Preparation and characterization of bonded silica hydride intermediate from triethoxysilane and dimethylmethoxysilane using supercritical carbon dioxide and dioxane as reaction medium

Journal of Chromatography A

Volumn 1236, Issue , 2012, Pages 42-50

  Ashu Arrah, Benjamin A ^a   Glennon, Jeremy D ^a   Albert, Klaus ^b  

^a UNIVERSITY COLLEGE CORK   (Ireland)

^b UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

Bonding methodology; Chemical functionalization; Silica hydride (SiH); Supercritical CO 2 and dioxane; Surface coverage and conversion efficiency; Triethoxysilane (TES) and dimethylmethoxysilane (DMMS)

Indexed keywords

BET SURFACE AREA; BONDED SILICA; CHEMICAL FUNCTIONALIZATION; CROSS-LINKAGE; FOURIER TRANSFORM INFRARED; FUNCTIONALIZATIONS; LIGAND DENSITY; MODIFICATION EFFICIENCY; NMR ANALYSIS; POLYMERIC SURFACES; REACTION CONDITIONS; REACTION MEDIUM; REACTION SOLVENTS; SILANIZATIONS; SILANOLS; SILICA HYDRIDE; SILICA PORES; SOLID-STATE NMR SPECTROSCOPY; SUPERCRITICAL CARBON DIOXIDES; SUPERCRITICAL CO 2 AND DIOXANE; SURFACE COVERAGES; TRIETHOXYSILANE;

BONDING; CONVERSION EFFICIENCY; ETHERS; HYDRIDES; LIGANDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC SOLVENTS; POLYMETHYL METHACRYLATES; PURIFICATION; REACTION INTERMEDIATES; SILICA; SUPERCRITICAL FLUID EXTRACTION; THERMOGRAVIMETRIC ANALYSIS; TOLUENE;

CARBON DIOXIDE;

CARBON DIOXIDE; DIMETHYLMETHOXYSILANE; DIOXANE; ORGANIC SOLVENT; SILANE DERIVATIVE; SILICA HYDRIDE; SILICON DIOXIDE; SUPERCRITICAL CARBON DIOXIDE; TOLUENE; TRIETHOXYSILANE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL BINDING; CROSS LINKING; GREEN CHEMISTRY; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRESSURE; PRIORITY JOURNAL; PURIFICATION; REACTION TIME; SOLID STATE; SURFACE PROPERTY; TEMPERATURE; THERMOGRAVIMETRY;

CARBON DIOXIDE; DIOXANES; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; POROSITY; SILANES; SILICATES; SPECTROSCOPY, FOURIER TRANSFORM INFRARED; SURFACE PROPERTIES; THERMOGRAVIMETRY;

EID: 84859269835     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.02.054     Document Type: Article

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