A multi-residue method for pesticides analysis in green coffee beans using gas chromatography-negative chemical ionization mass spectrometry in selective ion monitoring mode

Journal of Chromatography A

Volumn 1251, Issue , 2012, Pages 16-26

  Pizzutti, Ionara R ^a   de Kok, Andre ^b   Dickow Cardoso, Carmem ^a   Reichert, Bárbara ^a   de Kroon, Marijke ^b   Wind, Wouter ^b   Weber Righi, Laís ^a   Caiel da Silva, Rosselei ^a  

^a FEDERAL UNIVERSITY OF SANTA MARIA   (Brazil)

^b Voedsel en Waren Autoriteit Netherlands   (Netherlands)

Author keywords

Gas chromatography mass spectrometry (GC MS); Green coffee beans; Modified QuEChERS method; Negative chemical ionization (NCI); Pesticides; Selected ion monitoring (SIM) mode

Indexed keywords

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GREEN COFFEE BEANS; MODIFIED QUECHERS-METHOD; NEGATIVE CHEMICAL IONIZATION; SELECTED-ION MONITORING;

ACETONITRILE; CALIBRATION; DEGRADATION; DETECTORS; FUNGICIDES; GAS CHROMATOGRAPHY; HOMOGENIZATION METHOD; IONIZATION; ISOMERS; MAGNESIUM; MASS SPECTROMETRY; PESTICIDES; PHASE SEPARATION; RECOVERY; SILICA;

CHEMICAL ANALYSIS;

1,1 DICHLORO 2,2 BIS(4 CHLOROPHENYL)ETHYLENE; ACETIC ACID; ACETONITRILE; ALDRIN; BIFENTHRIN; CAPTAFOL; CAPTAN; CHLOROTHALONIL; CHLORPYRIFOS; CHLORPYRIFOS METHYL; DICOFOL; DIELDRIN; ENDOSULFAN; ENDRIN; FENITROTHION; FOLPET; HEPTACHLOR; HEXACHLOROBENZENE; LINDANE; MAGNESIUM SULFATE; MITOTANE; PARATHION; PARATHION METHYL; PERMETHRIN; PESTICIDE RESIDUE; PHTHALIMIDE; QUINTOZENE; SILICON DIOXIDE; TETRADIFON;

ACCURACY; AGRICULTURAL SLURRY; ARTICLE; CALIBRATION; COFFEE; ION MONITORING; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; PHASE SEPARATION; PRIORITY JOURNAL; PRODUCT RECOVERY; REPRODUCIBILITY; RESIDUE ANALYSIS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; VALIDATION PROCESS;

COFFEE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; PESTICIDE RESIDUES; REPRODUCIBILITY OF RESULTS; SEEDS; SENSITIVITY AND SPECIFICITY;

EID: 84864068780     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.06.041     Document Type: Article

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