS;

EID: 84879161102     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.05.024     Document Type: Article

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