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Upon heating 1:1 or 1:2 mixtures of 9a and indole neat for 4 h at 140-160 °C, he obtained the corresponding bis-indolylmethane for which he reported a melting point of 97 °C. For comparison, compound 11a melts between 119-120 °C For leading references on the Friedländer reaction, see
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See also ref. 10 Products, 6b, 11i, 11p and 17 were characterized by X-ray crystallography; see ESI for details
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