Critical assessment of extraction methods for the simultaneous determination of pesticide residues and mycotoxins in fruits, cereals, spices and oil seeds employing ultra-high performance liquid chromatography-tandem mass spectrometry

Journal of Chromatography A

Volumn 1262, Issue , 2012, Pages 8-18

  Lacina, Ondrej ^a   Zachariasova, Milena ^a   Urbanova, Jana ^a   Vaclavikova, Marta ^a   Cajka, Tomas ^a   Hajslova, Jana ^a  

^a INSTITUTE OF CHEMICAL TECHNOLOGY   (Czech Republic)

Author keywords

Liquid chromatography tandem mass spectrometry; Mycotoxins; Pesticide residues; Sample preparation

Indexed keywords

ANALYTES; AQUEOUS ACETONITRILE; BABY FOODS; CRITICAL ASSESSMENT; CURRENT TRENDS; EUROPEAN FOOD SAFETY AUTHORITIES; EXTRACTION EFFICIENCIES; EXTRACTION METHOD; EXTRACTION PROCEDURE; FOOD CONTAMINANTS; FOOD SAFETY CONTROL; HIGH-THROUGHPUT METHOD; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; MATRIX EFFECTS; MULTI-ANALYTES; MYCOTOXINS; NON-POLAR; OPTIMAL SAMPLES; PERFORMANCE CHARACTERISTICS; PESTICIDE RESIDUE; QUANTIFICATION LIMIT; RAPID ISOLATION; SAMPLE PREPARATION; SIMULTANEOUS DETERMINATIONS; SUNFLOWER SEEDS; TARGET ANALYTES; ULTRA-HIGH PERFORMANCE; WHEAT FLOURS;

ACETONITRILE; CHROMATOGRAPHY; ESSENTIAL OILS; EXPERIMENTS; FOOD PRODUCTS; FOOD SAFETY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; OILS AND FATS;

PESTICIDES;

ACETONITRILE; ESSENTIAL OIL; FAT; MYCOTOXIN; PESTICIDE RESIDUE; PIGMENT;

APPLE; ARTICLE; BABY FOOD; CEREAL; CONTROLLED STUDY; FLOUR; FOOD ANALYSIS; FOOD COMPOSITION; FOOD CONTAMINATION; FOOD SAFETY; FRUIT; INTERMETHOD COMPARISON; LIMIT OF DETECTION; MOISTURE; NONHUMAN; OIL SEED; PLANT SEED; PRIORITY JOURNAL; SPICE; SUNFLOWER; TANDEM MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; WHEAT;

CEREALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FOOD ANALYSIS; FRUIT; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; MYCOTOXINS; PESTICIDE RESIDUES; PLANT OILS; SPICES; TANDEM MASS SPECTROMETRY;

HELIANTHUS; MALUS X DOMESTICA; TRITICUM AESTIVUM;

EID: 84867202239     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.08.097     Document Type: Article

References (28)

1. Commission regulation (EC) No. 1881/2006 of 19 December 2006 setting maximum levels for certain contaminants in foodstuffs, (accessed on 22.10.11). http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2006:364:0005:0024:EN:PDF.
2. Commission regulation (EC) No. 1126/2007 of 28 September 2007 amending Regulation (EC) No. 1881/2006 setting maximum levels for certain contaminants in foodstuffs as regards Fusarium toxins in maize and maize products, (accessed on 22.10.11). http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2007:255:0014:0017:EN:PDF.
3. Regulation (EC) No. 396/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC, (accessed on 22.10.11). http://ec.europa.eu/sanco_pesticides/public/index.cfm.
4. Mol H.G.J., Plaza-Bolanos P., Zomer P., de Rijk T.C., Stolker A.A.M., Mulder P.P.J. Anal. Chem. 2008, 80(24):9450.
5. Romero-Gonzáles R., Frenich A.G., Vidal J.L.M., Prestes O.D., Grio S.L. J. Chromatogr. A 2011, 1218:1477.
6. Amate C.F., Unterluggauer H., Fischer R.J., Fernández-Alba A.R., Masselter S. Anal. Bioanal. Chem. 2010, 397:93.
7. Anastassiades M., Lehotay S.J., Štajnbaher D., Schenck F.J. J. AOAC Int. 2003, 86:412.
8. Lehotay S.J., Mastovska K., Lightfield A.R. J. AOAC Int. 2005, 88:615.
9. Frenich A.G., Vidal J.L.M., Romero-González R., del Mar Aguilera-Luiz M. Food Chem. 2009, 117:705.
10. Document SANCO/12495/2011 Method validation and quality control procedures for pesticide residues analysis in food and feed, (accessed on 28.03.12). http://ec.europa.eu/food/plant/protection/pesticides/docs/qualcontrol_en.pdf.
11. Pozo O.J., Sancho J.V., Ibáñez M., Hérnadez F., Niessen W.M.A. TrAC: Trends Anal. Chem. 2006, 25:1030.
12. Schürmann A., Dvorak V., Crüzer C., Butcher P., Kaufmann A. Rapid Commun. Mass Spectrom. 2009, 23:1196.
13. Botero-Coy A.M., Marín J.M., Ibáñez M., Sancho J.V., Hérnadez F. Anal. Bioanal. Chem. 2012, 402:2287.
14. Marín J.M., Garcia-Lor E., Sancho J.V., López F.J., Henrández F. J. Chromatogr. A 2009, 1216:1410.
15. Spanjer M.C., Rensen P.M., Scholten J.M. Food Addit. Contam. 2008, 25:472.
16. Sulyok M.M., Krska R., Schuhmaher R. Anal. Bioanal. Chem. 2007, 389:1505.
17. Alder L., Greulich K., Kempe G., Vieth B. Mass Spectrom. Rev. 2006, 25:838.
18. Pizzutti I.R., de Kok A., Zanella R., Adaime M.B., Hiemstra M., Wickert C., Prestes O.D. J. Chromatogr. A 2007, 1142:123.
19. Sulyok M., Berthiller F., Krska R., Schuhmacher R. Rapid Commun. Mass Spectrom. 2006, 20:2649.
20. Berger U., Oehme M., Kuhn F. J. Agric. Food Chem. 1999, 47:4240.
21. EN 15662:2008, Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE-QuEChERS-method.
22. Lehotay S.J., Son K.A., Kwon H., Koesukwiwat U., Fu W., Mastovska K., Hoh E., Leepipatpiboon N. J. Chromatogr. A 2010, 1217:2548.
23. Hafner M., Sulyok M., Schuhmacher R., Crews C., Krska R. World Mycotoxin J. 2008, 1:67.
24. Komarova E.L., Tolkachev O.N. Pharm. Chem. J. 2001, 35:504-513.
25. Zachariasova M., Lacina O., Malachova A., Kostelanska M., Poustka J., Godula M., Hajslova J. Anal. Chim. Acta 2010, 662:51.
26. Commission directive 2006/125/EC of 5 December 2006 on processed cereal-based foods and baby foods for infants and young children, (accessed on September 2011). http://eur-lex.europa.eu/LexUriServ/LexUriServ.do%3Furi=OJ%3AL%3A2006%3A339%3A0016%3A0035%3AEN%3APDF.
27. Kalachova K., Pulkrabova J., Drabova L., Cajka T., Kocourek V., Hajslova J. Anal. Chim. Acta 2011, 707:84.
28. Lacina O., Urbanova J., Poustka J., Hajslova J. J. Chromatogr. A 2010, 1217:648.