Analysis of phenylpiperazine-like stimulants in human hair as trimethylsilyl derivatives by gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 40, 2010, Pages 6274-6280

  Barroso, M ^a   Costa, S ^a   Dias, M ^a   Vieira, D N ^a   Queiroz, J A ^b   Lopez Rivadulla M ^c  

^a INSTITUTO NACIONAL DE MEDICINA LEGAL E CIÊNCIAS FORENSES   (Portugal)

^b UNIVERSITY OF BEIRA INTERIOR   (Portugal)

^c Instituto de Medicina Legal   (Spain)

Author keywords

GC MS; Hair; Piperazines

Indexed keywords

ANALYTES; BIOANALYTICAL METHODS; CORRELATION COEFFICIENT; FORENSIC TOXICOLOGY; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC/MS; HAIR; HUMAN HAIR; INTERNAL STANDARDS; LOWER LIMIT OF QUANTITATIONS; MIXED-MODE SOLID-PHASE EXTRACTION; PIPERAZINES; QUALITATIVE AND QUANTITATIVE ANALYSIS; ROUTINE ANALYSIS; SAMPLE CLEAN-UP; SELECTED ION MONITORING; SODIUM HYDROXIDES; TRIFLUOROACETAMIDES; TRIMETHYLCHLOROSILANES; TRIMETHYLSILYL; TRIMETHYLSILYL DERIVATIVES;

CHEMICAL ANALYSIS; EXTRACTION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY;

QUALITY CONTROL;

(3 CHLOROPHENYL)PIPERAZINE; 1 (3 TRIFLUOROMETHYLPHENYL)PIPERAZINE; 1 (4 METHOXYPHENYL)PIPERAZINE; CHLOROTRIMETHYLSILANE; PIPERAZINE DERIVATIVE; SODIUM HYDROXIDE; TRIFLUOROACETAMIDE DERIVATIVE; TRIMETHYLSILYL DERIVATIVE; UNCLASSIFIED DRUG;

ACCURACY; ACETYLATION; ARTICLE; CALIBRATION; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; CONTROLLED STUDY; CORRELATION COEFFICIENT; DERIVATIZATION; HAIR ANALYSIS; HUMAN; MASS FRAGMENTOGRAPHY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; SOLID PHASE EXTRACTION; STEREOCHEMISTRY;

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HAIR; HUMANS; LEAST-SQUARES ANALYSIS; PIPERAZINES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TRIMETHYLSILYL COMPOUNDS;

EID: 77956651160     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.08.001     Document Type: Article

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