Determination of geosmin and 2-methylisoborneol in water by headspace liquid-phase microextraction coupled with gas chromatography-mass spectrometry

Analytical Letters

Volumn 44, Issue 8, 2011, Pages 1544-1557

  Ma, Jiping ^a   Lu, Wenhui ^a,b   Li, Jinhua ^b   Song, Zhiwen ^a   Liu, Dongyan ^b   Chen, Lingxin ^b  

^a QINGDAO TECHNOLOGICAL UNIVERSITY   (China)

^b YANTAI INSTITUTE OF COASTAL ZONE RESEARCH   (China)

Author keywords

Gas chromatography mass spectrometry; Geosmin; Headspace liquid phase microextraction; 2 methylisoborneol; Single drop microextraction; Water samples

Indexed keywords

EID: 79959253266     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032719.2010.520384     Document Type: Article

References (30)

1. Benanou, D., F. Acobas, and D. M. R. Roubin. 2003. Analysis of off-flavors in the aquatic nvironment by stir bar sorptive extraction-thermal desorption-capillary GC/MS/ lfactometry. Anal. Bioanal. Chem. 376: 69-77.
2. Bruchet, A. 1999. Solved and unsolved cases of taste and odor episodes in the files of Inspector luzeau. Water Sci. Technol. 40: 15-22.
3. Fontana, A. R., R. G. Wuilloud, L. D. Martínez, and J. C. Altamirano. 2009. Simple pproach based on ultrasound-assisted emulsification-microextraction for determination f polibrominated flame retardants in water samples by gas chromatography-mass spectrometry. Chromatogr. A 1216: 147-153.
4. Gagné, F., J. Ridal, C. Blaise, and B. Brownlee. 1999. Toxicological effects of geosmin and 2-methylisoborneol on rainbow trout hepatocytes. Bull. Environ. Contam. Toxicol. 3: 174-180.
5. George, J. E., G. Payne, and D. Conn. 1997. Cost-effective low-level detection of geosmin and IB in water by large volume purge and trap GC/MS. Proceedings of American Water orks Association. Water Quality Technology Conference, November 9-12, Denver, CO.
6. Harmon, A. D. 1997. In Techniques for Analyzing Food Aroma, ed. R. Marsili. 81. New York: arcel Dekker.
7. He, Y., and H. K. Lee. 1997. Liquid-phase microextraction in a single drop of organic solvent y using a conventional microsyringe. Anal. Chem. 69: 4634-4640.
8. Huang, W. J., C. H. Lai, and Y. L. Cheng. 2007. Evaluation of extracellular products and utagenicity in cyanobacteria cultures separated from a eutrophic reservoir. Sci. Total nviron. 377: 214-223.
9. Jensen, S. E., C. L. Anders, L. J. Goatcher, and S. E. Hrudey. 1994. Actinomycetes as a factor in odour problems affecting drinking water from the North Saskatchewan River. Water es. 28: 1393-1401.
10. Kataoka, H., H. L. Lord, and J. Pawliszyn. 2000. Applications of solid-phase microextraction in food analysis. J. Chromatogr. A 880: 35-62.
11. Krasner, S. W., C. J. H. Wang, and M. J. Mcguire. 1981. Development of a closed-loop stripping technique for the analysis of taste-and odor-causing substances in drinking water. In Advances in the Identification and Analysis of Organic Pollutants in Water. Vol. 12, ed., L. H. Keith. AnnArbor, MI: Ann Arbor Science Publishers, Inc.
12. Lu, W. H., J. P. Ma, R. H. Xiao, and S. W. Zhu. 2009. Progress in pretreatment techniques for analysis on odorous compounds in environmental water. J. Instru. Anal. 28(5): 621-626.
13. Mallevialle, J., and I. H. Suffet, eds. 1987. Identification and Treatment of Tastes and Odors in Drinking Water. Denver, CO: American water works association research foundation/lyonnaise des Eaux, AWWA.
14. Nakamura, S., and N. Nakamura. 2001. Determination of 2-methylisoborneol and geosmin in water by gas chromatography-mass spectrometry using stir bar sorptive extraction. J. Sep. Sci. 24: 674-677.
15. Palmentier, J. P. F. P., V. Y. Taguchi, and S. W. D. Jenkins. 1998. The determination of geosmin and 2-methylisoborneol in water using isotope dilution high resolution mass spectrometry. Water Res. 32: 287-294.
16. Pawliszyn, J. 1997. Solid Phase Microextraction-Theory and Practice. New York: Wiley-VCH.
17. Psillakis, E., and N. Kalogerakis. 2002. Developments in single-drop microextraction. TrAC Trends Anal. Chem. 21: 54-64.
18. Saito, K., K. Okamura, and H. Kataoka. 2008. Determination of musty odorants, 2-methylisoborneol and geosmin, in environmental water by headspace solid-phase microextraction and gas chromatography-mass spectrometry. J. Chromatogr. A 1186: 434-437.
19. Salemi, A., S. Lacorte, and H. Bagheri. 2006. Automated trace determination of earthy-musty odorous compounds in water samples by on-line purge-and-trap-gas chromatography-mass spectrometry. J. Chromatogr. A 1136: 170-175.
20. Schrader, K. K., and M. E. Dennis. 2005. Cyanobacteria and earthy/musty compounds found in commercial catfish (Ictalurus punctatus) ponds in the Mississippi Delta and Mississippi-Alabama Blackland Prairie. Water Res. 39: 2807-2814.
21. Shin, H. S., and H. S. Ahn. 2000. Simple, rapid, and sensitive determination of odorous compounds in water by GC-MS. Chromatographia 59: 107-113.
22. Sung, Y. H., T. Y. Li, and S. D. Huang. 2005. Analysis of earthy and musty odors in water samples by solid-phase microextraction coupled with gas chromatogyaphy/ion trap mass spectrometry. Talanta 65: 518-524.
23. Tankeviciute, A., R. Kazlauskas, and V. Vickackaite. 2001. Headspace extraction of alcohols into a single drop. Analyst 126: 1674-1677.
24. Uwins, H. K., P. Teasdale, and H. Stratton. 2007. A case study investigating the occurrence of geosmin and 2-methylisoborneol (MIB) in the surface waters of the Hinze Dam, Gold Coast, Australia. Water Sci. Technol. 55: 231-238.
25. Watson, S. B., J. Ridal, B. Zaitlin, and A. Lo. 2003. Odours from pulp mill effluent treatment ponds: The origin of sifnificant levels of geosmin and 2-methylisoborneol (MIB). Chemosphere 51: 765-773.
26. Xie, Y. Q., J. He, and J. Huang. 2007. Determination of 2-methylisoborneol and geosmin produced by streptomyces sp. And Anabaena PCC7120. J. Agric. Food Chem. 55: 6823-6828.
27. Xu, L., C. Basheer, and H. K. Lee. 2007. Developments in single-drop microextraction. J. Chromatogr. A 1152: 184-192.
28. Zander, A. K., and P. Pingert. 1997. Membrane-based extraction for detection of tastes and odors in water. Water Res. 31: 301-309.
29. Zhang, L. F., R. K. Hu, and Z. G. Yang. 2005. Simultaneous picogram determination of "earthy-musty" odorous compounds in water using solid-phase microextraction and gas chromatography-mass spectrometry coupled with initial cool programmable temperature vaporizer inlet. J. Chromatogr. A 1098: 7-13.
30. Zhang, L. F., R. K. Hu, and Z. G. Yang. 2006. Routine analysis of off-flavor compounds in water at sub-part-per-trillion level by large-volume injection GC/MS with programmable temperature vaporizing inlet. Water Res. 40: 699-709.