Assessment of the chemical and enantiomeric purity of organic reference materials

TrAC - Trends in Analytical Chemistry

Volumn 30, Issue 4, 2011, Pages 628-640

  Yip, Yiu chung ^a   Wong, Siu kay ^a   Choi, Sik man ^b  

^a Homantin Government Offices   (Hong Kong)

^b Food and Environmental Hygiene Department   (Hong Kong)

Author keywords

Chemical purity; Differential scanning calorimetry; Enantiomeric purity; Gas chromatography; Inductively coupled plasma mass spectrometry; Ion chromatography; Karl Fischer titration; Liquid chromatography; Organic reference material; Quantitative nuclear magnetic resonance

Indexed keywords

CHEMICAL PURITY; ENANTIOMERIC PURITY; KARL FISCHER TITRATION; ORGANIC REFERENCE MATERIAL; QUANTITATIVE NUCLEAR MAGNETIC RESONANCE;

CAPILLARY ELECTROPHORESIS; DIFFERENTIAL SCANNING CALORIMETRY; ENANTIOMERS; GAS CHROMATOGRAPHY; IMPURITIES; INDUCTIVELY COUPLED PLASMA; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; ION CHROMATOGRAPHY; LIQUIDS; MOISTURE DETERMINATION; NUCLEAR MAGNETIC RESONANCE; PRINCIPAL COMPONENT ANALYSIS; RATING; RESONANCE; SPECTROMETRY; TITRATION; WATER CONTENT;

CHEMICAL ANALYSIS;

ORGANIC COMPOUND;

ACCREDITATION; CHEMICAL ANALYSIS; COULOMETRY; DIFFERENTIAL SCANNING CALORIMETRY; ENANTIOMER; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MATERIAL STATE; MOISTURE; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REVIEW; STANDARD; TITRIMETRY; VALIDATION PROCESS; WATER CONTENT;

EID: 79952900989     PISSN: 01659936     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.trac.2010.12.003     Document Type: Review

References (80)

1. NMIs and other designated institutes, CIPM/2005-07 (). http://www.bipm.org/en/cipm-mra/documents/.
2. Improving worldwide traceability and acceptance of measurements carried out within the CIPM MRA and the ILAC arrangement (). http://www.bipm.org/en/cipm-mra/cipm-ilac_joint_statement.html.
3. Calibration and measurement capabilities in the context of the CIPM MRA, CIPM MRA-D-04, Version 1, 2008 (). http://www.bipm.org/en/cipm-mra/documents/.
4. L. Mackay - Final report CCQM-P20a (Organic purity assessment series: P20a tributyltin chloride), 2002, OAWG archive document OAWG/-13.
5. S. Westwood - Final study report CCQM-P20.c.1 & P20.c.2 (Purity of atrazine), 2005, OAWG archive document OAWG/-18.
6. S. Westwood, Final study report CCQM-P20.d (Purity of chlorpyrifos), 2005, OAWG archive document OAWG/-19.
7. Westwood S., Josephs R., Daireaux A., Wielgosz R., Davies S., Kang M., Ting H., Phillip R., Malz F., Shimizu Y., Frias E., Pérez M., Apps P., Fernandes-Whaley M., De Vos B., Wiangnon K., Ruangrittinon N., Wood S., Duewer D., Schantz M., Bedner M., Hancock D., Esker J. Metrologia 2009, 46:08019.
8. Draft A summary report CCQM-P20.f (Digoxin), 2009, OAWG document OAWG/09-07.
9. Preliminary result summary CCQM-K55.a/CCQM-P117.a (17β-Estradiol), 2009, OAWG document OAWG/09-06.
10. International Organization for Standardization (ISO), Revision of Definitions for Reference Material and Certified Reference Material, ISO Guide 30:1992/Amd 1:2008, ISO, Geneva, Switzerland, 2008.
11. NIST Special Publication 1012: An approach to the metrologically sound traceable assessment of the chemical purity of organic reference materials 2004, NIST, Gaithersburg, MD, USA. D.L. Duewer, R.M. Parris, E. White, W.E. May, H. Elbaum (Eds.).
12. Le Goff T., Mazlum S., Wood S. Fuel 2009, 88:2025.
13. Yasueda S.-I., Higashiyama M., Shirasaki Y., Inada K., Ohtori A. J. Pharm. Biomed. Anal. 2004, 36:309.
14. King B., Westwood S. Fresenius' J. Anal. Chem. 2001, 370:194.
15. Saito T., Iwasawa R., Ihara T., Kinugasa S., Nomura A., Maeda T. Chromatography 2003, 24:117.
16. Elipe M.V.S. Anal. Chim. Acta 2003, 497:1.
17. Le Goff T., Wood S. Anal. Bioanal. Chem. 2008, 391:2035.
18. Kim D.-H., Chang J.-K., Sohn H.-J., Cho B.-G., Ko S.-R., Nho K.-B., Jang D.-S., Lee S.-M. Accred. Qual. Assur. 2010, 15:81.
19. Górecki T., Lynen F., Szucs R., Sandra P. Anal. Chem. 2006, 78:3186.
20. Welzig E., Drs E., Josephs R.D., Schothorst R.C., van Egmond H.P., Pettersson H., Chan D., Krska R. Mycotox. Res. 2005, 21:224.
21. Rizzo V., Pinciroli V. J. Pharm. Biomed. Anal. 2005, 38:851.
22. Wells R.J., Hook J.M., Al-Deen T.S., Hibbert D.B. J. Agric. Food. Chem. 2002, 50:3366.
23. Wells R.J., Cheung J., Hook J.M. Accred. Qual. Assur. 2004, 9:450.
24. Malz F., Jancke H. J. Pharm. Biomed. Anal. 2005, 38:813.
25. Saito T., Ihara T., Koike M., Kinugasa S., Fujimine Y., Nose K., Hirai T. Accred. Qual. Assur. 2009, 14:79.
26. Liu S.-Y., Hu C.-Q. Anal. Chim. Acta 2007, 602:114.
27. Shao G., Kautz R., Peng S., Cui G., Giese R.W. J. Chromatogr., A 2007, 1138:305.
28. Al-Deen T.S., Hibbert D.B., Hook J.M., Wells R.J. Accred. Qual. Assur. 2004, 9:55.
29. Malz F., Jancke H. Anal. Bioanal. Chem. 2006, 385:760.
30. Burton I.W., Quilliam M.A., Walter J.A. Anal. Chem. 2005, 77:3123.
31. Akoka S., Barantin L., Trierweiler M. Anal. Chem. 1999, 71:2554.
32. Remaud G.S., Silvestre V., Akoka S. Accred. Qual. Assur. 2005, 10:415.
33. Krska R., Schothorst R.C., van Egmond H.P., Josephs R.D., Lepschy J., Pettersson H., Chan D., Berthiller F., Schuhmacher R., Kandler W., Parich A., Welzig E. Anal. Bioanal. Chem. 2005, 382:1848.
34. Takatsu A., Eyama S., Saeki M. Accred. Qual. Assur. 2008, 13:409.
35. American Society for Testing and Materials (ASTM) International, Standard Test Method for Purity by Differential Scanning Calorimetry, E 928 - 08, ASTM International, West Conshohocken, PA, USA, 2008.
36. Charsley E.L., Laye P.G., Markham H.M., Le Goff T. Thermochim. Acta 2010, 497:72.
37. Archer D.G. J. Therm. Anal. Calorim. 2006, 85:131.
38. Widmann G., Scherrer O. J. Therm. Anal. Calorim. 1991, 37:1957.
39. Drozdzewska K., Kestens V., Held A., Roebben G., Linsinger T. J. Therm. Anal. Calorim. 2007, 88:757.
40. Kestens V., Roebben G., Linsinger T. Accred. Qual. Assur. 2010, 15:269.
41. International Organization for Standardization (ISO), Reference Materials - General and Statistical Principles for Certification, ISO Guide 35:2006, ISO, Geneva, Switzerland, 2006.
42. Ishikawa K., Hanari N., Shimizu Y., Ihara T., Maeda T., Nomura A., Yarita T., Kato K., Chiba K. Accred. Qual. Assur. 2008, 13:397.
43. Mathkar S., Kumar S., Bystol A., Olawoore K., Min D., Markovich R., Rustum A. J. Pharm. Biomed. Anal. 2009, 49:627.
44. Krska R., Schubert-Ullrich P., Josephs R.D., Emteborg H., Buttinger G., Pettersson H., van Egmond H.P., Schothorst R.C., MacDonald S., Chan D. Anal. Bioanal. Chem. 2007, 388:1215.
45. Yazgan S., Bernreuther A., Ulberth F., Isengard H.-D. Food Chem. 2006, 96:411.
46. American Society for Testing and Materials (ASTM) International, Standard Test Method for Water Using Volumetric Karl Fischer Titration, E 203 - 08, ASTM International, West Conshohocken, PA, USA, 2008.
47. Schöffski K. Food Control 2001, 12:427.
48. American Society for Testing and Materials (ASTM) International, Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration, E 1064 - 08, ASTM International, ASTM International, West Conshohocken, PA, USA, 2008.
49. Cedergren A., Jonsson S. Anal. Chem. 2001, 73:5611.
50. Kestens V., Conneely P., Bernreuther A. Food Chem. 2008, 106:1454.
51. Lanz M., De Caro C.A., Rüegg K., De Agostini A. Food Chem. 2006, 96:431.
52. European Pharmacopoeia, 6th edition, Identification and Control of Residual Solvents, Strasbourg, France, 2006.
53. Sitaramaraju Y., Riadi A., D'Autry W., Wolfs K., Hoogmartens J., Schepdael A.V., Adams E. J. Pharm. Biomed. Anal. 2008, 48:113.
54. Raghani A.R. J. Pharm. Biomed. Anal. 2002, 29:507.
55. Gottlieb H.E., Kotlyar V., Nudelman A. J. Org. Chem. 1997, 62:7512.
56. Ion Chromatography, third ed 2000, 59-80. Wiley-VCH Verlag GmbH, Weinheim, Germany. J.S. Fritz, D.T. Gjerde (Eds.).
57. Krska R., Welzig E., Josephs R.D., Kandler W., Pettersson H., MacDonald S., Charlton A., Brereton P., Hametner C., Berner D., Zöllner P. J. AOAC Int. 2003, 86:722.
58. Yip Y.C., Lam J.C.W., Tong W.F. Trends Anal. Chem. 2009, 28:214.
59. Parker D. Chem. Rev. 1991, 91:1441.
60. Saito K., Yato M., Ito T., Iwasaki Y., Ito R., Matsuki Y., Nakazawa H. Accred. Qual. Assur. 2008, 13:373.
61. Doležalová M., Tkaczyková M. J. Pharm. Biomed. Anal. 2001, 25:407.
62. Szejtli J. Pure Anal. Chem. 2004, 76:1825.
63. Cruz L.A., Hall R. J. Pharm. Biomed. Anal. 2005, 38:8.
64. Sänger-van de Griend C.E., Ek A.G., Widahl-Näsman M.E., Margareta Andersson E.K. J. Pharm. Biomed. Anal. 2006, 41:77.
65. Kagawa M., Machida Y., Nishi H., Haginaka J. J. Pharm. Biomed. Anal. 2005, 38:918.
66. Jaroszewski J.W., Olsson A. J. Pharm. Biomed. Anal. 1994, 12:295.
67. Hembury G.A., Borovkov V.V., Inoue Y. Chem. Rev. 2008, 108:1.
68. Provencher K.A., Wenzel T.J. Tetrahedron: Asymmetry 2008, 19:1797.
69. Wenzel T.J., Bourne C.E., Clark R.L. Tetrahedron: Asymmetry 2009, 20:2052.
70. Zheng Y.S., Zhang C. Org. Lett. 2004, 6:1189.
71. Ema T., Ouchi N., Doi T., Korenaga T., Sakai T. Org. Lett. 2005, 7:3985.
72. Ema T., Tanida D., Sakai T. J. Am. Chem. Soc. 2007, 129:10591.
73. Yang D., Li X., Fan Y.F., Zhang D.W. J. Am. Chem. Soc. 2005, 127:7996.
74. Lewis R.J., Vernoux J.P., Brereton I.M. J. Am. Chem. Soc. 1998, 120:5914.
75. Inoue M., Hirama M. Acc. Chem. Res. 2004, 37:961.
76. Inoue M., Miyazaki K., Ishihara Y., Tatami A., Ohnuma Y., Kawada Y., Komano K., Yamashita S., Lee N., Hirama M. Anal. Chem. 2006, 128:9352.
77. Lewis R.J., Jones A., Vernoux J.P. Anal. Chem. 1999, 71:247.
78. International Organization for Standardization (ISO), General Requirements for the Competence of Reference Material Producers, ISO Guide 34:2009, ISO, Geneva, Switzerland, 2009.
79. Steger H.F. Accred. Qual. Assur. 2003, 8:415.
80. International Organization for Standardization (ISO), General Requirements for the Competence of Testing and Calibration Laboratories, ISO/IEC 17025:2005, ISO, Geneva, Switzerland, 2005.