Multi-residue method for determination of seven neonicotinoid insecticides in grains using dispersive solid-phase extraction and dispersive liquid-liquid micro-extraction by high performance liquid chromatography

Food Chemistry

Volumn 134, Issue 3, 2012, Pages 1691-1698

  Wang, P ^a   Yang, X ^a,b   Wang, J ^b   Cui, J ^a   Dong, A J ^a   Zhao, H T ^a   Zhang, L W ^a   Wang, Z Y ^a   Xu, R B ^a   Li, W J ^a   Zhang, Y C ^a   Zhang, H ^a   Jing, J ^a  

^a HARBIN INSTITUTE OF TECHNOLOGY   (China)

^b INSTITUTE OF PLANT PROTECTION   (China)

Author keywords

DLLME; DSPE; Grains; HPLC; Multi residue analysis; Neonicotinoid insecticides

Indexed keywords

DLLME; DSPE; HPLC; MULTI-RESIDUE ANALYSIS; NEONICOTINOID INSECTICIDES;

ACETONITRILE; CARBON BLACK; CHROMATOGRAPHY; GRAIN (AGRICULTURAL PRODUCT); HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INSECTICIDES; ORGANIC SOLVENTS; PHASE SEPARATION; SOLVENT EXTRACTION;

LIQUIDS;

ACETAMIPRID; ACETONITRILE; CLOTHIANIDIN; DINOTEFURAN; IMIDACLOPRID; INSECTICIDE; NITENPYRAM; PESTICIDE; THIACLOPRID; THIAMETHOXAM; UNCLASSIFIED DRUG; ACETONITRILE DERIVATIVE; PESTICIDE RESIDUE; SOLVENT;

ARTICLE; GRAIN; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID PHASE MICROEXTRACTION; MAIZE; MILLET; NONHUMAN; OAT; PLANT RESIDUE; REACTION OPTIMIZATION; RESIDUE ANALYSIS; RICE; SOLID PHASE EXTRACTION; CEREAL; CHEMISTRY; PANICUM;

ZEA MAYS;

ACETONITRILES; AVENA SATIVA; CEREALS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; INSECTICIDES; LIQUID PHASE MICROEXTRACTION; ORYZA SATIVA; PANICUM; PESTICIDE RESIDUES; SOLID PHASE EXTRACTION; SOLVENTS; ZEA MAYS;

EID: 84861102188     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2012.03.103     Document Type: Article

References (37)

1. M. Anastassiades, S.J. Lehotay, and D. Štajnbaher Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "Dispersive Solid-Phase Extraction" for the determination of pesticide residues in produce Journal of AOAC International 86 2003 412 431
2. A. Arvolaa, L.L. Kia, and M. Dean Consumers' beliefs about whole and refined grain products in the UK, Italy and Finland Journal of Cereal Science 46 2007 197 206
3. M. Asensio-Ramos, J. Hernández-Borges, L.M. Ravelo-Pérez, and M.A. Rodríguez-Delgado Evaluation of a modified QuEChERS method for the extraction of pesticides from agricultural, ornamental and forestal soils Analytical and Bioanalytical Chemistry 396 2010 2307 2319
4. K. Banerjee, D.P. Oulkar, and S. Dasgupta Validation and uncertainty analysis of a multi-residue method for pesticides in grapes using ethyl acetate extraction and liquid chromatography-tandem mass spectrometry Journal of Chromatography A 1173 2007 98 109
5. R.C. Biever, J.R. Hoberg, and B. Jacobson Icon rice seed treatment toxicity to crayfish (Procambarus clarkii) in experimental rice paddies Environmental Toxicology and Chemistry 22 01 2009 164 174
6. L.S. Cai, J. Xing, L. Dong, and C.Y. Wu Application of polyphenyl methylsiloxane coated fiber for solid-phase microextraction combined with microwave-assisted extraction for the determination of organochlorine pesticides in Chinese teas Journal of Chromatography A 1015 2003 11 21
7. R. Cazorla-Reyes, J.L. Fernández-Moreno, and R. Romero-González Single solid phase extraction method for the simultaneous analysis of polar and non-polar pesticides in urine samples by gas chromatography and ultrahigh pressure chromatography coupled to tandem mass spectrometry Talanta 01 85 2011 183 196
8. G.Q. Chen, P.Y. Cao, and R.J. Liu A multi-residue method for fast determination of pesticides in tea by ultraperformance liquid chromatography-electrospray tandem mass spectrometry combined with modified QuEChERS sample preparation procedure Food Chemistry 125 2011 1406 1411
9. M.A. Farajzadeh, M. Bahram, and M.R. Vardast Dispersive liquid-liquid microextraction for the analysis of three organophosphorus pesticides in real samples by high performance liquid chromatography-ultraviolet detection and its optimization by experimental design Chemistry and Materials Science 172 2011 465 470
10. L. Fariña, E. Boido, F. Carrau, and E. Dellacassa Determination of volatile phenols in red wines by dispersive liquid-liquid microextraction and gas chromatography-mass spectrometry detection Journal of Chromatography A 1157 2007 46 50
11. P. Fidente, S. Seccia, and F. Vanni Analysis of nicotinoid insecticides residues in honey by solid matrix partition clean-up and liquid chromatography-electrospray mass spectrometry Journal of Chromatography A 1094 2005 175 178
12. C. Jansson, T. Pihlstrom, B.G. Öterdahl, and K.E. Markides A new multiresidue method for analysis of pesticide residues in fruit and vegetables using liquid chromatography with tandem mass spectrometric detection Journal of Chromatography A 1023 1 2004 93 104
13. R.R. Kozani, Y. Assadi, F. Shemirani, M.R. Millani Hosseini, and M.R. Jamali Determination of trihalomethanes in drinking water by dispersive liquid-liquid microextraction then gas chromatography with electron-capture detection Chromatographia 66 2007 81 86
14. S.Y. Liu, Z.T. Zheng, and F.L. Wei Simultaneous determination of seven neonicotinoid pesticide residues in food by ultraperformance liquid chromatography tandem mass spectrometry Journal of Agricultural and Food Chemistry 58 2010 3271 3278
15. K. Matsuda, S.D. Buckingham, and D. Kleier Neonicotinoids: Insecticides acting on insect nicotinic acetylcholine receptors Trends in Pharmacological Sciences 22 11 2001 573 580
16. A.D. Muccio, P. Fidente, and D.A. Barbini Application of solid-phase extraction and liquid chromatography-mass spectrometry to the determination of neonicotinoid pesticide residues in fruit and vegetable Journal of Chromatography A 1108 2006 01 06
17. S.A. Mueller, J.E. Anderson, and T.J. Wallington Impact of biofuel production and other supply and demand factors on food price increases in 2008 Biomass and Bioenergy 35 2011 1623 1632
18. H. Obana, M. Okihashi, and K. Akutsu Determination of acetamiprid, imidacloprid, and nitenpyram residues in vegetables and fruits by high-performance liquid chromatography with diode-array detection Journal of Agricultural and Food Chemistry 50 2002 4464 4467
19. H. Obana, M. Okihashi, and K. Akutsu Determination of neonicotinoid pesticide residues in vegetables and fruits with solid phase extraction and liquid chromatography mass spectrometry Journal of Agricultural and Food Chemistry 51 2003 2501 2505
20. Pesticide EU-MRLs Database (2008). European Union, Brussels. Available at: < http://ec.europa.eu/sanco-pesticides/public/index.cfm?event=substance. selection >.
21. M. Rancan, S. Rancan, S. Rossi, and A.G. Sabatini Determination of thiamethoxam residues in honeybees by high performance liquid chromatography with an electrochemical detector and post-column photochemical reactor Journal of Chromatography A 1123 2006 60 65
22. M. Rancan, A.G. Sabatini, G. Achilli, and G.C. Galletti Determination of imidacloprid and metabolites by liquid chromatography with an electrochemical detector and post column photochemical reactor Analytica Chimica Acta 555 2006 60 65
23. S. Seccia, P. Fidente, and D.A. Barbini Multiresidue determination of nicotinoid insecticide residues in drinking water by liquid chromatography with electrospray ionization mass spectrometry Analytica Chimica Acta 553 2005 21 26
24. S. Seccia, P. Fidente, and D. Montesano Determination of neonicotinoid insecticides residues in bovine milk samples by solid-phase extraction clean-up and liquid chromatography with diode-array detection Journal of Chromatography A 1214 2008 115 120
25. D. Štajnbaher, and L. Zupančič-Kralj Multiresidue method for determination of 90 pesticides in fresh fruits and vegetables using solid-phase extraction and gas chromatography-mass spectrometry Journal of Chromatography A 1015 1 2003 185 198
26. P. Venkateswarlu, K.R. Mohan, and C.R. Kumar Monitoring of multi-class pesticide residues in fresh grape samples using liquid chromatography with electrospray tandem mass spectrometry Food Chemistry 105 2007 1760 1766
27. H.X. Wang, M.H. Zhang, and Y. Cai Chapter 3-problems, challenges, and strategic options of grain security in china Advances in Agronomy 103 2009 101 147
28. E. Watanabe, K. Baba, and H. Eun Application of a commercial immunoassay to the direct determination of insecticide imidacloprid in fruit juices Food Chemistry 102 2007 745 750
29. E. Watanabe, K. Baba, and S. Miyake Analytical evaluation of enzyme-linked immunosorbent assay for neonicotinoid dinotefuran for potential application to quick and simple screening method in rice samples Talanta 84 2011 1107 1111
30. E. Watanabe, K. Bara, and H. Eun Simultaneous determination of neonicotinoid insecticides in agricultural samples by solid-phase extraction cleanup and liquid chromatography equipped with diode-array detection Journal of Agricultural and Food Chemistry 55 2007 3798 3804
31. E. Watanabe, H. Euna, and K. Baba Rapid and simple screening analysis for residual imidacloprid in agricultural products with commercially available ELISA Analytica Chimica Acta 521 2004 45 51
32. Q.H. Wu, Z. Li, and C. Wang Dispersive Solid-phase extraction clean-up combined with dispersive liquid-liquid microextraction or the determination of neonicotinoid insecticides in vegetable samples by high-performance liquid chromatography Food Analytical Methods 2011 10.1007/s12161-011-9200-x
33. Q.H. Wu, X. Zhou, and Y.M. Li Application of dispersive liquid-liquid microextraction combined with high-performance liquid chromatography to the determination of carbamate pesticides in water samples Chemistry and Materials Science 393 2009 1755 1761
34. Z.M. Xiao, X.W. Li, and X.L. Wang Determination of neonicotinoid insecticides residues in bovine tissues by pressurized solvent extraction and liquid chromatography-tandem mass spectrometry Journal of Chromatography B 879 2011 171 175
35. X. Yang, J. Wang, D.C. Xu, J.W. Qiu, Y. Ma, and J. Cui Simultaneous determination of 69 pesticide residues in coffee by gas chromatography-mass spectrometry Food Analytical Methods 4 2 2011 186 195
36. X. Yang, D.C. Xu, J.W. Qiu, H. Zhang, Y.C. Zhang, and A.J. Dong Simultaneous determination of 118 pesticide residues in china teas by gas chromatography-mass spectrometry Chemical Paper 63 1 2009 39 46
37. X. Yang, H. Zhang, Y. Liu, J. Wang, Y.C. Zhang, and A.J. Dong Multiresidue method for determination of 88 pesticides in berry fruits using solid-phase extraction and gas chromatography-mass spectrometry: Determination of 88 pesticides in berries using SPE and GC-MS Food Chemistry 127 2011 855 865