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Volumn 214, Issue , 2012, Pages 281-288

Emulsion droplet sizing using low-field NMR with chemical shift resolution and the block gradient pulse method

Author keywords

Bench top spectrometer; Chemical shift; Emulsions; Micro coils; PFG

Indexed keywords

DISPERSED DROPLETS; EMULSION DROPLETS; GAUSSIANS; LIQUID PHASE; LOW-FIELD NMR; MICROCOILS; NMR MAGNETS; NUMERICAL INVERSION; PFG; PHASE DISTRIBUTION; PULSE METHODS; PULSED FIELD GRADIENTS; SELF-DIFFUSION; SIGNAL SELECTION;

EID: 84855676562     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2011.11.020     Document Type: Article
Times cited : (51)

References (41)
  • 1
    • 71949085714 scopus 로고    scopus 로고
    • Characterization of food emulsions by PFG NMR
    • M.A. Voda, and J. van Duynhoven Characterization of food emulsions by PFG NMR Trends. Food Sci. Tech. 20 2009 533 543
    • (2009) Trends. Food Sci. Tech. , vol.20 , pp. 533-543
    • Voda, M.A.1    Van Duynhoven, J.2
  • 2
    • 0001446519 scopus 로고
    • Characterization of water-in-crude oil emulsions by the NMR self-diffusion technique
    • B. Balinov, O. Urdahl, O. Söderman, and J. Sjöblom Characterization of water-in-crude oil emulsions by the NMR self-diffusion technique Colloid Surface A 82 1994 173 181
    • (1994) Colloid Surface A , vol.82 , pp. 173-181
    • Balinov, B.1    Urdahl, O.2    Söderman, O.3    Sjöblom, J.4
  • 4
    • 0030293744 scopus 로고    scopus 로고
    • Effect of droplet size on rheology of emulsions
    • R. Pal Effect of droplet size on rheology of emulsions AICHE J. 42 1996 3181 3190
    • (1996) AICHE J. , vol.42 , pp. 3181-3190
    • Pal, R.1
  • 5
    • 0040610948 scopus 로고    scopus 로고
    • Composite structure formation in whey protein stabilized O/W emulsions. I. Influence of the dispersed phase on viscoelastic properties
    • PII S0268005X99000132
    • C.K. Reiffers-Magnani, J.L. Cuq, and H.J. Watzke Composite structure formation in whey protein stabilised o/w emulsions I. Influence of the dispersed phase on viscoelastic properties Food Hydrocolloids 13 1999 303 316 (Pubitemid 129499466)
    • (1999) Food Hydrocolloids , vol.13 , Issue.4 , pp. 303-316
    • Reiffers-Magnani, C.K.1    Cuq, J.L.2    Watzke, H.J.3
  • 6
    • 35349018463 scopus 로고    scopus 로고
    • Critical review of techniques and methodologies for characterization of emulsion stability
    • DOI 10.1080/10408390701289292, PII 783061133
    • D.J. McClements Critical review of techniques and methodologies for characterization of emulsion stability Crit. Rev. Food Sci. Nutr. 47 2007 611 649 (Pubitemid 47613322)
    • (2007) Critical Reviews in Food Science and Nutrition , vol.47 , Issue.7 , pp. 611-649
    • McClements, D.J.1
  • 7
    • 36849100445 scopus 로고
    • Restricted self-diffusion of protons in colloidal systems by the pulsed-gradient, spin-echo method
    • J.E. Tanner, and E.O. Stejskal Restricted self-diffusion of protons in colloidal systems by the pulsed-gradient, spin-echo method J. Chem. Phys. 49 1968 1768 1777
    • (1968) J. Chem. Phys. , vol.49 , pp. 1768-1777
    • Tanner, J.E.1    Stejskal, E.O.2
  • 8
    • 36849115486 scopus 로고
    • Self-diffusion coefficient of liquid lithium
    • J.S. Murday, and R.M. Cotts Self-diffusion coefficient of liquid lithium The J. Chem. Phys. 48 1968 4938 4945
    • (1968) The J. Chem. Phys. , vol.48 , pp. 4938-4945
    • Murday, J.S.1    Cotts, R.M.2
  • 9
    • 49649143174 scopus 로고
    • Pulsed NMR studies of restricted diffusion. I. Droplet size distributions in emulsions
    • K.J. Packer, and C. Rees Pulsed NMR studies of restricted diffusion. I. Droplet size distributions in emulsions J. Colloid Interface Sci. 40 1972 206 218
    • (1972) J. Colloid Interface Sci. , vol.40 , pp. 206-218
    • Packer, K.J.1    Rees, C.2
  • 12
    • 0029230004 scopus 로고
    • Determination of water droplet size distributions by low resolution PFG-NMR II. "solid" emulsions
    • I. Fourel, J.P. Guillement, and D. Le Botlan Determination of water droplet size distributions by low resolution PFG-NMR II. "Solid" emulsions J. Colloid Interface Sci. 169 1995 119 124
    • (1995) J. Colloid Interface Sci. , vol.169 , pp. 119-124
    • Fourel, I.1    Guillement, J.P.2    Le Botlan, D.3
  • 14
    • 0035879601 scopus 로고    scopus 로고
    • Measurement of oil droplet size distributions in food oil/water emulsions by time domain pulsed field gradient NMR
    • DOI 10.1006/jcis.2001.7603
    • G.J.W. Goudappel, J.P.M. van Duynhoven, and M.M.W. Mooren Measurement of oil droplet size distributions in food oil/water emulsions by time domain pulsed field gradient NMR J. Colloid Interface Sci. 239 2001 535 542 (Pubitemid 32641925)
    • (2001) Journal of Colloid and Interface Science , vol.239 , Issue.2 , pp. 535-542
    • Goudappel, G.J.W.1    Van Duynhoven, J.P.M.2    Mooren, M.M.W.3
  • 15
    • 11144220881 scopus 로고    scopus 로고
    • Evaluation of the precision of drop-size determination in oil/water emulsions by low-resolution NMR spectroscopy
    • DOI 10.1021/la048649v
    • P.S. Denkova, S. Tcholakova, N.D. Denkova, K.D. Danov, B. Campbell, C. Shawl, and D. Kim Evaluation of the precision of drop-size determination in oil/water emulsions by low resolution NMR spectroscopy Langmuir 20 2004 11402 11413 (Pubitemid 40049611)
    • (2004) Langmuir , vol.20 , Issue.26 , pp. 11402-11413
    • Denkova, P.S.1    Tcholakova, S.2    Denkov, N.D.3    Danov, K.D.4    Campbell, B.5    Shawl, C.6    Kim, D.7
  • 17
    • 0043195730 scopus 로고    scopus 로고
    • Enhanced characterization of oilfield emulsions via NMR diffusion and transverse relaxation experiments
    • A. Pena, and G.J. Hirsaki Enhanced characterization of oilfield emulsions via NMR diffusion and transverse relaxation experiments Adv. Colloid Interface Sci. 105 2003 103 150
    • (2003) Adv. Colloid Interface Sci. , vol.105 , pp. 103-150
    • Pena, A.1    Hirsaki, G.J.2
  • 18
    • 33947144131 scopus 로고    scopus 로고
    • Effect of processing on droplet cluster structure in emulsion gels
    • DOI 10.1016/j.foodhyd.2006.09.012, PII S0268005X0600230X
    • A. Bot, F.P. Duval, and W.G. Bouwman Effect of processing on droplet cluster structure in emulsion gels Food Hydrocolloids 21 2007 844 854 (Pubitemid 46400948)
    • (2007) Food Hydrocolloids , vol.21 , Issue.5-6 , pp. 844-854
    • Bot, A.1    Duval, F.P.2    Bouwman, W.G.3
  • 20
    • 7444261918 scopus 로고    scopus 로고
    • Resolving chemical shift spectra with a low-field NMR relaxometer
    • L. Grunin, and B. Blümich Resolving chemical shift spectra with a low-field NMR relaxometer Chem. Phys. Lett. 397 2004 306 308
    • (2004) Chem. Phys. Lett. , vol.397 , pp. 306-308
    • Grunin, L.1    Blümich, B.2
  • 21
    • 34548435692 scopus 로고    scopus 로고
    • NMR survey of reflected Brownian motion
    • DOI 10.1103/RevModPhys.79.1077
    • D.S. Grebenkov NMR Survey of reflected Brownian motion Rev. Modern Phys. 79 2007 1077 1137 (Pubitemid 47357951)
    • (2007) Reviews of Modern Physics , vol.79 , Issue.3 , pp. 1077-1137
    • Grebenkov, D.S.1
  • 22
    • 54949083869 scopus 로고    scopus 로고
    • Laplacian eigenfunctions in NMR. I. A numerical tool
    • D.S. Grebenkov Laplacian eigenfunctions in NMR. I. A numerical tool Concepts Mag. Reson. A 32A 2008 277 301
    • (2008) Concepts Mag. Reson. A , vol.32 A , pp. 277-301
    • Grebenkov, D.S.1
  • 23
    • 77952058428 scopus 로고    scopus 로고
    • Laplacian eigenfunctions in NMR. II. Theoretical advances
    • D.S. Grebenkov Laplacian eigenfunctions in NMR. II. Theoretical advances Concepts Mag. Reson. A 34A 2009 264 296
    • (2009) Concepts Mag. Reson. A , vol.34 A , pp. 264-296
    • Grebenkov, D.S.1
  • 24
    • 33646376290 scopus 로고
    • Spin diffusion measurements: Spin echoes in the presence of a time-dependent field gradient
    • E.O. Stejskal, and J.E. Tanner Spin diffusion measurements: spin echoes in the presence of a time-dependent field gradient J. Chem. Phys. 42 1965 288 292
    • (1965) J. Chem. Phys. , vol.42 , pp. 288-292
    • Stejskal, E.O.1    Tanner, J.E.2
  • 25
    • 0002152987 scopus 로고    scopus 로고
    • A multiple-narrow-pulse approximation for restricted diffusion in a time-varying field gradient
    • A. Caprihan, L.Z. Wang, and E. Fukushima A multiple-narrow-pulse approximation for restricted diffusion in a time-varying field gradient J. Magn. Reson. 118 1996 94 102 (Pubitemid 126751678)
    • (1996) Journal of Magnetic Resonance - Series A , vol.118 , Issue.1 , pp. 94-102
    • Caprihan, A.1    Wang, L.Z.2    Fukushima, E.3
  • 26
    • 0001887257 scopus 로고    scopus 로고
    • A simple matrix formalism for spin echo analysis of restricted diffusion under generalized gradient waveforms
    • P.T. Callaghan A simple matrix formalism for spin echo analysis of restricted diffusion under generalized gradient waveforms J. Magn. Reson. 129 1997 74 84 (Pubitemid 127454055)
    • (1997) Journal of Magnetic Resonance , vol.129 , Issue.1 , pp. 74-84
    • Callaghan, P.T.1
  • 27
    • 1942509464 scopus 로고    scopus 로고
    • Spin echo analysis of restricted diffusion under generalized gradient waveforms for spherical pores with relaxivity and interconnections
    • DOI 10.1560/JF3Q-URL3-5U20-WHLY
    • B.N. Ryland, and P.T. Callaghan Spin echo analysis of restricted diffusion under generalized gradient waveforms for spherical pores with relaxivity and interconnections Israel J. Chem. 43 2003 1 7 (Pubitemid 38497126)
    • (2003) Israel Journal of Chemistry , vol.43 , Issue.1-2 , pp. 1-7
    • Ryland, B.N.1    Callaghan, P.T.2
  • 28
    • 36149003638 scopus 로고
    • Bloch equations with diffusion terms
    • H.C. Torrey Bloch equations with diffusion terms Phys. Rev. 104 1956 563
    • (1956) Phys. Rev. , vol.104 , pp. 563
    • Torrey, H.C.1
  • 29
    • 0033170464 scopus 로고    scopus 로고
    • Theory of Spin Echo in Restricted Geometries under a Step-wise Gradient Pulse Sequence
    • A.V. Barzykin Theory of spin echo in restricted geometries under a step-wise gradient pulse sequence J. Magn. Reson. 139 1999 342 353 (Pubitemid 129608873)
    • (1999) Journal of Magnetic Resonance , vol.139 , Issue.2 , pp. 342-353
    • Barzykin, A.V.1
  • 30
    • 0037440825 scopus 로고    scopus 로고
    • Measurement of emulsion droplet sizes using PFG NMR and regularization methods
    • DOI 10.1016/S0021-9797(02)00131-5
    • K.G. Hollingsworth, and M.L. Johns Measurement of emulsion droplet sizes using PFG NMR and regularization methods J. Colloid Interface Sci. 258 2003 383 389 (Pubitemid 36293371)
    • (2003) Journal of Colloid and Interface Science , vol.258 , Issue.2 , pp. 383-389
    • Hollingsworth, K.G.1    Johns, M.L.2
  • 31
    • 34548394118 scopus 로고    scopus 로고
    • Operating nanoliter scale NMR microcoils in a 1 tesla field
    • DOI 10.1016/j.jmr.2007.06.008, PII S1090780707002005
    • A.F. McDowell, and N.L. Adolphi Operating nanoliter scale NMR microcoils in a 1 tesla field J. Magn. Reson. 188 2007 74 82 (Pubitemid 47369680)
    • (2007) Journal of Magnetic Resonance , vol.188 , Issue.1 , pp. 74-82
    • McDowell, A.F.1    Adolphi, N.L.2
  • 34
    • 84855641878 scopus 로고    scopus 로고
    • http://www.malvern.com/labeng/products/morphologi/particle-image- analyzer.htm.
  • 35
    • 43949165008 scopus 로고
    • The NMR self-diffusion method applied to restricted diffusion. Simulation of echo attenuation from molecules in spheres and between planes
    • B. Balinov, B. Jönsson, P. Linse, and O. Söderman The NMR self-diffusion method applied to restricted diffusion. Simulation of echo attenuation from molecules in spheres and between planes J. Magn. Reson. 104 1993 17 25
    • (1993) J. Magn. Reson. , vol.104 , pp. 17-25
    • Balinov, B.1    Jönsson, B.2    Linse, P.3    Söderman, O.4
  • 36
    • 0033200283 scopus 로고    scopus 로고
    • Flow and dispersion in porous media: Lattice-Boltzmann and NMR studies
    • B. Manz, L.F. Gladden, and P.B. Warren Flow and dispersion in porous media: lattice-Boltzmann and NMR studies ALCHE J. 45 1999 1845 1854 (Pubitemid 29446520)
    • (1999) AIChE Journal , vol.45 , Issue.9 , pp. 1845-1854
    • Manz, B.1    Gladden, L.F.2    Warren, P.B.3
  • 37
    • 14844289204 scopus 로고
    • Self-diffusion coefficients and rotational correlation times in polar liquids. III. Toluene
    • D.E. O'Reilly, and E.M. Peterson Self-diffusion coefficients and rotational correlation times in polar liquids. III. Toluene J. Chem. Phys. 56 1972 2262 2266
    • (1972) J. Chem. Phys. , vol.56 , pp. 2262-2266
    • O'Reilly, D.E.1    Peterson, E.M.2
  • 38
    • 0035744199 scopus 로고    scopus 로고
    • Difftrain: A novel approach to a true spectroscopic single-scan diffusion measurement
    • J.P. Stamps, B. Ottink, J.M. Visser, J.P.M. van Duynhoven, and R. Hulst Difftrain: a novel approach to a true spectroscopic single-scan diffusion measurement J. Magn. Reson. 151 2001 28 31
    • (2001) J. Magn. Reson. , vol.151 , pp. 28-31
    • Stamps, J.P.1    Ottink, B.2    Visser, J.M.3    Van Duynhoven, J.P.M.4    Hulst, R.5


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