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Volumn 8, Issue 2, 2012, Pages 175-185

LC-MS based global metabolite profiling of grapes: Solvent extraction protocol optimisation

Author keywords

Grape metabolome; LC MS; Metabolite profiling; Metabolomics; Sample preparation; Time of flight mass spectrometer

Indexed keywords

CHLOROFORM; METHANOL; WATER;

EID: 84857781822     PISSN: 15733882     EISSN: 15733890     Source Type: Journal    
DOI: 10.1007/s11306-011-0298-z     Document Type: Article
Times cited : (78)

References (42)
  • 1
    • 78649909049 scopus 로고    scopus 로고
    • H-1 NMR-based metabolomics combined with HPLC-PDA-MS-SPE-NMR for investigation of standardized Ginkgo biloba preparations
    • Agnolet, S., Jaroszewski, J., Verpoorte, R., & Staerk, D. (2010). H-1 NMR-based metabolomics combined with HPLC-PDA-MS-SPE-NMR for investigation of standardized Ginkgo biloba preparations. Metabolomics, 6, 292-302.
    • (2010) Metabolomics , vol.6 , pp. 292-302
    • Agnolet, S.1    Jaroszewski, J.2    Verpoorte, R.3    Staerk, D.4
  • 2
    • 72449177422 scopus 로고    scopus 로고
    • H-1 NMR-based metabonomics for the classification of Greek wines according to variety, region, and vintage. Comparison with HPLC data
    • Anastasiadi, M., Zira, A., Magiatis, P., Haroutounian, S., Skaltsounis, A., & Mikros, E. (2009). H-1 NMR-based metabonomics for the classification of Greek wines according to variety, region, and vintage. Comparison with HPLC data. Journal of Agriculture and Food Chemistry, 57, 11067-11074.
    • (2009) Journal of Agriculture and Food Chemistry , vol.57 , pp. 11067-11074
    • Anastasiadi, M.1    Zira, A.2    Magiatis, P.3    Haroutounian, S.4    Skaltsounis, A.5    Mikros, E.6
  • 4
    • 36148968834 scopus 로고    scopus 로고
    • Evaluation of a protocol for metabolic profiling studies on human blood plasma by combined ultra-performance liquid chromatography/mass spectrometry: From extraction to data analysis
    • Bruce, S., Jonsson, P., Antti, H., Cloarec, O., Trygg, J., Marklund, S., et al. (2008). Evaluation of a protocol for metabolic profiling studies on human blood plasma by combined ultra-performance liquid chromatography/mass spectrometry: From extraction to data analysis. Analytical Biochemistry, 372, 237-249.
    • (2008) Analytical Biochemistry , vol.372 , pp. 237-249
    • Bruce, S.1    Jonsson, P.2    Antti, H.3    Cloarec, O.4    Trygg, J.5    Marklund, S.6
  • 5
    • 66149126908 scopus 로고    scopus 로고
    • Investigation of human blood plasma sample preparation for performing metabolomics using ultrahigh performance liquid chromatographn y/mass spectrometry
    • Bruce, S. J., Tavazzi, I., Parisod, V., Rezzi, S., Kochhar, S., & Guy, P. A. (2009). Investigation of human blood plasma sample preparation for performing metabolomics using ultrahigh performance liquid chromatographn y/mass spectrometry. Analytical Chemistry, 81, 3285-3296.
    • (2009) Analytical Chemistry , vol.81 , pp. 3285-3296
    • Bruce, S.J.1    Tavazzi, I.2    Parisod, V.3    Rezzi, S.4    Kochhar, S.5    Guy, P.A.6
  • 6
    • 78649630860 scopus 로고    scopus 로고
    • The SSR-based molecular profile of 1005 grapevine (Vitis vinifera L.) accessions uncovers new synonymy and parentages, and reveals a large admixture amongst varieties of different geographic origin
    • Cipriani, G., et al. (2010). The SSR-based molecular profile of 1005 grapevine (Vitis vinifera L.) accessions uncovers new synonymy and parentages, and reveals a large admixture amongst varieties of different geographic origin. Theoretical and Applied Genetics, 121, 1569-1585.
    • (2010) Theoretical and Applied Genetics , vol.121 , pp. 1569-1585
    • Cipriani, G.1
  • 7
    • 75949087485 scopus 로고    scopus 로고
    • Selectivity and efficiency of different reversed-phase and mixed-mode sorbents to preconcentrate and isolate aroma molecules
    • Culleré, L., et al. (2010). Selectivity and efficiency of different reversed-phase and mixed-mode sorbents to preconcentrate and isolate aroma molecules. Journal of Chromatography A, 1217, 1557-1566.
    • (2010) Journal of Chromatography A , vol.1217 , pp. 1557-1566
    • Culleré, L.1
  • 8
    • 34248512719 scopus 로고    scopus 로고
    • Untargeted large-scale plant metabolomics using liquid chromatography coupled to mass spectrometry
    • De Vos, R. C., Moco, S., Lommen, A., Keurentjes, J. J., Bino, R. J., & Hall, R. D. (2007). Untargeted large-scale plant metabolomics using liquid chromatography coupled to mass spectrometry. Nature Protocols, 2, 778-791.
    • (2007) Nature Protocols , vol.2 , pp. 778-791
    • de Vos, R.C.1    Moco, S.2    Lommen, A.3    Keurentjes, J.J.4    Bino, R.J.5    Hall, R.D.6
  • 9
    • 56449108866 scopus 로고    scopus 로고
    • Methodology for profiling the steroid metabolome in animal tissues using ultraperformance liquid chromatography-electrospray-time-of-flight mass spectrometry
    • Flores-Valverde, A., & Hill, E. (2008). Methodology for profiling the steroid metabolome in animal tissues using ultraperformance liquid chromatography-electrospray-time-of-flight mass spectrometry. Analytical Chemistry, 80, 8771-8779.
    • (2008) Analytical Chemistry , vol.80 , pp. 8771-8779
    • Flores-Valverde, A.1    Hill, E.2
  • 10
    • 52449087246 scopus 로고    scopus 로고
    • Pre-analytical method for metabolic profiling of plant cell cultures of Passiflora garckei
    • Fraccaroli, M., Nicoletti, S., Maltese, F., Choi, Y., Guzzo, F., Levi, M., et al. (2008). Pre-analytical method for metabolic profiling of plant cell cultures of Passiflora garckei. Biotechnology Letters, 2008(30), 2031-2036.
    • (2008) Biotechnology Letters , vol.2008 , Issue.30 , pp. 2031-2036
    • Fraccaroli, M.1    Nicoletti, S.2    Maltese, F.3    Choi, Y.4    Guzzo, F.5    Levi, M.6
  • 11
    • 3242741850 scopus 로고    scopus 로고
    • Design of experiments: An efficient strategy to identify factors influencing extraction and derivatization of Arabidopsis thaliana samples in metabolomic studies with gas chromatography/mass spectrometry
    • Gullberg, J., Jonsson, P., Nordström, A., Sjöström, M., & Moritz, T. (2004). Design of experiments: An efficient strategy to identify factors influencing extraction and derivatization of Arabidopsis thaliana samples in metabolomic studies with gas chromatography/mass spectrometry. Analytical Biochemistry, 331, 283-295.
    • (2004) Analytical Biochemistry , vol.331 , pp. 283-295
    • Gullberg, J.1    Jonsson, P.2    Nordström, A.3    Sjöström, M.4    Moritz, T.5
  • 13
    • 72249107962 scopus 로고    scopus 로고
    • A comparison of metabolite extraction strategies for 1H-NMR-based metabolic profiling using mature leaf tissue from the model plant Arabidopsis thaliana
    • Kaiser, K. A., Barding, G. A., & Larive, C. K. (2009). A comparison of metabolite extraction strategies for 1H-NMR-based metabolic profiling using mature leaf tissue from the model plant Arabidopsis thaliana. Magnetic Resonance in Chemistry, 47, S147-S156.
    • (2009) Magnetic Resonance in Chemistry , vol.47
    • Kaiser, K.A.1    Barding, G.A.2    Larive, C.K.3
  • 14
    • 73349090880 scopus 로고    scopus 로고
    • Sample preparation for plant metabolomics
    • Kim, H., & Verpoorte, R. (2010). Sample preparation for plant metabolomics. Phytochemical Analysis, 21, 4-13.
    • (2010) Phytochemical Analysis , vol.21 , pp. 4-13
    • Kim, H.1    Verpoorte, R.2
  • 15
    • 77749320523 scopus 로고    scopus 로고
    • NMR-based metabolomic analysis of plants
    • Kim, H., Choi, Y., & Verpoorte, R. (2010). NMR-based metabolomic analysis of plants. Nature protocol, 5, 536-549.
    • (2010) Nature Protocol , vol.5 , pp. 536-549
    • Kim, H.1    Choi, Y.2    Verpoorte, R.3
  • 16
    • 44949181010 scopus 로고    scopus 로고
    • 1H NMR metabolite fingerprinting and metabolomic analysis of perchloric acid extracts from plant tissues
    • Kruger, N. J., Troncoso-Ponce, M. A., & Ratcliffe, R. G. (2008). 1H NMR metabolite fingerprinting and metabolomic analysis of perchloric acid extracts from plant tissues. Nature Protocol, 3, 1001-1012.
    • (2008) Nature Protocol , vol.3 , pp. 1001-1012
    • Kruger, N.J.1    Troncoso-Ponce, M.A.2    Ratcliffe, R.G.3
  • 17
    • 33947427846 scopus 로고    scopus 로고
    • Evaluation of metabolite extraction strategies from tissue samples using NMR metabolomics
    • Lin, C. Y., Wu, H., Tjeerdema, R. S., & Viant, M. R. (2007). Evaluation of metabolite extraction strategies from tissue samples using NMR metabolomics. Metabolomics, 3, 55-67.
    • (2007) Metabolomics , vol.3 , pp. 55-67
    • Lin, C.Y.1    Wu, H.2    Tjeerdema, R.S.3    Viant, M.R.4
  • 19
    • 77956586799 scopus 로고    scopus 로고
    • Optimization and evaluation of metabolite extraction protocols for untargeted metabolic profiling of liver samples by UPLC-MS
    • Masson, P., Alves, A. C., Ebbels, T. M. D., Nicholson, J. K., & Want, E. J. (2010). Optimization and evaluation of metabolite extraction protocols for untargeted metabolic profiling of liver samples by UPLC-MS. Analytical Chemistry, 82, 7779-7786.
    • (2010) Analytical Chemistry , vol.82 , pp. 7779-7786
    • Masson, P.1    Alves, A.C.2    Ebbels, T.M.D.3    Nicholson, J.K.4    Want, E.J.5
  • 20
    • 0345493734 scopus 로고    scopus 로고
    • Determination of indole-3-acetic acid, tryptophan and other indoles in must and wine by high-performance liquid chromatography with fluorescence detection
    • Mattivi, F., Vrhovsek, U., & Versini, G. (1999). Determination of indole-3-acetic acid, tryptophan and other indoles in must and wine by high-performance liquid chromatography with fluorescence detection. Journal of Chromatography A, 855, 227-235.
    • (1999) Journal of Chromatography A , vol.855 , pp. 227-235
    • Mattivi, F.1    Vrhovsek, U.2    Versini, G.3
  • 22
    • 65249146628 scopus 로고    scopus 로고
    • UPLC-MS-based analysis of human plasma for metabonomics using solvent precipitation or solid phase extraction
    • Michopoulos, F., Lai, L., Gika, H., Theodoridis, G., & Wilson, I. D. (2009). UPLC-MS-based analysis of human plasma for metabonomics using solvent precipitation or solid phase extraction. Journal of Proteome Research, 8, 2114-2121.
    • (2009) Journal of Proteome Research , vol.8 , pp. 2114-2121
    • Michopoulos, F.1    Lai, L.2    Gika, H.3    Theodoridis, G.4    Wilson, I.D.5
  • 24
    • 34548023950 scopus 로고    scopus 로고
    • Acidic acetonitrile for cellular metabolome extraction from Escherichiacoli
    • Rabinowitz, J. D., & Kimball, E. (2007). Acidic acetonitrile for cellular metabolome extraction from Escherichiacoli. Analytical Chemistry, 79, 6167-6173.
    • (2007) Analytical Chemistry , vol.79 , pp. 6167-6173
    • Rabinowitz, J.D.1    Kimball, E.2
  • 25
    • 77649186716 scopus 로고    scopus 로고
    • Analysis of skeletal muscle metabolome: Evaluation of extraction methods for targeted metabolite quantification using liquid chromatography tandem mass spectrometry
    • Rammouz, R. E., Létisse, F., Durand, S., Portais, J. C., Moussa, Z. W., & Fernandez, X. (2010). Analysis of skeletal muscle metabolome: Evaluation of extraction methods for targeted metabolite quantification using liquid chromatography tandem mass spectrometry. Analytical Biochemistry, 398, 169-177.
    • (2010) Analytical Biochemistry , vol.398 , pp. 169-177
    • Rammouz, R.E.1    Létisse, F.2    Durand, S.3    Portais, J.C.4    Moussa, Z.W.5    Fernandez, X.6
  • 26
    • 48749090666 scopus 로고    scopus 로고
    • Automated SPE-RP-HPLC fractionation of biofluids combined to off-line NMR spectroscopy for biomarker identification in metabonomics
    • Rezzi, S., Vera, F., Martin, F., Wang, S., Lawler, D., & Kochhar, S. (2008). Automated SPE-RP-HPLC fractionation of biofluids combined to off-line NMR spectroscopy for biomarker identification in metabonomics. Journal of Chromatography B, 871, 271-278.
    • (2008) Journal of Chromatography B , vol.871 , pp. 271-278
    • Rezzi, S.1    Vera, F.2    Martin, F.3    Wang, S.4    Lawler, D.5    Kochhar, S.6
  • 27
    • 79951480123 scopus 로고    scopus 로고
    • R Development Core Team, R Foundation for Statistical Computing. Austria: Vienna. ISBN 3-900051-07-0
    • R Development Core Team (2010). R: A language and environment for statistical computing. R Foundation for Statistical Computing. Austria: Vienna. ISBN 3-900051-07-0. http://www. R-project. org/.
    • (2010) R: A language and environment for statistical computing
  • 28
    • 37549064772 scopus 로고    scopus 로고
    • Simultaneous extraction of several metabolites of energy metabolism and related substances in mammalian cells: Optimization using experimental design
    • Ritter, J. B., Genzel, Y., & Reichl, U. (2008). Simultaneous extraction of several metabolites of energy metabolism and related substances in mammalian cells: Optimization using experimental design. Analytical Biochemistry, 373, 349-369.
    • (2008) Analytical Biochemistry , vol.373 , pp. 349-369
    • Ritter, J.B.1    Genzel, Y.2    Reichl, U.3
  • 29
    • 48749121080 scopus 로고    scopus 로고
    • A sample extraction and chromatographic strategy for increasing LC/MS detection coverage of the erythrocyte metabolome
    • Sana, T. R., Waddell, K., & Fischer, S. M. (2008). A sample extraction and chromatographic strategy for increasing LC/MS detection coverage of the erythrocyte metabolome. Journal of Chromatography B, 871, 314-321.
    • (2008) Journal of Chromatography B , vol.871 , pp. 314-321
    • Sana, T.R.1    Waddell, K.2    Fischer, S.M.3
  • 30
    • 74849138875 scopus 로고    scopus 로고
    • Global metabolic profiling of plant cell wall polysaccharide degradation by Saccharophagus degradans
    • Shin, M. H., Lee, D. Y., Skogerson, K., Wohlgemuth, G., Choi, I., Fiehn, O., et al. (2010a). Global metabolic profiling of plant cell wall polysaccharide degradation by Saccharophagus degradans. Biotechnology and Bioengineering, 105, 477-488.
    • (2010) Biotechnology and Bioengineering , vol.105 , pp. 477-488
    • Shin, M.H.1    Lee, D.Y.2    Skogerson, K.3    Wohlgemuth, G.4    Choi, I.5    Fiehn, O.6
  • 31
    • 77955133915 scopus 로고    scopus 로고
    • Evaluation of sampling and extraction methodologies for the global metabolic profiling of Saccharophagus degradans
    • Shin, M., Lee, D., Liu, K., Fiehn, O., & Kim, K. (2010b). Evaluation of sampling and extraction methodologies for the global metabolic profiling of Saccharophagus degradans. Analytical Chemistry, 82, 6660-6666.
    • (2010) Analytical Chemistry , vol.82 , pp. 6660-6666
    • Shin, M.1    Lee, D.2    Liu, K.3    Fiehn, O.4    Kim, K.5
  • 32
    • 32444446805 scopus 로고    scopus 로고
    • XCMS: Processing mass spectrometry data for metabolite profiling using nonlinear peak alignment, matching, and identification
    • Smith, C., Want, E., O'Maille, G., Abagyan, R., & Siuzdak, G. (2006). XCMS: Processing mass spectrometry data for metabolite profiling using nonlinear peak alignment, matching, and identification. Analytical Chemistry, 78, 779-787.
    • (2006) Analytical Chemistry , vol.78 , pp. 779-787
    • Smith, C.1    Want, E.2    O'Maille, G.3    Abagyan, R.4    Siuzdak, G.5
  • 33
    • 72049104846 scopus 로고    scopus 로고
    • Joint GC-MS and LC-MS platforms for comprehensive plant metabolomics: Repeatability and sample pre-treatment
    • t'Kindt, R., Morreel, K., Deforce, D., Boerjan, W., & van Bocxlaer, J. (2009). Joint GC-MS and LC-MS platforms for comprehensive plant metabolomics: Repeatability and sample pre-treatment. Journal of Chromatography B, 877, 3572-3580.
    • (2009) Journal of Chromatography B , vol.877 , pp. 3572-3580
    • t'Kindt, R.1    Morreel, K.2    Deforce, D.3    Boerjan, W.4    van Bocxlaer, J.5
  • 34
    • 60649089559 scopus 로고    scopus 로고
    • Highly sensitive feature detection for high resolution LC/MS
    • Tautenhahn, R., Bottcher, C., & Neumann, S. (2008). Highly sensitive feature detection for high resolution LC/MS. BMC Bioinformatics, 9, 504.
    • (2008) BMC Bioinformatics , vol.9 , pp. 504
    • Tautenhahn, R.1    Bottcher, C.2    Neumann, S.3
  • 35
    • 74549124767 scopus 로고    scopus 로고
    • Mechanical properties, phenolic composition and extractability indices of Barbera grapes of different soluble solids contents from several growing areas
    • Torchio, F., Cagnasso, E., Gerbi, V., & Rolle, L. (2010). Mechanical properties, phenolic composition and extractability indices of Barbera grapes of different soluble solids contents from several growing areas. Analytica Chimica Acta, 660, 183-189.
    • (2010) Analytica Chimica Acta , vol.660 , pp. 183-189
    • Torchio, F.1    Cagnasso, E.2    Gerbi, V.3    Rolle, L.4
  • 37
    • 41249098849 scopus 로고    scopus 로고
    • A high quality draft consensus sequence of the genome of a heterozygous grapevine variety
    • Velasco, R., Zharkikh, A., Troggio, M., Cartwright, D. A., Cestaro, A., Pruss, D., et al. (2007). A high quality draft consensus sequence of the genome of a heterozygous grapevine variety. PLoS ONE, 2, e1326.
    • (2007) PLoS ONE , vol.2
    • Velasco, R.1    Zharkikh, A.2    Troggio, M.3    Cartwright, D.A.4    Cestaro, A.5    Pruss, D.6
  • 38
    • 84889475179 scopus 로고    scopus 로고
    • Sampling and sample preparation
    • S. G. Villas-Bôas, U. Roessner, M. A. E. Hansen, J. Smedsgaard, and J. Nielsen (Eds.), New York: Wiley
    • Villas-Bôas, S. G. (2006). Sampling and sample preparation. In S. G. Villas-Bôas, U. Roessner, M. A. E. Hansen, J. Smedsgaard, & J. Nielsen (Eds.), Metabolome Analysis: An Introduction (pp. 39-82). New Jersey: Hoboken.
    • (2006) Metabolome Analysis: An Introduction , pp. 39-82
    • Villas-Bôas, S.G.1
  • 39
    • 28044440100 scopus 로고    scopus 로고
    • Global metabolite analysis of yeast: evaluation of sample preparation methods
    • Villas-Boas, S., Hojer-Pedersen, J., Akesson, M., Smedsgaard, J., & Nielsen, J. (2005a). Global metabolite analysis of yeast: evaluation of sample preparation methods. Yeast, 22, 1155-1169.
    • (2005) Yeast , vol.22 , pp. 1155-1169
    • Villas-Boas, S.1    Hojer-Pedersen, J.2    Akesson, M.3    Smedsgaard, J.4    Nielsen, J.5
  • 42
    • 36148989929 scopus 로고    scopus 로고
    • High-throughput tissue extraction protocol for NMR-and MS-based metabolomics
    • Wu, H., Southam, A. D., Hines, A., & Viant, M. R. (2008). High-throughput tissue extraction protocol for NMR-and MS-based metabolomics. Analytical Biochemistry, 372, 204-212.
    • (2008) Analytical Biochemistry , vol.372 , pp. 204-212
    • Wu, H.1    Southam, A.D.2    Hines, A.3    Viant, M.R.4


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