Multiresidue determination of 375 organic contaminants including pesticides, polychlorinated biphenyls and polyaromatic hydrocarbons in fruits and vegetables by gas chromatography-triple quadrupole mass spectrometry with introduction of semi-quantification approach

Journal of Chromatography A

Volumn 1270, Issue , 2012, Pages 283-295

  Banerjee, Kaushik ^a   Utture, Sagar ^a   Dasgupta, Soma ^a   Kandaswamy, Chandrasekar ^b   Pradhan, Saswati ^a   Kulkarni, Sunil ^b   Adsule, Pandurang ^a  

^a NATIONAL RESEARCH CENTRE FOR GRAPES   (India)

^b Agilent Technologies   (India)

Author keywords

Dioxin like polychlorinated biphenyls; Gas chromatography triple quadrupole mass spectrometry; Method validation; Multiresidue analysis, semi quantification; Polyaromatic hydrocarbons, pesticide residues

Indexed keywords

DIOXIN-LIKE POLYCHLORINATED BIPHENYLS; METHOD VALIDATIONS; MULTI-RESIDUE ANALYSIS; PESTICIDE RESIDUE; QUADRUPOLE MASS SPECTROMETRY;

CALIBRATION; FRUITS; GAS CHROMATOGRAPHY; HYDROCARBONS; IMPACT IONIZATION; MASS SPECTROMETRY; PESTICIDES; POLYCHLORINATED BIPHENYLS;

ORGANIC POLLUTANTS;

ACETIC ACID ETHYL ESTER; AMINE; BETA HEXACHLOROCYCLOHEXANE; CHLORPYRIFOS; CYHALOTHRIN; GRAPHITE; PESTICIDE; POLYCHLORINATED BIPHENYL; POLYCYCLIC AROMATIC HYDROCARBON;

ACCURACY; ARTICLE; CALIBRATION; CHEMICAL ANALYSIS; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DOSIMETRY; EUROPEAN UNION; FRUIT; GAS CHROMATOGRAPHY; GRAPE; LIMIT OF DETECTION; LIMIT OF QUANTITATION; NONHUMAN; OKRA; ONION; POMEGRANATE; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUADRUPOLE MASS SPECTROMETRY; QUANTITATIVE ANALYSIS; RESIDUE ANALYSIS; SOLID PHASE EXTRACTION; TOMATO; VEGETABLE;

ACETATES; FRUIT; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PESTICIDE RESIDUES; POLYCHLORINATED BIPHENYLS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; VEGETABLES;

ABELMOSCHUS; ALLIUM CEPA; LYCOPERSICON ESCULENTUM; LYTHRACEAE; VITACEAE;

EID: 84872271689     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.10.066     Document Type: Article

References (20)

1. Insecticides Registered under section 9 (3) of the Insecticides Act, 1968 as on 20/01/2012, New Delhi, India. (accessed 13.03.12). http://www.cibrc.nic.in/reg_products.htm.
2. Pesticide EU-MRLs, Regulation (EC) No 396/2005. (accessed 13.03.12). http://ec.europa.eu/sanco_pesticides/public/index.cfm.
3. Wong J.W., Zhang K., Tech K., Hayward D.G., Krynitsky A.J., Cassias I., Schenck F.J., Banerjee K., Dasgupta S., Brown D. J. Agric. Food Chem. 2010, 58:5884.
4. Savant R., Banerjee K., Utture S.C., Patil S.H., Ghaste M.S., Adsule P.G. J. Agric. Food Chem. 2010, 58:1447.
5. Walorczyk S. J. Chromatogr. A 2008, 1208:202.
6. Moreno J.L.F., Frenich A.G., Bolanos P.P., Vidal J.L.M. J. Mass Spectrom. 2008, 43:1235.
7. Utture S.C., Banerjee K., Dasgupta S., Patil S.H., Jadhav M.R., Wagh S.S., Kolekar S.S., Anuse M.A., Adsule P.G. J. Agric. Food Chem. 2011, 59:7866.
8. Method validation & quality control procedures for pesticide residues analysis in food & feed, Document No. SANCO/12495/2011.
9. Horwitz W., Albert R. J. AOAC Int. 2006, 89:1095.
10. Horwitz W., Kamps L.R., Boyer K.W. J. Assoc. Off. Anal. Chem. 1980, 63:1344.
11. Guide CG 4, Quantifying Uncertainty in Analytical Measurement, 3rd ed., EURACHEM [UK]/CITAC [UK]. 2012. http://www.measurementuncertainty.org/.
12. Banerjee K., Oulkar D.P., Dasgupta S., Patil S.B., Patil S.H., Savant R., Adsule P.G. J. Chromatogr. A 2007, 1173:98.
13. Dasgupta S., Banerjee K., Utture S., Kusari P., Wagh S., Dhumal K., Kolekar S., Adsule P.G. J. Chromatogr. A 2011, 1218:6780.
14. Mezcua M., Martinez-Uroz M.A., Wylie P.L., Fernandez-Alba A.R. J. AOAC Int. 2009, 92:1790.
15. Lehotay S.J. J. AOAC Int. 2007, 90:485.
16. Mol H.G.J., Rooseboom A., van Dam R., Roding M., Arondeus K., Sunarto S. Anal. Bioanal. Chem. 2007, 389:1715.
17. Utture S.C., Banerjee K., Kolekar S.S., Dasgupta S., Oulkar D.P., Patil S.H., Wagh S.S., Adsule P.G., Anuse M.A. Food Chem. 2012, 131:787.
18. Wylie P.L., Uchiyama K. J. AOAC Int. 1996, 79:571.
19. http://www.fao.org/ag/AGP/AGPP/Pesticid/JMPR/Download/97_eva/Chlorot.PDF.
20. http://www.fao.org/ag/AGP/AGPP/Pesticid/JMPR/Download/97_eva/Carbosul.PDF.