Preparation of a mercaptopropyl bonded silica intermediate in supercritical carbon dioxide: Synthesis, characterisation and chromatography of a quinine based chiral stationary phase

Journal of Chromatography A

Volumn 1156, Issue 1-2 SPEC. ISS., 2007, Pages 68-74

  Scully, Norma M ^a   O'Sullivan, Gerard P ^a   Healy, Liam O ^a   Glennon, Jeremy D ^a   Dietrich, Benjamin ^b   Albert, Klaus ^b  

^a UNIVERSITY COLLEGE CORK   (Ireland)

^b UNIVERSITY OF TÜBINGEN   (Germany)

Author keywords

Chiral stationary phase; Mercaptopropyl bonded silica; Supercritical carbon dioxide

Indexed keywords

CARBON DIOXIDE; CHIRALITY; CHROMATOGRAPHY; ELEMENTARY PARTICLES; FOURIER TRANSFORM INFRARED SPECTROSCOPY; POROUS SILICON; PRESSURE EFFECTS; SILICA; THERMAL EFFECTS;

CHIRAL STATIONARY PHASE; MERCAPTOPROPYL BONDED SILICA; REACTION TEMPERATURE; SUPERCRITICAL CARBON DIOXIDE;

SYNTHESIS (CHEMICAL);

CARBON 13; CARBON DIOXIDE; FREE RADICAL; ORGANIC SOLVENT; QUININE DERIVATIVE; SILICON DIOXIDE; THIOL DERIVATIVE;

ARTICLE; CHEMICAL BOND; CHIRAL CHROMATOGRAPHY; CHIRAL STATIONARY PHASE; CHIRALITY; DIFFUSE REFLECTANCE INFRARED FOURIER TRANSFORM SPECTROSCOPY; ENANTIOSELECTIVITY; INFRARED SPECTROSCOPY; LIQUID CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHASE SEPARATION; PHASE TRANSITION; PRESSURE; PRIORITY JOURNAL; REACTION TIME; SOLID STATE; SUPERCRITICAL FLUID; SURFACE PROPERTY; SYNTHESIS; TEMPERATURE; THERMOGRAVIMETRY; TIME;

CARBON DIOXIDE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; QUININE; SILICON DIOXIDE;

EID: 34250664664     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2006.12.037     Document Type: Article

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