Rapid determination of piperazine-type stimulants in human urine by microextraction in packed sorbent after method optimization using a multivariate approach

Journal of Chromatography A

Volumn 1222, Issue , 2012, Pages 116-120

  Moreno, I E D ^a   da Fonseca, B M ^a   Magalhaes A R ^a   Geraldes, V S ^a   Queiroz, J A ^a   Barroso, M ^b   Costa, S ^b   Gallardo, E ^a  

^a UNIVERSITY OF BEIRA INTERIOR   (Portugal)

^b INSTITUTO NACIONAL DE MEDICINA LEGAL E CIÊNCIAS FORENSES   (Portugal)

Author keywords

Factorial design; Microextraction by packed sorbent; Piperazines; Urine

Indexed keywords

ANALYTES; DETERMINATION COEFFICIENTS; ENDOGENOUS SUBSTANCES; FACTORIAL DESIGN; FORENSIC TOXICOLOGY; FRACTIONAL FACTORIAL DESIGNS; FREEZE/THAW CYCLES; HUMAN URINE; INFLUENCING FACTOR; LIQUID CHROMATOGRAPHY-DIODE ARRAY DETECTION; LOWER LIMIT OF QUANTITATIONS; MICROEXTRACTION; MULTIVARIATE APPROACH; PIPERAZINES; RAPID DETERMINATION; ROOM TEMPERATURE; ROUTINE ANALYSIS; SAMPLE DILUTION; SHORT PERIODS; URINE; URINE SAMPLE;

BODY FLUIDS; LIQUID CHROMATOGRAPHY; METHANOL; OPTIMIZATION; ORGANIC SOLVENTS; SCREENING; SORBENTS; SORPTION;

PIPE;

(3 CHLOROPHENYL)PIPERAZINE; 1 (3 TRIFLUOROMETHYLPHENYL)PIPERAZINE; 1 (4 METHOXYPHENYL)PIPERAZINE; ALCOHOL; PIPERAZINE; SOLVENT; SORBENT; UNCLASSIFIED DRUG;

ARTICLE; CALIBRATION; CONTROLLED STUDY; DIODE; DRUG DETERMINATION; DRUG ISOLATION; EXTRACTION; FACTORIAL DESIGN; FORENSIC TOXICOLOGY; FREEZE THAWING; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MICROEXTRACTION BY PACKED SORBENT; PRIORITY JOURNAL; PROCESS OPTIMIZATION; ROOM TEMPERATURE; THERMOSTABILITY; URINALYSIS;

CALIBRATION; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, LIQUID; DRUG STABILITY; HUMANS; MULTIVARIATE ANALYSIS; PIPERAZINES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SEROTONIN RECEPTOR AGONISTS; STREET DRUGS;

EID: 84855577615     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.12.016     Document Type: Article

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