Alternative method for gas chromatography-mass spectrometry analysis of short-chain fatty acids in faecal samples

Journal of Separation Science

Volumn 35, Issue 15, 2012, Pages 1906-1913

  García Villalba, Rocio ^a   Giménez Bastida, Juan A ^a   García Conesa, Maria T ^a   Tomás Barberán, Francisco A ^a   Carlos Espín, Juan ^a   Larrosa, Mar ^a  

^a RESEARCH GROUP ON QUALITY   (Spain)

Author keywords

Faecal samples; Gas chromatography; Mass spectrometry; Short chain fatty acids; Solvent extraction

Indexed keywords

ALTERNATIVE METHODS; ANALYTICAL METHOD; BACTERIAL METABOLISM; BIOLOGICAL SAMPLES; DERIVATIZATIONS; END-PRODUCTS; ETHYL ACETATES; FAECAL SAMPLES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GAS CHROMATOGRAPHY-MASS SPECTROMETRY METHODS; HEALTH BENEFITS; INTERNAL STANDARDS; LARGE BOWEL; LIMITS OF DETECTION; MATRIX EFFECTS; SHORT-CHAIN FATTY ACIDS; VALERIC ACIDS; VOLATILE COMPOUNDS; WIDE-LINEAR RANGE;

CARBOHYDRATES; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; SOLVENT EXTRACTION; VOLATILE ORGANIC COMPOUNDS;

BACTERIA;

ACETIC ACID ETHYL ESTER; SHORT CHAIN FATTY ACID; VOLATILE AGENT;

ANALYTIC METHOD; ANIMAL EXPERIMENT; ARTICLE; DERIVATIZATION; FECES; HUMAN; HUMAN EXPERIMENT; LIMIT OF DETECTION; MASS FRAGMENTOGRAPHY; NONHUMAN; NORMAL HUMAN; PRIORITY JOURNAL; RAT; STANDARD;

ANIMALS; FATTY ACIDS, VOLATILE; FECES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; MALE; RATS; RATS, INBRED F344;

BACTERIA (MICROORGANISMS); RATTUS;

EID: 84864577726     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201101121     Document Type: Article

References (28)

1. Won, J. M. W., Jenkins, D. J. A., J. Nutr. 2007, 137, 2539S-2546S.
2. Tpooing, D. L., Clifton, P. M., Physiol. Rev. 2001, 81, 1031-1064.
3. Macfarlane, S., Macfarlane, G. T., Proc. Nutr. Soc. 2003, 62, 67-72.
4. Henningsson, A. M., Nyman, E. M., Björck, I. M., J. Sci. Food Agric. 2002, 82, 385-393.
5. Havenaar, R., Beneficial Microbes. 2011, 2, 103-114.
6. Binder, H. J., Annu. Rev. Physiol. 2010, 72, 297-313.
7. Wong, J. M., de Souza, R., Kendall, C. W., Emam, A., Jenkins, D. J., J. Clin. Gastroenterol. 2006, 40, 235-243.
8. Scharlau, D., Borowicki, A., Habermann, N., Hofmann, T., Klenow, S., Miene, C., Munjal, U., Stein, K., Glei, M., Mutat. Res. 2009, 682, 39-53.
9. Vitali, B., Ndagijimana, M., Cruciani, F., Carnevali, P., Candela, M., Guerzoni, M. E., Brigidi, P., BMC Microbiol. 2010, 10, 4-17.
10. McGrath, L. T., Weir, C. D., Maynard, S., Rowlands, B. J., Anal. Biochem. 1992, 207, 227-230.
11. Zijlstra, J. B., Beukema, J., Wolthers, B. G., Byrne, B. M., Groen, A., Dankert, J., Clin. Chim. Acta 1977, 78, 243-250.
12. Tangerman, A., van Schaik, A., Meuwese-Arends, M. T., van Tongeren, J. H. M., Clin. Chim. Acta 1983, 133, 341-348.
13. Remesy, C., Demigne, C., Biochem. J. 1974, 141, 85-91.
14. Cummings, J. H., Pomare, E. W., Branch, W. J., Naylor, C. P. E., Mcfarlane, G. T., Gut 1987, 28, 1221-1227.
15. Henningsson, A. M., Björck, I. M., Nyman, E. M., J. Nutr. 2002, 132, 3098-3104.
16. Buchanan, D. N., Thoene, J. G., Clin. Chim. Acta 1985, 145, 183-191.
17. Ryan, J. P., Anal. Biochem. 1980, 108, 374-384.
18. Zhao, G., Nyman, M., Jönsson, A., Biomed. Chromatogr. 2006, 20, 674-682.
19. Tangerman, A., Nagengast, F. M., Anal. Biochem. 1996, 236, 1-8.
20. Mills, G. A., Walker, V., Mughal, H., J. Chromatogr. B 1999, 730, 113-122.
21. Mills, G. A., Walker, V., J. Chromatogr. A 2000, 902, 267-287.
22. Bianchi, F., Dall'Asta, M., Del Rio, D., Mangia, A., Musci, M., Scazzina, F., Food Chem. 2011, 129, 200-205.
23. Hoentjen, F., Welling, G. W., Harmsen, H. J., Zhang, X., Snart, J., Tannock, G. W., Lien, K., Churchill, T. A., Lupicki, M., Dieleman, L. A., Inflammatory Bowel Dis. 2005, 11, 977-985.
24. Curie, L. A., Pure Appl. Chem. 1995, 67, 1699-1723.
25. Kruve, A., Künnapas, A., Herodes, K., Leito, I., J. Chromatogr. A 2008, 1187, 58-66.
26. Hercegová, A., Domotorová, M., Matisová, E., J. Chromatogr. A 2007, 1153, 54-73.
27. Leis, H. J., Schütz, H., Windischhofer, W., Anal. Bioanal. Chem. 2011, 400, 2663-2670.
28. Mcfarlane, S., Macfarlane, G. T., Proc. Nutr. Soc. 2003, 62, 67-72.