Silica hydride intermediate for octadecylsilica and phenyl bonded phase preparation via heterogeneous hydrosilation in supercritical carbon dioxide

Journal of Chromatography A

Volumn 1218, Issue 15, 2011, Pages 1974-1982

  Scully, N M ^a   Ashu Arrah, B A ^a   Nagle, A P ^a   Omamogho, J O ^a   O'Sullivan, G P ^a   Friebolin, V ^b   Dietrich, B ^b   Albert, K ^b   Glennon, J D ^a  

^a UNIVERSITY COLLEGE CORK   (Ireland)

^b UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

Endcapping; Green chemistry; Hydrosilation; Silica hydride; Supercritical carbon dioxide; Supercritical functionalisation

Indexed keywords

END CAPPING; GREEN CHEMISTRY; HYDROSILATION; SILICA HYDRIDE; SUPER-CRITICAL; SUPERCRITICAL CARBON DIOXIDES;

CARBON DIOXIDE; CONVERSION EFFICIENCY; EFFLUENT TREATMENT; ETHERS; FREE RADICALS; HYDROSILYLATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC SOLVENTS; REACTION INTERMEDIATES; SILANES; SILICA; SILICON; SPECTRUM ANALYSIS; STYRENE; SUPERCRITICAL FLUIDS; TOLUENE;

SUPERCRITICAL FLUID EXTRACTION;

CARBON DIOXIDE; OCTADECENE; OCTADECYLSILICON DIOXIDE; ORGANIC SOLVENT; SILICA HYDRIDE; SILICON DIOXIDE; STYRENE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CHROMATOGRAPHY; DIFFERENTIAL SCANNING CALORIMETRY; DIFFUSE REFLECTANCE SPECTROSCOPY; HYDROSILATION; INFRARED SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE; PRESSURE; PRIORITY JOURNAL; SILANISATION; SPECTROSCOPY; TEMPERATURE; THERMOGRAVIMETRY; TIME;

CALORIMETRY, DIFFERENTIAL SCANNING; CARBON DIOXIDE; CARBON ISOTOPES; CHROMATOGRAPHY, SUPERCRITICAL FLUID; FREE RADICALS; GREEN CHEMISTRY TECHNOLOGY; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PHENOLS; SILICATES; SILICON; SILICON DIOXIDE; SPECTROSCOPY, FOURIER TRANSFORM INFRARED; TEMPERATURE;

EID: 79952818102     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.11.046     Document Type: Article

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