Formation of palladium nanofilms using electrochemical atomic layer deposition (E-ALD) with chloride complexation

Langmuir

Volumn 29, Issue 5, 2013, Pages 1592-1600

  Sheridan, Leah B ^a   Gebregziabiher, Daniel K ^a   Stickney, John L ^a   Robinson, David B ^b  

^a UNIVERSITY OF GEORGIA   (United States)

^b SANDIA NATIONAL LABORATORIES   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMIC LAYER; COMPLEXING AGENTS; DEPOSIT THICKNESS; DEPOSITION SYSTEMS; DIRECT TRANSFER; EXCHANGE RATES; FLOW CELLS; HOMOGENEOUS FILMS; METALLIC SURFACE; NANO FILMS; OPEN CIRCUITS; PD THIN FILMS; POLYCRYSTALLINE; RATE OF REPLACEMENT; UNDERPOTENTIAL DEPOSITS;

ATOMIC LAYER DEPOSITION; ATOMS; CHLORINE COMPOUNDS; DEPOSITS; ELECTRON PROBE MICROANALYSIS; GOLD DEPOSITS; IONS; PALLADIUM COMPOUNDS;

PALLADIUM;

CHLORIDE; COPPER; GOLD; METAL NANOPARTICLE; PALLADIUM;

ARTICLE; CHEMISTRY; ELECTROCHEMICAL ANALYSIS;

CHLORIDES; COPPER; ELECTROCHEMICAL TECHNIQUES; GOLD; METAL NANOPARTICLES; PALLADIUM;

EID: 84873400556     PISSN: 07437463     EISSN: 15205827     Source Type: Journal    
DOI: 10.1021/la303816z     Document Type: Article

References (64)

1. Adams, B. D.; Chen, A. C. The role of palladium in a hydrogen economy Mater. Today 2011, 14, 282-289
2. Randler, R. J.; Kolb, D. M.; Ocko, B. M.; Robinson, I. K. Electrochemical copper deposition on Au(100): a combined in situ STM and in situ surface X-ray diffraction study Surf. Sci. 2000, 447, 187-200 (Pubitemid 30557952)
3. Noh, J. S.; Lee, J. M.; Lee, W. Low-dimensional palladium nanostructures for fast and reliable hydrogen gas detection Sensors 2011, 11, 825-851
4. Niessen, R. A. H.; Vermeulen, P.; Notten, P. H. L. The electrochemistry of Pd-coated MgySc(1-y) thin film electrodes: a thermodynamic and kinetic study Electrochim. Acta 2006, 51, 2427-2436 (Pubitemid 43243719)
5. Tan, Z. P.; Chiu, C.; Heilweil, E. J.; Bendersky, L. A. Thermodynamics, kinetics and microstructural evolution during hydrogenation of iron-doped magnesium thin films Int. J. Hydrogen Energy 2011, 36, 9702-9713
6. Lai, B. K.; Kerman, K.; Ramanathan, S. Methane-fueled thin film micro-solid oxide fuel cells with nanoporous palladium anodes J. Power Sources 2011, 196, 6299-6304
7. Kang, S.; Heo, P.; Lee, Y. H.; Ha, J.; Chang, I.; Cha, S. W. Low intermediate temperature ceramic fuel cell with Y-doped BaZrO(3) electrolyte and thin film Pd anode on porous substrate Electrochem. Commun. 2011, 13, 374-377
8. Zhang, J. T.; Qiu, C. C.; Ma, H. Y.; Liu, X. Y. Facile fabrication and unexpected electrocatalytic activity of palladium thin films with hierarchical architectures J. Phys. Chem. C 2008, 112, 13970-13975
9. Barlow, F.; Elshabini-Riad, A.; Brown, R. Film deposition techniques and processes. In Thin Film Technology Handbook; Barlow, F.; Elshabini-Riad, A., Ed.; McGraw-Hill: New York, 1997.
10. Electrochemical Society Transactions; The Electrochemical Society: Pennington, NJ, 2007; Vol. 11.
11. George, S. M. Atomic layer deposition: an overview Chem. Rev. 2010, 110, 111-131
12. Stickney, J. L. Electrochemical Atomic Layer Epitaxy (EC-ALE): Nanoscale Control in the Electrodeposition of Compound Semiconductors. In Advances in Electrochemical Science and Engineering; Alkire, R. C.,; Kolb, D. M., Ed. Wiley-VCH: Weinheim, Germany, 2002; Vol. 7.
13. Adzic, R. R. Electrocatalytic Properties of the Surfaces Modified by Foreign Metal Adatoms; Wiley-Interscience: New York, 1984; Vol. 13, pp 159-260.
14. Herrero, E.; Buller, L. J.; Abruna, H. D. Underpotential deposition at single crystal surfaces of Au, Pt, Ag and other materials Chem. Rev. 2001, 101, 1897-1930 (Pubitemid 35381670)
15. Kolb, D. M. Advances in Electrochemistry and Electrochemical Engineering; John Wiley: New York, 1978; Vol. 11, p 125.
16. Brankovic, S. R.; Wang, J. X.; Adzic, R. R. Metal monolayer deposition by replacement of metal adlayers on electrode surfaces Surf. Sci. 2001, 474, L173-L179
17. Mrozek, M. F.; Xie, Y.; Weaver, M. J. Surface-enhanced Raman scattering on uniform platinum-group overlayers: preparation by redox replacement of underpotential-deposited metals on gold Anal. Chem. 2001, 73, 5953-5960 (Pubitemid 34042211)
18. Vasilic, R.; Dimitrov, N. Epitaxial growth by monolayer-restricted galvanic displacement Electrochem. Solid State Lett. 2005, 8, C173-C176
19. Kim, Y. G.; Kim, J. Y.; Vairavapandian, D.; Stickney, J. L. Platinum nanofilm formation by EC-ALE via redox replacement of UPD copper: studies using in-situ scanning tunneling microscopy J. Phys. Chem. B 2006, 110, 17998-18006 (Pubitemid 44555473)
20. Thambidurai, C.; Gebregziabiher, D. K.; Liang, X. H.; Zhang, Q. H.; Ivanova, V.; Haumesser, P. H.; Stickney, J. L. E-ALD of Cu nanofilms on Ru/Ta wafers using surface limited redox replacement J. Electrochem. Soc. 2010, 157, D466-D471
21. Thambidurai, C.; Kim, Y. G.; Jayaraju, N.; Venkatasamy, V.; Stickney, J. L. Copper nanofilm formation by electrochemical ALD J. Electrochem. Soc. 2009, 156, D261-D268
22. Thambidurai, C.; Kim, Y. G.; Stickney, J. L. Electrodeposition of Ru by atomic layer deposition (ALD) Electrochim. Acta 2008, 53, 6157-6164
23. Gebregziabiher, D. K.; Kim, Y. G.; Thambidurai, C.; Ivanova, V.; Haumesser, P. H.; Stickney, J. L. Electrochemical atomic layer deposition of copper nanofilms on ruthenium J. Cryst. Growth 2010, 312, 1271-1276
24. Viyannalage, L. T.; Vasilic, R.; Dimitrov, N. Epitaxial growth of Cu on Au(111) and Ag(111) by surface limited redox replacement-An electrochemical and STM study J. Phys. Chem. C 2007, 111, 4036-4041 (Pubitemid 46548891)
25. Vasilic, R.; Viyannalage, L. T.; Dimitrov, N. Epitaxial growth of Ag on Au(111) by galvanic displacement of Pb and Tl monolayers J. Electrochem. Soc. 2006, 153, C648-C655
26. Fayette, M.; Liu, Y.; Bertrand, D.; Nutariya, J.; Vasiljevic, N.; Dimitrov, N. From Au to Pt via surface limited redox replacement of Pb UPD in one-cell configuration Langmuir 2011, 27, 5650-5658
27. Jayaraju, N.; Vairavapandian, D.; Kim, Y. G.; Banga, D.; Stickney, J. L. Electrochemical atomic layer deposition (E-ALD) of Pt nanofilms using SLRR cycles J. Electrochem. Soc. 2012, 159, D616-D622
28. McCurry, D. A.; Kamundi, M.; Fayette, M.; Wafula, F.; Dimitrov, N. All electrochemical fabrication of a platinized nanoporous Au thin-film catalyst ACS Appl. Mater. Interfaces 2011, 3, 4459-4468
29. Jayaraju, N. Electrochemical Atomic Layer Deposition (E-ALD) of Pt and PtRu Nanofilms. Ph.D. Dissertation, University of Georgia, Athens, GA, 2010.
30. Sheridan, L. B.; Czerwiniski, J.; Jayaraju, N.; Gebregziabiher, D. K.; Stickney, J. L.; Robinson, D. B.; Soriaga, M. P. Electrochemical atomic layer deposition (E-ALD) of palladium nanofilms by surface limited redox replacement (SLRR), with EDTA complexation Electrocatalysis 2012, 3, 96-107
31. Tang, J.; Petri, M.; Kibler, L. A.; Kolb, D. M. Pd deposition onto Au(111) electrodes from sulphuric acid solution Electrochim. Acta 2005, 51, 125-132 (Pubitemid 41360519)
32. Kibler, L. A.; Kleinert, M.; Randler, R.; Kolb, D. M. Initial stages of Pd deposition on Au(hkl)-part I: Pd on Au(111) Surf. Sci. 1999, 443, 19-30 (Pubitemid 129588393)
33. Quayum, M. E.; Ye, S.; Uosaki, K. Mechanism for nucleation and growth of electrochemical palladium deposition on an Au(111) electrode J. Electroanal. Chem. 2002, 520, 126-132 (Pubitemid 34201169)
34. Takahasi, M.; Hayashi, Y.; Mizuki, J.; Tamura, K.; Kondo, T.; Naohara, H.; Uosaki, K. Pseudomorphic growth of Pd monolayer on Au(111) electrode surface Surf. Sci. 2000, 461, 213-218
35. Lebouin, C.; Olivier, Y. S.; Sibert, E.; Millet, P.; Maret, M.; Faure, R. Electrochemically elaborated palladium nanofilms on Pt(111): characterization and hydrogen insertion study J. Electroanal. Chem. 2009, 626, 59-65
36. Baricuatro, J. H.; Hossain, M. A.; Park, Y. S.; Soriaga, M. P. UHV-EC characterization of ultrathin films electrodeposited on well-defined noble metals. I: Pd on Pt(111) Electrocatalysis 2010, 1, 28-33
37. Wade, T. L.; Sorenson, T. A.; Stickney, J. L. Interfacial Electrochemistry; Marcel Dekker: New York, 1999.
38. Stickney, J. L. Electrochemical Atomic Layer Epitaxy. In Electroanalytical Chemistry; Bard, A. J.; Rubinstein, I., Eds.; Taylor & Francis: London, 2005; Vol. 21, pp 75-209.
39. Sanabria-Chinchilla, J.; Baricuatro, J. H.; Soriaga, M. P.; Hernandez, F.; Baltruschat, H. Electrocatalytic hydrogenation and oxidation of aromatic compounds studied by ITEMS: benzene and p-dihydroxybenzene at ultrathin Pd films electrodeposited on Au(hkl) surfaces J. Colloid Interface Sci. 2007, 314, 152-159 (Pubitemid 47187425)
40. Gokcen, D.; Bae, S. E.; Brankovic, S. R. Stoichiometry of Pt submonolayer deposition via surface-limited redox replacement reaction J. Electrochem. Soc. 2010, 157, D582-D587
41. Ghodbane, O.; Roue, L.; Belanger, D. Study of the electroless deposition of Pd on Cu-modified graphite electrodes by metal exchange reaction Chem. Mater. 2008, 20, 3495-3504
42. Abys, J. A.; Dullaghan, C. A. Electrodeposition of Palladium and Palladium Alloys. In Modern Electroplating, 4 th ed.; Schlesinger, M.; Paunovic, M., Eds.; Wiley: New York, 2000; pp 483-554.
43. Takahasi, M.; Tamura, K.; Mizuki, J.; Kondo, T.; Uosaki, K., Orientation dependence of Pd growth on Au electrode surfaces. J. Phys.: Condens. Matter 2010, 22.
44. Naohara, H.; Ye, S.; Uosaki, K. Electrochemical layer-by-layer growth of palladium on an Au(111) electrode surface: evidence for important role of adsorbed Pd complex J. Phys. Chem. B 1998, 102, 4366-4373 (Pubitemid 128576709)
45. Kibler, L. A.; El-Aziz, A. M.; Kolb, D. M. Electrochemical behaviour of pseudomorphic overlayers: Pd on Au(111) J. Mol. Catal. A: Chem. 2003, 199, 57-63
46. Baldauf, M.; Kolb, D. M. A hydrogen adsorption and absorption study with ultrathin Pd overlayers on Au(111) and Au(100) Electrochim. Acta 1993, 38, 2145-2153
47. Cruywagen, J. J.; Kriek, R. J. Complexation of palladium(II) with chloride and hydroxide J. Coord. Chem. 2007, 60, 439-447
48. Elding, L. I. Palladium(II) halide complexes. I. Stabilities and spectra of palladium(II) chloro and bromo aqua complexes Inorg. Chim. Acta 1972, 6, 647-651
49. Basolo, F. Mechanisms of Inorganic Reactions: A Study of Metal Complexes in Solution, 2 nd ed.; Wiley: New York, 1967.
50. Templeton, D. H.; Watt, G. W.; Garner, C. S. The formal electrode potentials of palladium in aqueous hydrochloric and perchloric acid solutions. Stability of chloropalladite ion J. Am. Chem. Soc. 1943, 65, 1608-1612
51. 2+ couple J. Chem. Soc. A 1967, 1301-1304
52. Kragten, J. The stability constant of Pd-EDTA Talanta 1978, 25, 239-240
53. Aochi, Y. O.; Sawyer, D. T. Proton nuclear magnetic resonance studies of ethylenediaminetetraacetic acid complexes of zirconium(4), hafnium(4) and palladium(2) S Inorg. Chem. 1966, 5, 2085-2092
54. Ware, M. J. An investigation of platinum and palladium printing J. Photogr. Sci. 1986, 34, 13-25
55. Jayaraju, N.; Vairavapandian, D.; Kim, Y.G.; Banga, D.; Stickney, J. L. Electrochemical atomic layer deposition (ALD) of Pt nanofilms using SLRR cycles J. Electrochem. Soc. 2012, 159, D616-D622
56. Venables, J. Introduction to Surface and Thin Film Processes; Cambridge University Press: Cambridge, U.K., 2000.
57. Kibler, L. A.; Kleinert, M.; Lazarescu, V.; Kolb, D. M. Initial stages of palladium deposition on Au(h k l) part III: Pd on Au(110) Surf. Sci. 2002, 498, 175-185 (Pubitemid 34097385)
58. Naohara, H.; Ye, S.; Uosaki, K. Epitaxial growth of a palladium layer on an Au(100) electrode J. Electroanal. Chem. 1999, 473, 2-9 (Pubitemid 30507109)
59. Grden, M.; Lukaszewski, M.; Jerkiewicz, G.; Czerwinski, A. Electrochemical behaviour of palladium electrode: oxidation, electrodissolution and ionic adsorption Electrochim. Acta 2008, 53, 7583-7598
60. Lukaszewski, M.; Hubkowska, K.; Czerwinski, A. Electrochemical absorption and oxidation of hydrogen on palladium alloys with platinum, gold and rhodium Phys. Chem. Chem. Phys. 2010, 12, 14567-14572
61. Czerwinski, A.; Kiersztyn, I.; Grden, M.; Czapla, J. The study of hydrogen sorption in palladium limited volume electrodes (Pd-LVE) I. Acidic solutions J. Electroanal. Chem. 1999, 471, 190-195
62. Bartlett, P. N.; Gollas, B.; Guerin, S.; Marwan, J. The preparation and characterisation of H-1-e palladium films with a regular hexagonal nanostructure formed by electrochemical deposition from lyotropic liquid crystalline phases Phys. Chem. Chem. Phys. 2002, 4, 3835-3842
63. 4 solution Electrochim. Acta 1991, 36, 1235-1240 (Pubitemid 23594387)
64. Hamelin, A. Cyclic voltammetry at gold single-crystal surfaces 0.1. Behaviour at low-index faces J. Electroanal. Chem. 1996, 407, 1-11 (Pubitemid 126368976)